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Microencapsulation of concentrated sulfuric acid with an epoxy vinyl ester shell

Journal Article · · Sandia journal manuscript; Not yet accepted for publication
OSTI ID:1426933
 [1];  [2];  [3];  [4]
  1. Sandia National Lab. (SNL-NM), Albuquerque, NM (United States). Organic Materials Dept.
  2. Sandia National Lab. (SNL-NM), Albuquerque, NM (United States). Center for Integrated Technologies
  3. Washington State Univ., Pullman, WA (United States). Chemistry Dept.
  4. Chicago State Univ., IL (United States). Department of Chemistry and James Franck Institute

Microencapsulation is the process of placing a shell composed of a synthetic or biological polymer completely around another chemical for the purpose of delaying or slowing its release. We report that Sandia National Laboratories was interested in microencapsulating concentrated sulfuric for a specific application. Historically, acids have been encapsulated many times using various techniques. However, the encapsulation of mineral acids has proven difficult due to the lack of a shell material robust enough to prevent premature leakage of the capsule. Using the Polymer-Polymer Incompatibility (PPI) technique, we screened a variety of shell materials and found our best results were with Derakane® 411-350, an epoxy vinyl ester resin (EVER) polymer.

Research Organization:
Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA)
DOE Contract Number:
AC04-94AL85000
OSTI ID:
1426933
Report Number(s):
SAND--2009-2794J; 463477
Journal Information:
Sandia journal manuscript; Not yet accepted for publication, Journal Name: Sandia journal manuscript; Not yet accepted for publication; ISSN 9999-0014
Publisher:
Sandia
Country of Publication:
United States
Language:
English

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