Hydrogen production using ammonia borane

Hamilton, Charles W; Baker, R. Thomas; Semelsberger, Troy A; Shrestha, Roshan P

Hydrogen production using ammonia borane

Patent · Mon Dec 23 23:00:00 EST 2013

OSTI ID:1111472

Hamilton, Charles W; Baker, R. Thomas; Semelsberger, Troy A; Shrestha, Roshan P

Hydrogen ("H.sub.2") is produced when ammonia borane reacts with a catalyst complex of the formula L.sub.nM-X wherein M is a base metal such as iron, X is an anionic nitrogen- or phosphorus-based ligand or hydride, and L is a neutral ancillary ligand that is a neutral monodentate or polydentate ligand.

Research Organization:: LANL (Los Alamos National Laboratory (LANL), Los Alamos, NM (United States))

Sponsoring Organization:: USDOE

DOE Contract Number:: AC52-06NA25396

Assignee:: Los Alamos National Security, LLC (Los Alamos, NM)

Patent Number(s):: 8,613,902

Application Number:: 12/416,835

OSTI ID:: 1111472

Country of Publication:: United States

Language:: English

References (9)

The Metal−Ligand Bifunctional Catalysis: A Theoretical Study on the Ruthenium(II)-Catalyzed Hydrogen Transfer between Alcohols and Carbonyl Compounds Yamakawa, Masashi; Ito, Hisashi; Noyori, Ryoji Journal of the American Chemical Society, Vol. 122, Issue 7 https://doi.org/10.1021/ja991638h	journal	February 2000
Transition Metal-Catalyzed Formation of Boron−Nitrogen Bonds: Catalytic Dehydrocoupling of Amine-Borane Adducts to Form Aminoboranes and Borazines Jaska, Cory A.; Temple, Karen; Lough, Alan J. Journal of the American Chemical Society, Vol. 125, Issue 31 https://doi.org/10.1021/ja030160l	journal	August 2003
Thermal decomposition of B–N–H compounds investigated by using combined thermoanalytical methods Baitalow, F.; Baumann, J.; Wolf, G. Thermochimica Acta, Vol. 391, Issue 1-2 https://doi.org/10.1016/S0040-6031(02)00173-9	journal	August 2002
Amineborane-Based Chemical Hydrogen Storage: Enhanced Ammonia Borane Dehydrogenation in Ionic Liquids Bluhm, Martin E.; Bradley, Mark G.; Butterick, Robert Journal of the American Chemical Society, Vol. 128, Issue 24 https://doi.org/10.1021/ja062085v	journal	June 2006
Efficient Catalysis of Ammonia Borane Dehydrogenation Denney, Melanie C.; Pons, Vincent; Hebden, Travis J. Journal of the American Chemical Society, Vol. 128, Issue 37 https://doi.org/10.1021/ja062419g	journal	September 2006
Ruthenium-Catalyzed Dehydrogenation of Ammonia Boranes Blaquiere, Nicole; Diallo-Garcia, Sarah; Gorelsky, Serge I. Journal of the American Chemical Society, Vol. 130, Issue 43 https://doi.org/10.1021/ja804235t	journal	October 2008
Base Metal Catalyzed Dehydrogenation of Ammonia−Borane for Chemical Hydrogen Storage Keaton, Richard J.; Blacquiere, Johanna M.; Baker, R. Tom Journal of the American Chemical Society, Vol. 129, Issue 7 https://doi.org/10.1021/ja066860i	journal	February 2007
Acid Initiation of Ammonia–Borane Dehydrogenation for Hydrogen Storage Stephens, Frances H.; Baker, R. Tom; Matus, Myrna H. Angewandte Chemie International Edition, Vol. 46, Issue 5 https://doi.org/10.1002/anie.200603285	journal	January 2007
Ruthenium Complexes with Cooperative PNP Ligands: Bifunctional Catalysts for the Dehydrogenation of Ammonia-Borane Käß, Martina; Friedrich, Anja; Drees, Markus Angewandte Chemie International Edition, Vol. 48, Issue 5 https://doi.org/10.1002/anie.200805108	journal	January 2009

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