ac Sensing Using Nitrogen-Vacancy Centers in a Diamond Anvil Cell up to 6 GPa

Wang, Z.; McPherson, C.; Kadado, R.; Brandt, N.; Edwards, S.; Casey, W. H.; Curro, N. J.

doi:10.1103/physrevapplied.16.054014

Title: ac Sensing Using Nitrogen-Vacancy Centers in a Diamond Anvil Cell up to 6 GPa

Journal Article · Fri Nov 05 00:00:00 EDT 2021 · Physical Review Applied

DOI:https://doi.org/10.1103/physrevapplied.16.054014· OSTI ID:1830753

Wang, Z. ^[1]; McPherson, C. ^[1]; Kadado, R. ^[1]; Brandt, N. ^[1];

^[1];

^[1]

Univ. of California, Davis, CA (United States)

Nitrogen-vacancy color centers in diamond have attracted broad attention as quantum sensors for both static and dynamic magnetic, electrical, strain, and thermal fields and are particularly attractive for quantum sensing under pressure in diamond anvil cells. Optically based nuclear magnetic resonance may be possible at pressures greater than a few gigapascals and offers an attractive alternative to conventional Faraday-induction-based detection. In this work, we present ac sensing results and demonstrate synchronized readout up to 6 GPa but find that the sensitivity is reduced due to inhomogeneities of the microwave field and pressure within the sample space. These experiments enable the possibility of all-optical high resolution magnetic resonance of nanoliter sample volumes at high pressures.

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Research Organization:: Univ. of California, Davis, CA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Chemical Sciences, Geosciences & Biosciences Division

Grant/Contract Number:: FG02-05ER15693

OSTI ID:: 1830753

Journal Information:: Physical Review Applied, Vol. 16, Issue 5; ISSN 2331-7019

Publisher:: American Physical Society (APS)Copyright Statement

Country of Publication:: United States

Language:: English

References (51)

