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Role of contamination on the bondline integrity of composite structures

Thesis/Dissertation ·
DOI:https://doi.org/10.2172/1342569· OSTI ID:1342569
 [1]
  1. Iowa State Univ., Ames, IA (United States)

Adhesively bonding composite structures have many applications in aerospace, automotive and submarine industries. The adhesive bonding joints have substantial advantage over the traditional metallic mechanical bonding joints, such as rivet and welding. However, the adhesive bonding joints require additional steps of surface preparation and cleaning to ensure consistent bond strength. In application, the adhesively bonded joints are exposed to environmental degradation and industrial solvent contaminates. Accordingly, the assurance of reliability of bonded composite structures requires detailed investigation of the role of contaminates on bondline integrity. This dissertation focuses on assessing the contaminates effect on the adhesive bondline integrity. A combined experimental and numerical framework is developed to study the contamination effect on the adhesive mechanical properties and adhesive joint strength. The bondline integrity were examined for a system of adhesive (EA9394) and the carbonfiber system (Hexply IM7/8552), after being subjected to different level of exposures to aviation hydraulic fluids and mold cleaning agents. A testing protocol based on nanoindentation for initial screening is used to predict the interfacial fracture characteristics after exposure to contamination. It is found the adhesive modulus and stiffness dropped by up to 10% for the hydraulic fluid contaminates, suggesting increase of the plastic dissipation within the bondline. However, the trend for the cleaning agent was not clear since the modulus drop while its hardness increased.

Research Organization:
Ames Laboratory (AMES), Ames, IA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC02-07CH11358
OSTI ID:
1342569
Report Number(s):
IS--T 3172
Country of Publication:
United States
Language:
English

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