Deep Eutectic Solvents: A Review of Fundamentals and Applications

Hansen, Benworth B.; Spittle, Stephanie; Chen, Brian; Poe, Derrick; Zhang, Yong; Klein, Jeffrey M.; Horton, Alexandre; Adhikari, Laxmi; Zelovich, Tamar; Doherty, Brian W.; Gurkan, Burcu; Maginn, Edward J.; Ragauskas, Arthur; Dadmun, Mark; Zawodzinski, Thomas A.; Baker, Gary A.; Tuckerman, Mark E.; Savinell, Robert F.; Sangoro, Joshua R.

doi:10.1021/acs.chemrev.0c00385

Title: Deep Eutectic Solvents: A Review of Fundamentals and Applications

Journal Article · Mon Dec 14 00:00:00 EST 2020 · Chemical Reviews

DOI:https://doi.org/10.1021/acs.chemrev.0c00385· OSTI ID:1808446

Hansen, Benworth B. ^[1]; Spittle, Stephanie ^[1];

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Univ. of Tennessee, Knoxville, TN (United States)
Case Western Reserve Univ., Cleveland, OH (United States)
Univ. of Notre Dame, IN (United States)
Univ. of Missouri, Columbia, MO (United States)
New York Univ. (NYU), NY (United States)

Deep eutectic solvents (DESs) are an emerging class of mixtures characterized by significant depressions in melting points compared to those of the neat constituent components. These green materials are promising for applications as inexpensive ’designer’ solvents exhibiting a host of tunable physicochemical properties. Here, a detailed review of the current literature reveals the lack of predictive understanding of the microscopic mechanisms that govern the structure-property relationships in this class of solvents. Complex hydrogen bonding behavior is postulated as the root cause of their melt-ing point depressions and physicochemical properties; to understand these hydrogen bonded networks, it is imperative to study these systems as dynamic entities using both simulations and experiments. This review emphasizes recent research efforts in order to elucidate the next steps needed to develop a fundamental framework for understanding DESs. It covers recent developments in DES research, frames outstanding scientific questions, and identifies gainful research thrusts that would advance the field towards predictive models and fundamental understanding of these solvents.

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Research Organization:: Case Western Reserve Univ., Cleveland, OH (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: SC0019409

