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Title: Performance demonstration program plan for analysis of simulated headspace gases

Technical Report ·
DOI:https://doi.org/10.2172/171269· OSTI ID:171269

The Performance Demonstration Program (PDP) for analysis of headspace gases will consist of regular distribution and analyses of test standards to evaluate the capability for analyzing VOCs, hydrogen, and methane in the headspace of transuranic (TRU) waste throughout the Department of Energy (DOE) complex. Each distribution is termed a PDP cycle. These evaluation cycles will provide an objective measure of the reliability of measurements performed for TRU waste characterization. Laboratory performance will be demonstrated by the successful analysis of blind audit samples of simulated TRU waste drum headspace gases according to the criteria set within the text of this Program Plan. Blind audit samples (hereinafter referred to as PDP samples) will be used as an independent means to assess laboratory performance regarding compliance with the QAPP QAOs. The concentration of analytes in the PDP samples will encompass the range of concentrations anticipated in actual waste characterization gas samples. Analyses which are required by the WIPP to demonstrate compliance with various regulatory requirements and which are included in the PDP must be performed by laboratories which have demonstrated acceptable performance in the PDP.

Research Organization:
USDOE Carlsbad Area Office, NM (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
OSTI ID:
171269
Report Number(s):
DOE/CAO-95-1076; ON: DE96003981; NC: NONE; TRN: 96:003730
Resource Relation:
Other Information: PBD: Jun 1995
Country of Publication:
United States
Language:
English