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X-ray topography characterization of gallium nitride substrates for power device development

Journal Article · · Journal of Crystal Growth
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  1. Stony Brook Univ., NY (United States)
  2. State Univ. of New York Polytechnic Inst., Albany New York
  3. Army Research Lab., Adelphi, MD (United States)
  4. Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
  5. Yale Univ., New Haven, CT (United States)
  6. Arizona State Univ., Tempe, AZ (United States)

Gallium nitride substrates grown by the hydride vapor phase epitaxy (HVPE) method using a patterned growth process have been characterized by synchrotron monochromatic beam X-ray topography in the grazing incidence geometry. Images reveal a starkly heterogeneous distribution of dislocations with areas as large as 0 3 mm2 containing threading dislocation densities below 103 cm-2 in between a grid of strain centers with higher threading dislocation densities (> 104 cm-2). Basal plane dislocation densities in these areas are as low as 104 cm-2. By comparing the recorded images of dislocations with ray tracing simulations of expected dislocations in GaN, the Burgers vectors of the dislocations have been determined. The distribution of threading screw/mixed dislocations (TSDs/TMDs), threading edge dislocations (TEDs) and basal plane dislocations (BPDs) is discussed with implications for fabrication of power devices.

Research Organization:
Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States)
Sponsoring Organization:
USDOE Advanced Research Projects Agency - Energy (ARPA-E)
Grant/Contract Number:
AC04-94AL85000
OSTI ID:
1634813
Alternate ID(s):
OSTI ID: 1775944
Report Number(s):
SAND2020--6126J; 686719
Journal Information:
Journal of Crystal Growth, Journal Name: Journal of Crystal Growth Journal Issue: C Vol. 544; ISSN 0022-0248
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English

References (21)

Characterization of Threading Dislocations in PVT-Grown AlN Substrates via x-Ray Topography and Ray Tracing Simulation journal January 2014
GaN single crystal growth using high-purity Na as a flux journal July 2002
Thermodynamical properties of III–V nitrides and crystal growth of GaN at high N2 pressure journal June 1997
Ammonothermal growth of bulk GaN journal August 2008
Excellent crystallinity of truly bulk ammonothermal GaN journal August 2008
Bulk GaN crystals grown by HVPE journal May 2009
PVT growth of GaN bulk crystals journal March 2011
Direct evidence of micropipe-related pure superscrew dislocations in SiC journal January 1999
Inhomogeneous spatial distribution of reverse bias leakage in GaN Schottky diodes journal March 2001
Analysis of reverse-bias leakage current mechanisms in GaN grown by molecular-beam epitaxy journal January 2004
THE PREPARATION AND PROPERTIES OF VAPOR‐DEPOSITED SINGLE‐CRYSTAL‐LINE GaN journal November 1969
Degradation of hexagonal silicon-carbide-based bipolar devices journal January 2006
Observations of the influence of threading dislocations on the recombination enhanced partial dislocation glide in 4H-silicon carbide epitaxial layers journal April 2007
Direct determination of dislocation sense of closed-core threading screw dislocations using synchrotron white beam x-ray topography in 4H silicon carbide journal October 2007
Synchrotron radiation x-ray topography and defect selective etching analysis of threading dislocations in GaN journal August 2014
CXL. Dislocations in thin plates journal December 1951
Formation of helical dislocations in ammonothermal GaN substrate by heat treatment journal January 2016
GaN Substrate Technologies for Optical Devices journal October 2013
Growth of GaN Crystals by Na Flux Method journal January 2013
Rapid growth of bulk GaN crystal using GaN powder as source material journal January 2005
Grazing Incidence X-ray Topographic Studies of Threading Dislocations in Hydrothermal Grown ZnO Single Crystal Substrates journal January 2013

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