Hydrogen embrittlement of additively manufactured austenitic stainless steel 316 L

Bertsch, K. M.; Nagao, A.; Rankouhi, B.; Kuehl, B.; Thoma, D. J.

doi:10.1016/j.corsci.2021.109790

Title: Hydrogen embrittlement of additively manufactured austenitic stainless steel 316 L

Abstract

Additive manufacturing (AM) is a promising means of production of austenitic stainless steel (SS) parts for hydrogen service. The hydrogen embrittlement resistance of SS 316 L parts manufactured by powder-bed-fed selective laser melting (SLM) and directed energy deposition (DED) was examined using slow strain rate tensile testing. The influence of the hierarchical AM microstructures on mechanical response, microstructural evolution, and void formation were analyzed using multiscale electron microscopy. The presence of hydrogen reduced ductility in as-built DED materials, but did not significantly influence the response in as-built SLM material or heat-treated materials. Microstructural features driving these different responses are discussed.

Authors:

Bertsch, K. M. ^[1]; Nagao, A. ^[2]; Rankouhi, B. ^[3]; Kuehl, B. ^[3]; Thoma, D. J. ^[3]

Univ. of Wisconsin, Madison, WI (United States); Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
Kyushu Univ., Fukuoka (Japan)
Univ. of Wisconsin, Madison, WI (United States)

Publication Date:: Wed Sep 01 00:00:00 EDT 2021

Research Org.:: Georgia Institute of Technology, Atlanta, GA (United States); Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Org.:: USDOE National Nuclear Security Administration (NNSA)

OSTI Identifier:: 1828176

Alternate Identifier(s):: OSTI ID: 1833209; OSTI ID: 1842687

Report Number(s):: LLNL-JRNL-821384
Journal ID: ISSN 0010-938X; TRN: US2216000

Grant/Contract Number:: NA0003921; AC52-07NA27344

Resource Type:: Accepted Manuscript

Journal Name:: Corrosion Science

Additional Journal Information:: Journal Volume: 192; Journal ID: ISSN 0010-938X

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; Additive manufacturing; Hydrogen embrittlement; Dislocations; Stainless steel; Transmission electron microscopy

Citation Formats


                    Bertsch, K. M., Nagao, A., Rankouhi, B., Kuehl, B., and Thoma, D. J. Hydrogen embrittlement of additively manufactured austenitic stainless steel 316 L.  United States: N. p., 2021. 
Web.  doi:10.1016/j.corsci.2021.109790.

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                    Bertsch, K. M., Nagao, A., Rankouhi, B., Kuehl, B., & Thoma, D. J. Hydrogen embrittlement of additively manufactured austenitic stainless steel 316 L.  United States.  https://doi.org/10.1016/j.corsci.2021.109790

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                    Bertsch, K. M., Nagao, A., Rankouhi, B., Kuehl, B., and Thoma, D. J. Wed .  
"Hydrogen embrittlement of additively manufactured austenitic stainless steel 316 L".  United States.  https://doi.org/10.1016/j.corsci.2021.109790.  https://www.osti.gov/servlets/purl/1828176.

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@article{osti_1828176,

  title        = {Hydrogen embrittlement of additively manufactured austenitic stainless steel 316 L},

  author       = {Bertsch, K. M. and Nagao, A. and Rankouhi, B. and Kuehl, B. and Thoma, D. J.},

  abstractNote = {Additive manufacturing (AM) is a promising means of production of austenitic stainless steel (SS) parts for hydrogen service. The hydrogen embrittlement resistance of SS 316 L parts manufactured by powder-bed-fed selective laser melting (SLM) and directed energy deposition (DED) was examined using slow strain rate tensile testing. The influence of the hierarchical AM microstructures on mechanical response, microstructural evolution, and void formation were analyzed using multiscale electron microscopy. The presence of hydrogen reduced ductility in as-built DED materials, but did not significantly influence the response in as-built SLM material or heat-treated materials. Microstructural features driving these different responses are discussed.},

  doi          = {10.1016/j.corsci.2021.109790},

  journal      = {Corrosion Science},

  number       = ,

  volume       = 192,

  place        = {United States},

  year         = {Wed Sep 01 00:00:00 EDT 2021},

  month        = {Wed Sep 01 00:00:00 EDT 2021}

}

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Brass, A. -M.; Chêne, J.
Corrosion Science, Vol. 48, Issue 10
DOI: 10.1016/j.corsci.2005.11.004

Hydrogen-induced intergranular failure of iron
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Wang, Shuai; Martin, May L.; Sofronis, Petros
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On the failure of surface damage to assess the hydrogen-enhanced deformation ahead of crack tip in a cyclically loaded austenitic stainless steel
journal, June 2019