Electronic Properties and Metrology Applications of the Diamond ${NV}^{-}$ Center under Pressure Doherty, Marcus W.; Struzhkin, Viktor V.; Simpson, David A. Physical Review Letters, Vol. 112, Issue 4 https://doi.org/10.1103/PhysRevLett.112.047601	journal	January 2014
Novel color center platforms enabling fundamental scientific discovery Norman, Victoria A.; Majety, Sridhar; Wang, Zhipan InfoMat, Vol. 3, Issue 8 https://doi.org/10.1002/inf2.12128	journal	June 2020
Diamond formation due to a pH drop during fluid–rock interactions Sverjensky, Dimitri A.; Huang, Fang Nature Communications, Vol. 6, Issue 1 https://doi.org/10.1038/ncomms9702	journal	November 2015
NMR signal averaging in 62T pulsed fields Meier, Benno; Greiser, Sebastian; Haase, Jürgen Journal of Magnetic Resonance, Vol. 210, Issue 1 https://doi.org/10.1016/j.jmr.2011.02.007	journal	May 2011
Measuring magnetic field texture in correlated electron systems under extreme conditions Yip, King Yau; Ho, Kin On; Yu, King Yiu Science, Vol. 366, Issue 6471 https://doi.org/10.1126/science.aaw4278	journal	December 2019
Quantum diamond spectrometer for nanoscale NMR and ESR spectroscopy Bucher, Dominik B.; Aude Craik, Diana P. L.; Backlund, Mikael P. Nature Protocols, Vol. 14, Issue 9 https://doi.org/10.1038/s41596-019-0201-3	journal	August 2019
Imaging stress and magnetism at high pressures using a nanoscale quantum sensor Hsieh, S.; Bhattacharyya, P.; Zu, C. Science, Vol. 366, Issue 6471 https://doi.org/10.1126/science.aaw4352	journal	December 2019
Water in the deep Earth: The dielectric constant and the solubilities of quartz and corundum to 60kb and 1200°C Sverjensky, Dimitri A.; Harrison, Brandon; Azzolini, David Geochimica et Cosmochimica Acta, Vol. 129 https://doi.org/10.1016/j.gca.2013.12.019	journal	March 2014
Wide frequency dielectric properties of CVD diamond Ibarra, A.; González, M.; Vila, R. Diamond and Related Materials, Vol. 6, Issue 5-7 https://doi.org/10.1016/S0925-9635(96)00724-8	journal	April 1997
Optically detected magnetic resonance of high-density ensemble of NV ⁻ centers in diamond Matsuzaki, Y.; Morishita, H.; Shimooka, T. Journal of Physics: Condensed Matter, Vol. 28, Issue 27 https://doi.org/10.1088/0953-8984/28/27/275302	journal	May 2016
Submillihertz magnetic spectroscopy performed with a nanoscale quantum sensor Schmitt, Simon; Gefen, Tuvia; Stürner, Felix M. Science, Vol. 356, Issue 6340 https://doi.org/10.1126/science.aam5532	journal	May 2017
Activation and Reaction Volumes in Solution. 3 Drljaca, A.; Hubbard, C. D.; van Eldik, R. Chemical Reviews, Vol. 98, Issue 6 https://doi.org/10.1021/cr970461b	journal	September 1998
Magnetic measurements on micrometer-sized samples under high pressure using designed NV centers Lesik, Margarita; Plisson, Thomas; Toraille, Loïc Science, Vol. 366, Issue 6471 https://doi.org/10.1126/science.aaw4329	journal	December 2019
Pressure calibration of diamond anvil Raman gauge to 310GPa Akahama, Yuichi; Kawamura, Haruki Journal of Applied Physics, Vol. 100, Issue 4 https://doi.org/10.1063/1.2335683	journal	August 2006
Coherence levels and coherence pathways in NMR. A simple way to design phase cycling procedures Bain, Alex D. Journal of Magnetic Resonance (1969), Vol. 56, Issue 3 https://doi.org/10.1016/0022-2364(84)90305-6	journal	February 1984
Pressure and temperature dependence of the longitudinal proton relaxation times in supercooled water to −87 °C and 2500 bar Lang, E.; Lüdemann, H. ‐D. The Journal of Chemical Physics, Vol. 67, Issue 2 https://doi.org/10.1063/1.434878	journal	July 1977
Activation and reaction volumes in solution Asano, T.; Le Noble, W. J. Chemical Reviews, Vol. 78, Issue 4 https://doi.org/10.1021/cr60314a004	journal	August 1978
