Summary and Evaluation of NRC-Sponsored Stellite 6 Aging and Friction Tests
This report describes four sets of tests sponsored by the U.S. Nuclear Regulatory Commission and conducted by the Idaho National Engineering and Environmental Laboratory. The tests support research addressing the need to provide assurance that motor-operated valves are able to perform their intended safety function, usually to open or close against specified (design basis) flow and pressure loads. One of the parameters that affects a gate valve's operability is the friction between the disc seats and the valve body seats. In most gate valves, these surfaces are hardfaced with Stellite 6, a cobalt-based alloy. The tests described in this report investigate the changes that occur in the friction as the Stellite 6 surfaces develop an oxide film as they age. Stellite 6 specimens were aged in a corrosion autoclave, the oxide films were examined and characterized, and the specimens were subjected to friction testing in a friction autoclave. A very thin oxide film formed after only a fe w days of natural aging. Even a very thin oxide film caused an increase in friction. The surface structure of the oxide film was dominated by a hard crystalline structure, such that the friction response was analogous to rubbing two pieces of sandpaper together. In the limited data provided by naturally aged specimens (78 days maximum exposure, very thin oxide films), the friction increased with greater aging time, approaching an as-yet-undetermined plateau. Although the thickness of the oxide film increased with greater aging time, the mechanical properties of the oxide film (larger granules with greater aging time) appeared to play a greater role in the friction response. Friction testing of specimens subjected to simulated in-service testing strokes at intervals during the aging process showed only a slight decrease in friction, compared to other specimens. Results from specimens subjected to accelerated aging were inconclusive, because of differences in the structure and comp osition of the oxide films, compared to naturally aged specimens. For the naturally aged specimens, the highest friction occurred on the first stroke. The first stroke smeared the oxide film and dislodged some of the granules, so that subsequent strokes saw lower friction values and less variation in the friction. This result underscores the importance of planning in-plant tests so that data are collected from the first stroke following a period of inactivity.
- Research Organization:
- Idaho National Lab. (INL), Idaho Falls, ID (United States)
- Sponsoring Organization:
- US Department of Energy (US)
- DOE Contract Number:
- AC07-94ID13223
- OSTI ID:
- 766386
- Report Number(s):
- INEEL/EXT-99-00116; TRN: AH200038%%514
- Resource Relation:
- Other Information: PBD: 1 Apr 1999
- Country of Publication:
- United States
- Language:
- English
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