Atom Probe Tomography for Catalysis Applications: A Review

Barroo, Cédric; Akey, Austin J.; Bell, David C.

doi:10.3390/app9132721

Title: Atom Probe Tomography for Catalysis Applications: A Review

Journal Article · Fri Jul 05 00:00:00 EDT 2019 · Applied Sciences

DOI:https://doi.org/10.3390/app9132721· OSTI ID:1595104

^[1]; Akey, Austin J. ^[2]; Bell, David C. ^[2]

Université Libre de Bruxelles, Brussels (Belgium); Harvard Univ., Cambridge, MA (United States)
Harvard Univ., Cambridge, MA (United States)

Atom probe tomography is a well-established analytical instrument for imaging the 3D structure and composition of materials with high mass resolution, sub-nanometer spatial resolution and ppm elemental sensitivity. Thanks to recent hardware developments in Atom Probe Tomography (APT), combined with progress on site-specific focused ion beam (FIB)-based sample preparation methods and improved data treatment software, complex materials can now be routinely investigated. From model samples to complex, usable porous structures, there is currently a growing interest in the analysis of catalytic materials. APT is able to probe the end state of atomic-scale processes, providing information needed to improve the synthesis of catalysts and to unravel structure/composition/reactivity relationships. This review focuses on the study of catalytic materials with increasing complexity (tip-sample, unsupported and supported nanoparticles, powders, self-supported catalysts and zeolites), as well as sample preparation methods developed to obtain suitable specimens for APT experiments.

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Research Organization:: Energy Frontier Research Centers (EFRC) (United States). Integrated Mesoscale Architectures for Sustainable Catalysis (IMASC); Harvard Univ., Cambridge, MA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); National Science Foundation (NSF)

Grant/Contract Number:: SC0012573; 1541959

OSTI ID:: 1595104

Journal Information:: Applied Sciences, Vol. 9, Issue 13; ISSN 2076-3417

Publisher:: MDPICopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 10 works

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Parikh, Pritesh A.; Chung, Hyeseung; Vo, Ethan A.; +3 more

Atom Probe Tomography for understanding microstructural and chemical changes in nuclear materials

Conference · Thu Dec 19 00:00:00 EST 2019 · OSTI ID:1595104

Bachhav, Mukesh

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36 MATERIALS SCIENCE
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
atom probe tomography
APT
FIB sample preparation
alloy engineering
core-shell structure
nanoporous catalyst
zeolite
correlative techniques

Title: Atom Probe Tomography for Catalysis Applications: A Review

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