NMR at pressures up to 90 GPa Meier, Thomas; Khandarkhaeva, Saiana; Petitgirard, Sylvain Journal of Magnetic Resonance, Vol. 292 https://doi.org/10.1016/j.jmr.2018.05.002	journal	July 2018
Hyperfine interaction in the ground state of the negatively charged nitrogen vacancy center in diamond Felton, S.; Edmonds, A. M.; Newton, M. E. Physical Review B, Vol. 79, Issue 7 https://doi.org/10.1103/PhysRevB.79.075203	journal	February 2009
Magnetic flux tailoring through Lenz lenses for ultrasmall samples: A new pathway to high-pressure nuclear magnetic resonance Meier, Thomas; Wang, Nan; Mager, Dario Science Advances, Vol. 3, Issue 12 https://doi.org/10.1126/sciadv.aao5242	journal	December 2017
NMR probe for high pressure and high temperature de Langen, M.; Prins, K. O. Review of Scientific Instruments, Vol. 66, Issue 11 https://doi.org/10.1063/1.1146087	journal	November 1995
Epitaxial diamond encapsulation of metal microprobes for high pressure experiments Weir, Samuel T.; Akella, Jagannadham; Aracne-Ruddle, Chantel Applied Physics Letters, Vol. 77, Issue 21 https://doi.org/10.1063/1.1326838	journal	November 2000
Design and Analysis of Microcoils for NMR Microscopy Peck, T. L.; Magin, R. L.; Lauterbur, P. C. Journal of Magnetic Resonance, Series B, Vol. 108, Issue 2, p. 114-124 https://doi.org/10.1006/jmrb.1995.1112	journal	August 1995
The nitrogen-vacancy colour centre in diamond Doherty, Marcus W.; Manson, Neil B.; Delaney, Paul Physics Reports, Vol. 528, Issue 1 https://doi.org/10.1016/j.physrep.2013.02.001	journal	July 2013
Improving resolution of solid state NMR in dense molecular hydrogen Meier, Thomas; Khandarkhaeva, Saiana; Jacobs, Jeroen Applied Physics Letters, Vol. 115, Issue 13 https://doi.org/10.1063/1.5123232	journal	September 2019
Hyperpolarization-Enhanced NMR Spectroscopy with Femtomole Sensitivity Using Quantum Defects in Diamond Bucher, Dominik B.; Glenn, David R.; Park, Hongkun Physical Review X, Vol. 10, Issue 2 https://doi.org/10.1103/PhysRevX.10.021053	journal	June 2020
Perspectives of shaped pulses for EPR spectroscopy Spindler, Philipp E.; Schöps, Philipp; Kallies, Wolfgang Journal of Magnetic Resonance, Vol. 280 https://doi.org/10.1016/j.jmr.2017.02.023	journal	July 2017
Activation and reaction volumes in solution. 2 Van Eldik, R.; Asano, T.; Le Noble, W. J. Chemical Reviews, Vol. 89, Issue 3 https://doi.org/10.1021/cr00093a005	journal	May 1989
Simple clamp pressure cell up to 30 kbar Fujiwara, Hiroshi; Kadomatsu, Hideoki; Tohma, Kiyokazu Review of Scientific Instruments, Vol. 51, Issue 10 https://doi.org/10.1063/1.1136061	journal	October 1980
Magnetic Sensing inside a Diamond Anvil Cell via Nitrogen-Vacancy Center Spins ^* Shang, Yan-Xing; Hong, Fang; Dai, Jian-Hong Chinese Physics Letters, Vol. 36, Issue 8 https://doi.org/10.1088/0256-307X/36/8/086201	journal	August 2019
Diamond NV centers for quantum computing and quantum networks Childress, Lilian; Hanson, Ronald MRS Bulletin, Vol. 38, Issue 2 https://doi.org/10.1557/mrs.2013.20	journal	February 2013
² H and ¹³⁹ La NMR Spectroscopy in Aqueous Solutions at Geochemical Pressures Ochoa, Gerardo; Pilgrim, Corey D.; Martin, Michele N. Angewandte Chemie International Edition, Vol. 54, Issue 51 https://doi.org/10.1002/anie.201507773	journal	September 2015
Ruby under pressure Syassen, K. High Pressure Research, Vol. 28, Issue 2 https://doi.org/10.1080/08957950802235640	journal	June 2008
Carbon speciation in saline solutions in equilibrium with aragonite at high pressure Facq, Sébastien; Daniel, Isabelle; Montagnac, Gilles Chemical Geology, Vol. 431 https://doi.org/10.1016/j.chemgeo.2016.03.021	journal	August 2016
Dielectric properties of water under extreme conditions and transport of carbonates in the deep Earth Pan, D.; Spanu, L.; Harrison, B. Proceedings of the National Academy of Sciences, Vol. 110, Issue 17 https://doi.org/10.1073/pnas.1221581110	journal	March 2013