OSTI ID:: 1808446

Journal Information:: Chemical Reviews, Vol. 121, Issue 3; ISSN 0009-2665

Publisher:: American Chemical SocietyCopyright Statement

Country of Publication:: United States

Language:: English

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The physicochemical and thermodynamic properties of the choline chloride-based deep eutectic solvents Troter, Dragan; Todorovic, Zoran; Djokic-Stojanovic, Dusica Journal of the Serbian Chemical Society, Vol. 82, Issue 9 https://doi.org/10.2298/JSC170225065T	journal	January 2017
Solubilities of carbon dioxide in the eutectic mixture of levulinic acid (or furfuryl alcohol) and choline chloride Lu, Meizhen; Han, Guoqiang; Jiang, Yaotai The Journal of Chemical Thermodynamics, Vol. 88 https://doi.org/10.1016/j.jct.2015.04.021	journal	September 2015
Organic Eutectic Electrolytes for Future Flow Batteries Cong, Guangtao; Lu, Yi-Chun Chem, Vol. 4, Issue 12 https://doi.org/10.1016/j.chempr.2018.11.018	journal	December 2018
Zn-based eutectic mixture as anolyte for hybrid redox flow batteries Wang, Yiyu; Niu, Zhihui; Zheng, Qi Scientific Reports, Vol. 8, Issue 1 https://doi.org/10.1038/s41598-018-24059-x	journal	April 2018
Tailoring and recycling of deep eutectic solvents as sustainable and efficient extraction media Jeong, Kyung Min; Lee, Min Sang; Nam, Min Woo Journal of Chromatography A, Vol. 1424 https://doi.org/10.1016/j.chroma.2015.10.083	journal	December 2015
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Natural deep eutectic solvent mediated pretreatment of rice straw: bioanalytical characterization of lignin extract and enzymatic hydrolysis of pretreated biomass residue Kumar, Adepu K.; Parikh, Bhumika S.; Pravakar, Mohanty Environmental Science and Pollution Research, Vol. 23, Issue 10 https://doi.org/10.1007/s11356-015-4780-4	journal	June 2015
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From Molecular Fragments to the Bulk: Development of a Neural Network Potential for MOF-5 Eckhoff, Marco; Behler, Jörg Journal of Chemical Theory and Computation, Vol. 15, Issue 6 https://doi.org/10.1021/acs.jctc.8b01288	journal	April 2019
Dielectric relaxation in acetamide + urea deep eutectics and neat molten urea: Origin of time scales via temperature dependent measurements and computer simulations Mukherjee, Kallol; Das, Suman; Tarif, Ejaj The Journal of Chemical Physics, Vol. 149, Issue 12 https://doi.org/10.1063/1.5040071	journal	September 2018
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DNA and RNA in Anhydrous Media: Duplex, Triplex, and G-Quadruplex Secondary Structures in a Deep Eutectic Solvent Mamajanov, Irena; Engelhart, Aaron E.; Bean, Heather D. Angewandte Chemie International Edition, Vol. 49, Issue 36 https://doi.org/10.1002/anie.201001561	journal	July 2010
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Quantum Chemical Evaluation of Deep Eutectic Solvents for the Extractive Desulfurization of Fuel Wagle, Durgesh V.; Zhao, Hua; Deakyne, Carol A. ACS Sustainable Chemistry & Engineering, Vol. 6, Issue 6 https://doi.org/10.1021/acssuschemeng.8b00224	journal	March 2018
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Effective Release of Intracellular Enzymes by Permeating the Cell Membrane with Hydrophobic Deep Eutectic Solvents Cao, Jun; Wu, Rong; Dong, Qihui ChemBioChem, Vol. 21, Issue 5 https://doi.org/10.1002/cbic.201900502	journal	November 2019
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Electrodeposition of Cu–In alloys from a choline chloride based deep eutectic solvent for photovoltaic applications Malaquias, João C.; Steichen, Marc; Thomassey, Matthieu Electrochimica Acta, Vol. 103 https://doi.org/10.1016/j.electacta.2013.04.068	journal	July 2013
Design, synthesis and properties of acidic deep eutectic solvents based on choline chloride Cui, Yingna; Li, Changping; Yin, Jingmei Journal of Molecular Liquids, Vol. 236 https://doi.org/10.1016/j.molliq.2017.04.052	journal	June 2017
Ionic liquids in biotransformations: from proof-of-concept to emerging deep-eutectic-solvents Domínguez de María, Pablo; Maugeri, Zaira Current Opinion in Chemical Biology, Vol. 15, Issue 2 https://doi.org/10.1016/j.cbpa.2010.11.008	journal	April 2011
Insights into the impact of deep eutectic solvents on horseradish peroxidase: Activity, stability and structure Wu, Ben-Pei; Wen, Qing; Xu, Hong Journal of Molecular Catalysis B: Enzymatic, Vol. 101 https://doi.org/10.1016/j.molcatb.2014.01.001	journal	March 2014
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Carbon Dioxide Solubilities in Decanoic Acid-Based Hydrophobic Deep Eutectic Solvents Zubeir, Lawien F.; van Osch, Dannie J. G. P.; Rocha, Marisa A. A. Journal of Chemical & Engineering Data, Vol. 63, Issue 4 https://doi.org/10.1021/acs.jced.7b00534	journal	March 2018
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Efficient and Selective Extraction of ^99m TcO ₄ ^– from Aqueous Media Using Hydrophobic Deep Eutectic Solvents Phelps, Tim E.; Bhawawet, Nakara; Jurisson, Silvia S. ACS Sustainable Chemistry & Engineering, Vol. 6, Issue 11 https://doi.org/10.1021/acssuschemeng.8b03950	journal	October 2018
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Fruit sugar-based deep eutectic solvents and their physical properties Hayyan, Adeeb; Mjalli, Farouq S.; AlNashef, Inas M. Thermochimica Acta, Vol. 541 https://doi.org/10.1016/j.tca.2012.04.030	journal	August 2012

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