Mapping of Texture and Phase Fractions in Heterogeneous Stress States during Multiaxial Loading of Biomedical Superelastic NiTi

Nicholson, Douglas E.; Padula, Santo A.; Benafan, Othmane; Bunn, Jeffrey R.; Payzant, Andrew; An, Ke; Penumadu, Dayakar; Vaidyanathan, Raj

doi:10.1002/adma.202005092

Title: Mapping of Texture and Phase Fractions in Heterogeneous Stress States during Multiaxial Loading of Biomedical Superelastic NiTi

Journal Article · Sun Dec 20 00:00:00 EST 2020 · Advanced Materials

DOI:https://doi.org/10.1002/adma.202005092· OSTI ID:1769254

Nicholson, Douglas E. ^[1]; Padula, Santo A. ^[2]; Benafan, Othmane ^[2];

^[3];

^[3]; Penumadu, Dayakar ^[4]; Vaidyanathan, Raj ^[1]

Univ. of Central Florida, Orlando, FL (United States)
NASA Glenn Research Center, Cleveland, OH (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Univ. of Tennessee, Knoxville, TN (United States)

Thermoelastic deformation mechanisms in polycrystalline biomedical-grade superelastic NiTi are spatially mapped using in situ neutron diffraction during multiaxial loading and heating. The trigonal R-phase is formed from the cubic phase during cooling to room temperature and subsequently deforms in compression, tension, and torsion. The resulting R-phase variant microstructure from the variant reorientation and detwinning processes are equivalent for the corresponding strain in tension and compression, and the variant microstructure is reversible by isothermal loading. The R-phase variant microstructure is consistent between uniaxial and torsional loading when the principal stress directions of the stress state are considered (for the crystallographic directions observed here). The variant microstructure evolution is tracked and the similarity in general behavior between uniaxial and torsional loading, in spite of the implicit heterogeneous stress state associated with torsional loading, pointed to the ability of the reversible thermoelastic transformation in NiTi to accommodate stress and strain mismatch with deformation. This ability of the R-phase, despite its limited variants, to accommodate stress and strain and satisfy strain incompatibility in addition to the existing internal stresses has significance for reducing irrecoverable deformation mechanisms during loading and cycling through the phase transformation.

View Accepted Manuscript (DOE)

Cite

Export

Save

Research Organization:: Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1769254

Journal Information:: Advanced Materials, Vol. 33, Issue 5; ISSN 0935-9648

Publisher:: WileyCopyright Statement

Country of Publication:: United States

Language:: English

References (28)

