Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates

Gao, Pu-Xian; Lu, Xingxu; Hoang, Son

Title: Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates

Patent · Tue Oct 11 00:00:00 EDT 2022

OSTI ID:1986672

Gao, Pu-Xian; Lu, Xingxu; Hoang, Son

A method of making a titanium dioxide nanowire array includes contacting a substrate with a solvent comprising a titanium (III) precursor, an acid, and an oxidant while microwave heating the solvent, thereby forming a hydrogen titanate H2Ti2O5.H2O nanowire array. The hydrogen titanate nanowire array is annealed to form a titanium dioxide nanowire array. The substrate is seeded with titanium dioxide before starting the hydrothermal synthesis of the hydrogen titanate nanowire array. The titanium dioxide nanowire array is loaded with a platinum group metal to form an exhaust gas catalyst. The titanium dioxide nanowire array can be used to catalyze oxidation of combustion exhaust.

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Research Organization:: Univ. of Connecticut, Storrs, CT (United States)

Sponsoring Organization:: USDOE; National Science Foundation (NSF)

DOE Contract Number:: EE0006854; CBET-1344792

Assignee:: The University of Connecticut (Farmington, CT)

Patent Number(s):: 11,465,129

Application Number:: 16/465,969

OSTI ID:: 1986672

Resource Relation:: Patent File Date: 06/01/2018

Country of Publication:: United States

Language:: English

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