Biologically inspired reinforcement using polydopamine of polymer bound composites

Herman, Matthew Joseph; Liu, Cheng; Watkins, Erik Benjamin; Miller, Nathan Andrew; Duque, Amanda Lynn; Yeager, John David

doi:10.1016/j.compositesb.2023.110563

Title: Biologically inspired reinforcement using polydopamine of polymer bound composites

Journal Article · Tue Jan 31 00:00:00 EST 2023 · Composites. Part B, Engineering

DOI:https://doi.org/10.1016/j.compositesb.2023.110563· OSTI ID:1923638

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Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

Interfacial strength plays a critical role in the mechanical properties of a composite system. In this work, a proven mock high explosive (HE), 5-iodo-2’-deoxyuridine (IDOX) was coated by the adhesive promoting polymer polydopamine (PDA), then formulated with an Estane binder system to form an improved HE mock composite. An extensive comparison study of mechanical properties was performed to determine the effects, if any, of PDA on the composite system. To aid in interpretation of the mechanical test data, neutron reflectometry experiments were performed to determine the thickness and structure of the as deposited PDA films. The mechanical performance of PDA-treated IDOX was then compared to untreated specimens by compression testing in the Brazilian disk geometry. The results strongly suggested that the structure of PDA consists of two layers: one low in density caused by polymer agglomerates attaching to the substrate during polymerization, and the second high in density caused by controlled linear deposition of polydopamine. Finally, the mechanical testing showed that PDA greatly increased the stiffness and yield strength of IDOX based mocks without causing any disruption to the underlying crystal system.

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Research Organization:: Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA); USDOE Laboratory Directed Research and Development (LDRD) Program

Grant/Contract Number:: 89233218CNA000001

OSTI ID:: 1923638

Alternate ID(s):: OSTI ID: 1961236

Report Number(s):: LA-UR-22-25031

Journal Information:: Composites. Part B, Engineering, Vol. 254; ISSN 1359-8368

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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Title: Biologically inspired reinforcement using polydopamine of polymer bound composites

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