Temperature dependent deformation of the B2 austenite phase of a NiTi shape memory alloy Benafan, O.; Noebe, R. D.; Padula, S. A. International Journal of Plasticity, Vol. 51 https://doi.org/10.1016/j.ijplas.2013.06.003	journal	December 2013
Analysis of neutron diffraction spectra acquired in situ during stress-induced transformations in superelastic NiTi Vaidyanathan, R.; Bourke, M. A. M.; Dunand, D. C. Journal of Applied Physics, Vol. 86, Issue 6 https://doi.org/10.1063/1.371163	journal	September 1999
Measurement of the lattice plane strain and phase fraction evolution during heating and cooling in shape memory NiTi Qiu, S.; Krishnan, V. B.; Padula, S. A. Applied Physics Letters, Vol. 95, Issue 14 https://doi.org/10.1063/1.3245308	journal	October 2009
A Thermal Conduction Switch Based on low Hysteresis Nitife Shape Memory Alloy Helical Springs Krishnan, V. B.; Bewerse, C.; Notardonato, W. U. ADVANCES IN CRYOGENIC ENGINEERING MATERIALS: Transactions of the International Cryogenic Materials Conference - ICMC, Vol. 54, AIP Conference Proceedings https://doi.org/10.1063/1.2900374	conference	January 2008
Thermomechanical cycling of a NiTi shape memory alloy-macroscopic response and microstructural evolution Benafan, O.; Noebe, R. D.; Padula, S. A. International Journal of Plasticity, Vol. 56 https://doi.org/10.1016/j.ijplas.2014.01.006	journal	May 2014
Low temperature deformation of the R-phase in a NiTiFe shape memory alloy Krishnan, V. B.; Shmalo, S. B.; Rathod, C. R. Applied Physics Letters, Vol. 97, Issue 9 https://doi.org/10.1063/1.3481694	journal	August 2010
Rietveld refinement with spallation neutron powder diffraction data Von Dreele, R. B.; Jorgensen, J. D.; Windsor, C. G. Journal of Applied Crystallography, Vol. 15, Issue 6 https://doi.org/10.1107/S0021889882012722	journal	December 1982
Understanding the Deformation and Fracture of Nitinol Endovascular Stents Using In Situ Synchrotron X-Ray Microdiffraction Mehta, A.; Gong, X. -Y.; Imbeni, V. Advanced Materials, Vol. 19, Issue 9 https://doi.org/10.1002/adma.200601916	journal	May 2007
On elastic moduli and elastic anisotropy in polycrystalline martensitic NiTi Qiu, S.; Clausen, B.; Padula, S. A. Acta Materialia, Vol. 59, Issue 13 https://doi.org/10.1016/j.actamat.2011.04.018	journal	August 2011
Loading Path and Control Mode Effects During Thermomechanical Cycling of Polycrystalline Shape Memory NiTi Nicholson, D. E.; Benafan, O.; Padula, S. A. Shape Memory and Superelasticity, Vol. 4, Issue 1 https://doi.org/10.1007/s40830-017-0136-x	journal	January 2018
Texture evolution during nitinol martensite detwinning and phase transformation Cai, S.; Schaffer, J. E.; Ren, Y. Applied Physics Letters, Vol. 103, Issue 24 https://doi.org/10.1063/1.4846495	journal	December 2013
Phase fraction, texture and strain evolution in superelastic NiTi and NiTi–TiC composites investigated by neutron diffraction Vaidyanathan, R.; Bourke, M. A. M.; Dunand, D. C. Acta Materialia, Vol. 47, Issue 12 https://doi.org/10.1016/S1359-6454(99)00214-1	journal	September 1999
Deformation and transition behavior associated with theR-phase in Ti-Ni alloys Miyazaki, S.; Otsuka, K. Metallurgical Transactions A, Vol. 17, Issue 1 https://doi.org/10.1007/BF02644442	journal	January 1986
The R-phase transition and associated shape memory mechanism in Ti-Ni single crystals Miyazaki, S.; Wayman, C. M. Acta Metallurgica, Vol. 36, Issue 1 https://doi.org/10.1016/0001-6160(88)90037-5	journal	January 1988
R-phase transformation phenomena in thermomechanically loaded NiTi polycrystals Šittner, P.; Landa, M.; Lukáš, P. Mechanics of Materials, Vol. 38, Issue 5-6 https://doi.org/10.1016/j.mechmat.2005.05.025	journal	May 2006
Physical metallurgy of Ti–Ni-based shape memory alloys Otsuka, K.; Ren, X. Progress in Materials Science, Vol. 50, Issue 5 https://doi.org/10.1016/j.pmatsci.2004.10.001	journal	July 2005
Texture, strain, and phase-fraction measurements during mechanical cycling in superelastic NiTi Vaidyanathan, R.; Bourke, M. A. M.; Dunand, D. C. Metallurgical and Materials Transactions A, Vol. 32, Issue 13 https://doi.org/10.1007/s11661-001-1012-y	journal	March 2001
In-situ synchrotron high energy X-ray diffraction study of micro-mechanical behaviour of R phase reorientation in nanocrystalline NiTi alloy Feng, Bo; Kong, Xiangguang; Hao, Shijie Acta Materialia, Vol. 194 https://doi.org/10.1016/j.actamat.2020.05.004	journal	August 2020
The Role of Parent Phase Compliance on the Fatigue Lifetime of Ni–Ti Bonsignore, Craig; Shamini, Ali; Duerig, Tom Shape Memory and Superelasticity, Vol. 5, Issue 4 https://doi.org/10.1007/s40830-019-00253-2	journal	November 2019
Design and development of a shape memory alloy activated heat pipe-based thermal switch Benafan, O.; Notardonato, W. U.; Meneghelli, B. J. Smart Materials and Structures, Vol. 22, Issue 10 https://doi.org/10.1088/0964-1726/22/10/105017	journal	September 2013
Texture memory and strain-texture mapping in a NiTi shape memory alloy Ye, B.; Majumdar, B. S.; Dutta, I. Applied Physics Letters, Vol. 91, Issue 6 https://doi.org/10.1063/1.2768899	journal	August 2007
3D Mapping of Crystallographic Phase Distribution using Energy-Selective Neutron Tomography Woracek, Robin; Penumadu, Dayakar; Kardjilov, Nikolay Advanced Materials, Vol. 26, Issue 24 https://doi.org/10.1002/adma.201400192	journal	April 2014
Temperature-dependent behavior of a polycrystalline NiTi shape memory alloy around the transformation regime Benafan, O.; Noebe, R. D.; Padula, S. A. Scripta Materialia, Vol. 68, Issue 8 https://doi.org/10.1016/j.scriptamat.2012.11.042	journal	April 2013
Design and implementation of a multiaxial loading capability during heating on an engineering neutron diffractometer Benafan, O.; Padula, S. A.; Skorpenske, H. D. Review of Scientific Instruments, Vol. 85, Issue 10 https://doi.org/10.1063/1.4896042	journal	October 2014
Method to determine hkl strains and shear moduli under torsion using neutron diffraction Woracek, R.; Bunn, J. R.; Penumadu, D. Applied Physics Letters, Vol. 100, Issue 19 https://doi.org/10.1063/1.4712043	journal	May 2012
Role of B19′ martensite deformation in stabilizing two-way shape memory behavior in NiTi Benafan, O.; Padula, S. A.; Noebe, R. D. Journal of Applied Physics, Vol. 112, Issue 9 https://doi.org/10.1063/1.4764313	journal	November 2012
Current capabilities of the residual stress diffractometer at the high flux isotope reactor Cornwell, P.; Bunn, J.; Fancher, C. M. Review of Scientific Instruments, Vol. 89, Issue 9 https://doi.org/10.1063/1.5037593	journal	September 2018
Texture evolution during isothermal, isostrain, and isobaric loading of polycrystalline shape memory NiTi Nicholson, D. E.; Padula, S. A.; Benafan, O. Applied Physics Letters, Vol. 110, Issue 25 https://doi.org/10.1063/1.4989523	journal	June 2017

