WIPP waste characterization program sampling and analysis guidance manual

Technical Report · Tue Jan 01 00:00:00 EST 1991

DOI:https://doi.org/10.2172/5784654· OSTI ID:5784654

The Waste Isolation Pilot Plant (WIPP) Waste Characterization Program Sampling and Analysis Guidance Manual (Guidance Manual) provides a unified source of information on the sampling and analytical techniques that enable Department of Energy (DOE) facilities to comply with the requirements established in the current revision of the Quality Assurance Program Plan (QAPP) for the WIPP Experimental-Waste Characterization Program (the Program). This Guidance Manual includes all of the sampling and testing methodologies accepted by the WIPP Project Office (DOE/WPO) for use in implementing the Program requirements specified in the QAPP. This includes methods for characterizing representative samples of transuranic (TRU) wastes at DOE generator sites with respect to the gas generation controlling variables defined in the WIPP bin-scale and alcove test plans, as well as waste container headspace gas sampling and analytical procedures to support waste characterization requirements under the WIPP test program and the Resource Conservation and Recovery Act (RCRA). The procedures in this Guidance Manual are comprehensive and detailed and are designed to provide the necessary guidance for the preparation of site specific procedures. The use of these procedures is intended to provide the necessary sensitivity, specificity, precision, and comparability of analyses and test results. The solutions to achieving specific program objectives will depend upon facility constraints, compliance with DOE Orders and DOE facilities' operating contractor requirements, and the knowledge and experience of the TRU waste handlers and analysts. With some analytical methods, such as gas chromatography/mass spectrometry, the Guidance Manual procedures may be used directly. With other methods, such as nondestructive/destructive characterization, the Guidance Manual provides guidance rather than a step-by-step procedure.

• Research Organization: Westinghouse Electric Corp., Carlsbad, NM (United States). Waste Isolation Div.
• Sponsoring Organization: USDOE; USDOE, Washington, DC (United States)
• DOE Contract Number: AC04-86AL31950
• OSTI ID: 5784654
• Report Number(s): DOE/WIPP-91-043; ON: DE92005367
• Resource Relation: Other Information: PBD: [1991]
• Country of Publication: United States
• Language: English

Related Subjects

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE WASTES FROM NUCLEAR FACILITIES
37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
ALPHA-BEARING WASTES
CHEMICAL ANALYSIS
SAMPLING
MANUALS
ORGANIC COMPOUNDS
CALIBRATION
CLEANING
CONTAINERS
GAS CHROMATOGRAPHY
GASEOUS WASTES
MASS SPECTROMETERS
MEASURING INSTRUMENTS
PRESSURE GAGES
QUALITY ASSURANCE
QUALITY CONTROL
SPECTROPHOTOMETRY
TEMPERATURE MEASUREMENT
WIPP
CHROMATOGRAPHY
CONTROL
DOCUMENT TYPES
FUNCTIONAL MODELS
MATERIALS
NATIONAL ORGANIZATIONS
NUCLEAR FACILITIES
PILOT PLANTS
RADIOACTIVE MATERIALS
RADIOACTIVE WASTE FACILITIES
RADIOACTIVE WASTES
SEPARATION PROCESSES
SPECTROMETERS
UNDERGROUND FACILITIES
US DOE
US ORGANIZATIONS
WASTES
052002* - Nuclear Fuels- Waste Disposal & Storage
400102 - Chemical & Spectral Procedures