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Title: Synthesis of iron based hydrocracking catalysts

Patent ·
OSTI ID:868793

A method of preparing a fine particle iron based hydrocracking catalyst and the catalyst prepared thereby. An iron (III) oxide powder and elemental sulfur are reacted with a liquid hydrogen donor having a hydroaromatic structure present in the range of from about 5 to about 50 times the weight of iron (III) oxide at a temperature in the range of from about 180.degree. C. to about 240.degree. C. for a time in the range of from about 0 to about 8 hours. Various specific hydrogen donors are disclosed. The catalysts are active at low temperature (<350.degree. C.) and low pressure.

Research Organization:
National Energy Technology Laboratory (NETL), Pittsburgh, PA, Morgantown, WV (United States); USDOE Pittsburgh Energy Technology Center (PETC), PA (United States)
Assignee:
United States of America as represented by United States (Washington, DC)
Patent Number(s):
US 5214015
OSTI ID:
868793
Country of Publication:
United States
Language:
English

References (4)

Finely dispersed iron, iron-molybdenum, and sulfated iron oxides as catalysts for coprocessing reactions journal September 1991
Catalysis in direct coal liquefaction by sulfated metal oxides journal May 1991
Iron compounds and iron catalysts: Activity in reactions relevant to direct coal liquefaction journal December 1991
Catalytic roles of iron and hydrogen sulphide on hydrogenation of coal journal May 1984