Similar Records

Uniaxial, Pure Bending, and Column Buckling Experiments on Superelastic NiTi Rods and Tubes

Journal Article · Fri Mar 23 00:00:00 EDT 2018 · International Journal of Solids and Structures · OSTI ID:1769254

Watkins, Ryan T.; Reedlunn, Benjamin; Daly, Samantha; +1 more

Phase fraction, texture and strain evolution in superelastic NiTi and NiTi-TiC composites investigated by neutron diffraction

Journal Article · Wed Sep 29 00:00:00 EDT 1999 · Acta Materialia · OSTI ID:1769254

Vaidyanathan, R; Bourke, M A.M.; Dunand, D C

In situ, 3D characterization of the deformation mechanics of a superelastic NiTi shape memory alloy single crystal under multiscale constraint

Journal Article · Mon Nov 20 00:00:00 EST 2017 · Acta Materialia · OSTI ID:1769254

Paranjape, Harshad M.; Paul, Partha P.; Amin-Ahmadi, Behnam; +6 more

Related Subjects

36 MATERIALS SCIENCE
NiTi
shape memory alloy
R-phase
torsion
multi-axial

Title: Mapping of Texture and Phase Fractions in Heterogeneous Stress States during Multiaxial Loading of Biomedical Superelastic NiTi

Citation Formats

References (28)

Similar Records

Related Subjects