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Title: Waste tank vapor project: Vapor space characterization of waste tank 241-BY-104: Results from samples collected on June 24, 1994

Technical Report ·
DOI:https://doi.org/10.2172/10196544· OSTI ID:10196544

This report describes results of the analyses of tank-headspace samples taken from Hanford waste Tank 241-BY-104 (referred to as Tank BY-104) on June 24, 1994. The Pacific Northwest Laboratory (PNL) contracted with Westinghouse Hanford Company (WHC) to provide sampling devices and analyze inorganic and organic samples collected from the tank headspace. The sample job was designated S4019 and was performed by WHC on June 24, 1994 using the vapor sampling system (VSS). The results of the analyses are expected to be used in the determination of safety and toxicological issues related to the tank-headspace gas as described in the WHC report entitled Data Quality Objectives for Generic In-Tank Health and Safety Vapor Issue Resolution, WHC-SD-WM-DQO-002, Rev. 0. Sampling devices, including 16 sorbent trains (for inorganic analyses), and 5 SUMMA{trademark} canisters (for organic analyses), were supplied to the WHC sampling staff on June 20, 1994. Samples were taken (by WHC) on June 24. The samples were returned from the field on June 27. The inorganic samples delivered to PNL on chain-of-custody (COC) 006893 included 16 sorbent trains as described in Tables 2.2, 2.3, and 2.4. Additional inorganic blank spikes were obtained from related sample jobs. SUMMA{trademark} samples delivered to PNL on COC 006896 included one ambient air sample, one ambient-air sample through the sampling system, and three tank-headspace SUMMA{trademark} canister samples. The samples were inspected upon delivery to the 326/23B laboratory and logged into PNL laboratory record book 55408. Custody of the sorbent trains was transferred to PNL personnel performing the inorganic analysis and stored at refrigerated ({le}10{degrees}C) temperature until the time of analysis. Access to the 326/23B laboratory is limited to PNL personnel working on the waste-tank safety program.

Research Organization:
Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC06-76RL01830
OSTI ID:
10196544
Report Number(s):
PNL-10208; ON: DE95003803; TRN: 94:010746
Resource Relation:
Other Information: PBD: Nov 1994
Country of Publication:
United States
Language:
English