In situ characterization of nanoparticles using Rayleigh scattering

Santra, Biswajit; Shneider, Mikhail N.; Car, Roberto

doi:10.1038/srep40230

Title: In situ characterization of nanoparticles using Rayleigh scattering

Journal Article · Tue Jan 10 00:00:00 EST 2017 · Scientific Reports

DOI:https://doi.org/10.1038/srep40230· OSTI ID:1347998

Santra, Biswajit ^[1]; Shneider, Mikhail N. ^[1]; Car, Roberto ^[1]

Princeton Univ., Princeton, NJ (United States)

Here, we report a theoretical analysis showing that Rayleigh scattering could be used to monitor the growth of nanoparticles under arc discharge conditions. We compute the Rayleigh scattering cross sections of the nanoparticles by combining light scattering theory for gas-particle mixtures with calculations of the dynamic electronic polarizability of the nanoparticles. We find that the resolution of the Rayleigh scattering probe is adequate to detect nanoparticles as small as C₆₀ at the expected concentrations of synthesis conditions in the arc periphery. Larger asymmetric nanoparticles would yield brighter signals, making possible to follow the evolution of the growing nanoparticle population from the evolution of the scattered intensity. Observable spectral features include characteristic resonant behaviour, shape-dependent depolarization ratio, and mass-dependent line shape. Direct observation of nanoparticles in the early stages of growth with unobtrusive laser probes should give insight on the particle formation mechanisms and may lead to better-controlled synthesis protocols.

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Research Organization:: Princeton Plasma Physics Laboratory (PPPL), Princeton, NJ (United States)

Sponsoring Organization:: USDOE

OSTI ID:: 1347998

Journal Information:: Scientific Reports, Vol. 7; ISSN 2045-2322

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 18 works

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