Wang, Shuai; Nygren, Kelly E.; Nagao, Akihide
Scripta Materialia, Vol. 166
DOI: 10.1016/j.scriptamat.2019.03.010

Evidence for Dislocation Transport of Hydrogen in Aluminum
journal, May 1982

Albrecht, J.; Bernstein, I. M.; Thompson, Anthony W.
Metallurgical Transactions A, Vol. 13, Issue 5
DOI: 10.1007/BF02642394

On the influence of grain size on the TWIP/TRIP-effect and texture development in high-manganese steels
journal, April 2019

Sevsek, Simon; Brasche, Frederike; Molodov, Dmitri A.
Materials Science and Engineering: A, Vol. 754
DOI: 10.1016/j.msea.2019.03.072

The onset of twinning in metals: a constitutive description
journal, November 2001

Meyers, M. A.; Vöhringer, O.; Lubarda, V. A.
Acta Materialia, Vol. 49, Issue 19
DOI: 10.1016/S1359-6454(01)00300-7

Interrogating the Effects of Hydrogen on the Behavior of Planar Deformation Bands in Austenitic Stainless Steel
journal, February 2021

Sabisch, J. E. C.; Sugar, J. D.; Ronevich, J.
Metallurgical and Materials Transactions A, Vol. 52, Issue 4
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Hydrogen embrittlement of metals
journal, January 1972

Louthan, M. R.; Caskey, G. R.; Donovan, J. A.
Materials Science and Engineering, Vol. 10
DOI: 10.1016/0025-5416(72)90109-7

New insights on cellular structures strengthening mechanisms and thermal stability of an austenitic stainless steel fabricated by laser powder-bed-fusion
journal, January 2021

Voisin, Thomas; Forien, Jean-Baptiste; Perron, Aurelien
Acta Materialia, Vol. 203
DOI: 10.1016/j.actamat.2020.11.018

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Similar Records

Title: Hydrogen embrittlement of additively manufactured austenitic stainless steel 316 L

Abstract

Citation Formats

Dislocation Cell Formation in Metals journal, July 1970

Hydrogen-enhanced-plasticity mediated decohesion for hydrogen-induced intergranular and “quasi-cleavage” fracture of lath martensitic steels journal, March 2018

Signatures of the unique microstructure of additively manufactured steel observed via diffraction journal, October 2018

Enumeration of the hydrogen-enhanced localized plasticity mechanism for hydrogen embrittlement in structural materials journal, February 2019

Hydrogen Embrittlement Understood journal, March 2015

The predominant role of strain-induced vacancies in hydrogen embrittlement of steels: Overview journal, February 2019

Hydrogen embrittlement in compositionally complex FeNiCoCrMn FCC solid solution alloy journal, February 2018

Hydrogen-enhanced localization of plasticity in an austenitic stainless steel journal, November 1995

The effect of nanosized (Ti,Mo)C precipitates on hydrogen embrittlement of tempered lath martensitic steel journal, August 2014

Influence of low temperature prestrain on hydrogen gas embrittlement of metastable austenitic stainless steels journal, August 2013

Effect of pre-strain on hydrogen embrittlement of metastable austenitic stainless steel under different hydrogen conditions journal, October 2019

Additive manufacturing of metallic components – Process, structure and properties journal, March 2018

Effects of alloy composition and strain hardening on tensile fracture of hydrogen-precharged type 316 stainless steels journal, January 2008

Hydrogen Embrittlement Susceptibility of Fe-Mn Binary Alloys with High Mn Content: Effects of Stable and Metastable ε-Martensite, and Mn Concentration journal, March 2016

Overview of hydrogen embrittlement in high-Mn steels journal, April 2017

Dislocation network in additive manufactured steel breaks strength–ductility trade-off journal, May 2018

Predicting twinning stress in fcc metals: Linking twin-energy pathways to twin nucleation journal, December 2007

Slip systems extracted from lattice rotations and dislocation structures journal, May 2008

Hydrogen related failure of steels – a new aspect journal, August 2004

Hydrogen-assisted failure in Ni-based superalloy 718 studied under in situ hydrogen charging: The role of localized deformation in crack propagation journal, April 2017

Effect of weld composition and microstructure on hydrogen assisted fracture of austenitic stainless steels journal, January 1983

On the thermo-mechanical behavior and hydrogen compatibility of 22-13-5 stainles steel journal, June 1975

Stacking fault energies of seven commercial austenitic stainless steels journal, July 1975

Corrosion of Additively Manufactured Alloys: A Review journal, October 2018

Failure Analysis of SUS316L Flexible Hose for Hydrogen Station and Fatigue Life Prediction Method [水素ステーション水素漏洩トラブルの解析とSUS316Lフレキシブルホースの疲労寿命予測] journal, January 2009

