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Title: Method for recovering valuable elements from precombustion coal-based materials

Patent ·
OSTI ID:2293898

A method for recovering valuable elements from pre-combustion coal-based materials includes the steps of grinding the materials to a predetermined size, roasting the ground materials at a temperature of 600° C.-700° C. for a predetermined residence time needed for mineral decomposition, submerging the roasted, ground materials in a solution of lixiviant, filtering the lixiviant solution to separate residual solids from a pregnant leach solution including the valuable elements and recovering and concentrating the valuable elements from the pregnant leach solution.

Research Organization:
Univ. of Kentucky, Lexington, KY (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
FE0031525
Assignee:
University of Kentucky Research Foundation (Lexington, KY)
Patent Number(s):
11,821,054
Application Number:
16/832,157
OSTI ID:
2293898
Resource Relation:
Patent File Date: 03/27/2020
Country of Publication:
United States
Language:
English

References (20)

Kinetics of mixed rare earths minerals decomposed by CaO with NaCl-CaCl2 melting salt journal December 2010
High temperature dephosphorization behavior of monazite concentrate with charred coal journal December 2010
A review on the cracking, baking and leaching processes of rare earth element concentrates journal August 2017
Application of sequential extraction and hydrothermal treatment for characterization and enrichment of rare earth elements from coal fly ash journal November 2018
Characterization and recovery of rare earth elements and other critical metals (Co, Cr, Li, Mn, Sr, and V) from the calcination products of a coal refuse sample journal May 2020
Effect of pretreatment on synchysite-Ce (CaCe(CO3)2F) leaching journal July 2007
Influence of NaCl-CaCl2 on Decomposing REPO4 with CaO journal December 2007
Thermal treatment for the separation of phosphate and recovery of rare earth metals (REMs) from Korean monazite journal January 2015
Effect of Pre-reaction Ball Milling on Kinetics of Lanthanum Phosphate Roasting with Sodium Carbonate journal April 2018
Kinetics of Roasting Decomposition of the Rare Earth Elements by CaO and Coal journal June 2017
Chemical extraction of rare earth elements from coal ash journal November 2017
Chlorination kinetics of fluorine-fixed rare earth concentrate journal July 2003
Process development to recover rare earth metals from monazite mineral: A review journal August 2015
Enhanced leachability of rare earth elements from calcined products of bituminous coals journal October 2019
Reaction process of monazite and bastnaesite mixed rare earth minerals calcined by CaO-NaCl-CaCl2 journal August 2007
Study on Roasting Decomposition of Mixed Rare Earth Concentrate in CaO-NaCl-CaCl2 journal December 2006
Calcination pretreatment effects on acid leaching characteristics of rare earth elements from middlings and coarse refuse material associated with a bituminous coal source journal August 2019
Mechanochemical decomposition of monazite to assist the extraction of rare earth elements journal November 2009
Lithium leaching recovery and mechanisms from density fractions of an Illinois Basin bituminous coal journal May 2020
Leaching kinetics of rare earth elements and fluoride from mixed rare earth concentrate after roasting with calcium hydroxide and sodium hydroxide journal November 2017