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Title: Effect of aging on failure mechanism of Alloy 709 at various temperatures

Journal Article · · Materials Characterization
 [1];  [2];  [1]
  1. North Carolina State Univ., Raleigh, NC (United States). Dept. of Mechanical and Aerospace Engineering. Advanced Materials Research Laboratory (AMRL)
  2. Univ. of Birmingham (United Kingdom). School of Metallurgy and Materials

Alloy 709 is a novel austenitic stainless steel with high temperature creep strength, weldability, and corrosion resistance. These properties make the material suitable for applications in the structure of next-generation nuclear power plants. Enduring high temperatures for an extended period of time in the harsh environments of a nuclear power plant results in thermal aging of the material. Therefore, it is imperative to study the effect of thermal aging on the microstructure and mechanical properties of Alloy 709 before its application in the next generation power plants. In this study, hot-processed (forged + rolled), annealed and quenched ingots of Alloy 709 are aged at 650 °C for 2000 h in air and then tested at various temperatures up to 850 °C in an in-situ heating-loading Scanning Electron Microscope (SEM) equipped with Energy Dispersive Spectroscopy (EDS) and Electron Backscatter Diffraction (EBSD). The effect of testing temperature and aging on microstructural evolutions during tensile testing of as-received and aged samples are studied. Furthermore, both as-received and aged samples displayed serrations and drop in ductility at elevated temperatures, due to the effect of dynamic strain aging (DSA). The occurrence of DSA activity was found within temperatures range of 500 °C–750 °C in as-received and 550 °C - 650 °C in aged samples. The aged samples showed less elongation accompanied by shallower dimples on the fractured surface, indicating less ductile failure mechanism compared to as-received samples. Failure mechanism observations on the fracture surface using SEM fractography are correlated to the observations made on the sample surface using in-situ SEM to achieve a complementary set of information to better understand the failure mechanism of this novel alloy.

Research Organization:
North Carolina State University, Raleigh, NC (United States)
Sponsoring Organization:
USDOE Office of Nuclear Energy (NE); Research Council of the United Kingdom (RCUK)
Grant/Contract Number:
NE0008451; EP/N016351/1
OSTI ID:
1850488
Alternate ID(s):
OSTI ID: 1778601
Journal Information:
Materials Characterization, Vol. 171, Issue C; ISSN 1044-5803
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English

References (14)

Evaluation of the Effects of Thermal Aging of Austenitic Stainless Steel Welds Using Small Punch Test journal January 2015
Microstructural evolution of Alloy 709 during aging journal August 2019
A Re-examination of the Portevin-Le Chatelier Effect in Alloy 718 in Connection with Oxidation-Assisted Intergranular Cracking journal August 2014
Mechanism of dynamic strain aging and characterization of its effect on the low-cycle fatigue behavior in type 316L stainless steel journal April 2005
A study on tensile properties of Alloy 709 at various temperatures journal August 2018
Structural materials for Gen-IV nuclear reactors: Challenges and opportunities journal December 2008
Effects of dynamic strain aging on the subsequent mechanical properties of carbon steels journal December 1978
Dynamic Strain Ageing Behaviour of Modified 9Cr-1Mo Steel Under Monotonic and Cyclic Loading journal January 2017
Dynamic Strain Aging of Various Steels journal October 1982
Serrated yielding in an advanced stainless steel Fe-25Ni-20Cr (wt%) journal March 2019
Generation-IV nuclear power: A review of the state of the science journal December 2008
Deformation microstructure and tensile properties of Alloy 709 at different temperatures journal August 2019
Effect of dynamic strain aging on high temperature properties of austenitic stainless steel journal August 2004
Serrated plastic flow journal September 1984

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