In situ Raman study and thermodynamic model of aqueous carbonate speciation in equilibrium with aragonite under subduction zone conditions Facq, Sébastien; Daniel, Isabelle; Montagnac, Gilles Geochimica et Cosmochimica Acta, Vol. 132 https://doi.org/10.1016/j.gca.2014.01.030	journal	May 2014
High-resolution magnetic resonance spectroscopy using a solid-state spin sensor Glenn, David R.; Bucher, Dominik B.; Lee, Junghyun Nature, Vol. 555, Issue 7696 https://doi.org/10.1038/nature25781	journal	March 2018
Long-time electron spin storage via dynamical suppression of hyperfine-induced decoherence in a quantum dot Zhang, Wenxian; Konstantinidis, N. P.; Dobrovitski, V. V. Physical Review B, Vol. 77, Issue 12 https://doi.org/10.1103/PhysRevB.77.125336	journal	March 2008
Superconductivity at 250 K in lanthanum hydride under high pressures Drozdov, A. P.; Kong, P. P.; Minkov, V. S. Nature, Vol. 569, Issue 7757 https://doi.org/10.1038/s41586-019-1201-8	journal	May 2019
Quantum sensing Degen, C. L.; Reinhard, F.; Cappellaro, P. Reviews of Modern Physics, Vol. 89, Issue 3 https://doi.org/10.1103/RevModPhys.89.035002	journal	July 2017
New, compensated Carr-Purcell sequences Gullion, Terry; Baker, David B.; Conradi, Mark S. Journal of Magnetic Resonance (1969), Vol. 89, Issue 3 https://doi.org/10.1016/0022-2364(90)90331-3	journal	October 1990
Anvil cell gasket design for high pressure nuclear magnetic resonance experiments beyond 30 GPa Meier, Thomas; Haase, Jürgen Review of Scientific Instruments, Vol. 86, Issue 12 https://doi.org/10.1063/1.4939057	journal	December 2015
Conventional superconductivity at 203 kelvin at high pressures in the sulfur hydride system Drozdov, A. P.; Eremets, M. I.; Troyan, I. A. Nature, Vol. 525, Issue 7567 https://doi.org/10.1038/nature14964	journal	August 2015
Optically detected magnetic resonance of nitrogen vacancies in a diamond anvil cell using designer diamond anvils Steele, L. G.; Lawson, M.; Onyszczak, M. Applied Physics Letters, Vol. 111, Issue 22 https://doi.org/10.1063/1.5004153	journal	November 2017
The signal-to-noise ratio of the nuclear magnetic resonance experiment Hoult, D. I.; Richards, R. E. Journal of Magnetic Resonance (1969), Vol. 24, Issue 1, p. 71-85 https://doi.org/10.1016/0022-2364(76)90233-X	journal	October 1976
A High-Pressure, High-Resolution NMR Probe for Experiments at 500 MHz Ballard, Lance; Yu, Aimee; Reiner, Carl Journal of Magnetic Resonance, Vol. 133, Issue 1 https://doi.org/10.1006/jmre.1998.1463	journal	July 1998
Evidence for Superconductivity above 260 K in Lanthanum Superhydride at Megabar Pressures Somayazulu, Maddury; Ahart, Muhtar; Mishra, Ajay K. Physical Review Letters, Vol. 122, Issue 2 https://doi.org/10.1103/PhysRevLett.122.027001	journal	January 2019
Evolution of hyperfine parameters across a quantum critical point in ${CeRhIn}_{5}$ Lin, C. H.; Shirer, K. R.; Crocker, J. Physical Review B, Vol. 92, Issue 15 https://doi.org/10.1103/PhysRevB.92.155147	journal	October 2015
Nonmagnetic indenter-type high-pressure cell for magnetic measurements Kobayashi, T. C.; Hidaka, H.; Kotegawa, H. Review of Scientific Instruments, Vol. 78, Issue 2 https://doi.org/10.1063/1.2459512	journal	February 2007
Multipulse Double-Quantum Magnetometry with Near-Surface Nitrogen-Vacancy Centers Mamin, H. J.; Sherwood, M. H.; Kim, M. Physical Review Letters, Vol. 113, Issue 3 https://doi.org/10.1103/PhysRevLett.113.030803	journal	July 2014
High-sensitivity NMR beyond 200,000 atmospheres of pressure Meier, T.; Reichardt, S.; Haase, J. Journal of Magnetic Resonance, Vol. 257 https://doi.org/10.1016/j.jmr.2015.05.007	journal	August 2015

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