Phase coexistence and domain configuration in Pb(Mg1/3Nb2/3)O3-0.34PbTiO3 single crystal revealed by synchrotron-based X-ray diffractive three-dimensional reciprocal space mapping and piezoresponse force microscopy

Wang, Ruixue; Xu, Han; Yang, Bin; Luo, Zhenlin; Sun, Enwei; Zhao, Jiangtao; Zheng, Limei; Dong, Yongqi; Zhou, Hua; Ren, Yang; Gao, Chen; Cao, Wenwu

doi:10.1063/1.4946776

Title: Phase coexistence and domain configuration in Pb(Mg_1/3Nb_2/3)O₃-0.34PbTiO₃ single crystal revealed by synchrotron-based X-ray diffractive three-dimensional reciprocal space mapping and piezoresponse force microscopy

Journal Article · Fri Apr 15 00:00:00 EDT 2016 · Applied Physics Letters

DOI:https://doi.org/10.1063/1.4946776· OSTI ID:1256890

Wang, Ruixue ^[1]; Xu, Han ^[2]; Yang, Bin ^[1]; Luo, Zhenlin ^[2]; Sun, Enwei ^[1]; Zhao, Jiangtao ^[2];

^[1]; Dong, Yongqi ^[2]; Zhou, Hua ^[3]; Ren, Yang ^[3]; Gao, Chen ^[2];

^[4]

Harbin Inst. of Technology, Harbin (China)
Univ. of Science and Technology of China, Anhui (China)
Argonne National Lab. (ANL), Argonne, IL (United States)
Harbin Inst. of Technology, Harbin (China); Pennsylvania State Univ., University Park, PA (United States)

The crystalline phases and domain configuration in the morphotropic phase boundary composition Pb(Mg_1/3Nb_2/3)O₃-0.34PbTiO₃ (PMN-0.34PT) single crystal have been investigated by synchrotronbased X-ray 3D Reciprocal Space Mapping (3D-RSM) and Piezoresponse Force Microscopy. The coexistence of tetragonal (T) and monoclinic MC phases in this PMN-0.34PT single crystal is confirmed. The affiliation of each diffraction spot in the 3D-RSM was identified with the assistance of qualitative simulation. Most importantly, the twinning structure between different domains in such a mixed phase PMN-PT crystal is firmly clarified, and the spatial distribution of different twin domains is demonstrated. Additionally, the lattice parameters of T and MC phases in PMN-0.34PT single crystal as well as the tilting angles of crystal lattices caused by the interfacial lattice mismatch are determined.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); National Natural Science Foundation of China (NSFC)

Grant/Contract Number:: AC02-06CH11357; 2013CB632900; 11374010; 11434009

OSTI ID:: 1256890

Alternate ID(s):: OSTI ID: 1420601

Journal Information:: Applied Physics Letters, Vol. 108, Issue 15; ISSN 0003-6951

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 27 works

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Title: Phase coexistence and domain configuration in Pb(Mg1/3Nb2/3)O3-0.34PbTiO3 single crystal revealed by synchrotron-based X-ray diffractive three-dimensional reciprocal space mapping and piezoresponse force microscopy

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Title: Phase coexistence and domain configuration in Pb(Mg_1/3Nb_2/3)O₃-0.34PbTiO₃ single crystal revealed by synchrotron-based X-ray diffractive three-dimensional reciprocal space mapping and piezoresponse force microscopy