Hydrogen environment embrittlement of stable austenitic steels journal, November 2012

Experimental validation and microstructure characterization of topology optimized, additively manufactured SS316L components journal, March 2020

Effects of hydrogen on tensile properties and fracture surface morphologies of Type 316L stainless steel journal, February 2014

HVEM studies of the effects of hydrogen on the deformation and fracture of AISI type 316 austenitic stainless steel journal, November 1990

Void initiation in ductile fracture journal, November 1973

The role of localized deformation in hydrogen-assisted crack propagation in 21Cr–6Ni–9Mn stainless steel journal, August 2009

Hydrogen induced grain boundary fracture in high purity nickel and its alloys—Enhanced hydrogen diffusion along grain boundaries journal, March 1988

Effect of dislocation cell walls on hydrogen adsorption, hydrogen trapping and hydrogen embrittlement resistance journal, April 2020

Ductile Fracture by Void Growth to Coalescence book, January 2010

Analysis of the strategies for bridging the gap towards the Hydrogen Economy journal, November 2016

Conformity between Mechanics and Microscopic Functions of Hydrogen in Failure journal, January 2012

Correlation between dislocation organization and slip bands: TEM and AFM investigations in hydrogen-containing nickel and nickel–chromium journal, June 2015

The effect of grain size and aging on hydrogen embrittlement of a maraging steel journal, September 2008

Neutron diffraction measurements of residual stress in additively manufactured stainless steel journal, December 2016

The dislocation cell size and dislocation density in copper deformed at temperatures between 25 and 700°C journal, April 1972

The Effect of Pre-Strain on the Resistance to Hydrogen Embrittlement in 316L Austenitic Stainless Steel journal, January 2014

Superior resistance to hydrogen damage for selective laser melted 316L stainless steel in a proton exchange membrane fuel cell environment journal, April 2020

On the formation and nature of quasi-cleavage fracture surfaces in hydrogen embrittled steels journal, February 2011

Origin of dislocation structures in an additively manufactured austenitic stainless steel 316L journal, October 2020

On the physical differences between tensile testing of type 304 and 316 austenitic stainless steels with internal hydrogen and in external hydrogen journal, September 2010

Hydrogen-assisted failure in a twinning-induced plasticity steel studied under in situ hydrogen charging by electron channeling contrast imaging journal, July 2013

The synergistic action and interplay of hydrogen embrittlement mechanisms in steels and iron: Localized plasticity and decohesion journal, July 2019

Hydrogen-assisted quasi-cleavage fracture in a single crystalline type 316 austenitic stainless steel journal, October 2013

Hydrogen-induced strain localization and failure of austenitic stainless steels at high hydrogen concentrations journal, June 1991

Microstructural properties controlling hydrogen environment embrittlement of cold worked 316 type austenitic stainless steels journal, March 2015

Effect of strain-induced martensite on hydrogen embrittlement of austenitic stainless steels investigated by combined tension and hydrogen release methods journal, June 2013

A critical review of powder-based additive manufacturing of ferrous alloys: Process parameters, microstructure and mechanical properties journal, April 2018

Corrosion of Additively Manufactured Stainless Steels—Process, Structure, Performance: A Review journal, February 2021

Alloying effects on the stacking fault energy in austenitic stainless steels from first-principles theory journal, August 2006

A dimensionless number for predicting universal processing parameter boundaries in metal powder bed additive manufacturing journal, January 2021

Subgrain-controlled grain growth in the laser-melted 316 L promoting strength at high temperatures journal, May 2018

Validation of void growth models using X-ray microtomography characterization of damage in dual phase steels journal, December 2011

Hydrogen thermal desorption relevant to delayed-fracture susceptibility of high-strength steels journal, February 2001

Hydrogen effects on dislocation activity in austenitic stainless steel journal, June 2006

Influence of solidification structures on radiation-induced swelling in an additively-manufactured austenitic stainless steel journal, September 2019

Hydrogen embrittlement of catholically hydrogen-precharged 304L austenitic stainless steel: Effect of plastic pre-strain journal, August 2014

Hydrogen-enhanced compatibility constraint for intergranular failure in FCC FeNiCoCrMn high-entropy alloy journal, May 2021

Hydrogen-enhanced localized plasticity—a mechanism for hydrogen-related fracture journal, March 1994

Grain detection from 2d and 3d EBSD data—Specification of the MTEX algorithm journal, December 2011

Strengthening mechanisms in directed energy deposited austenitic stainless steel journal, February 2019

Hydrogen-induced compatibility constraints across grain boundaries drive intergranular failure of Ni journal, July 2019

Influence of hydrogen on dislocation self-organization in Ni journal, August 2017

The effect of pre-straining and δ-ferrite on the embrittlement of 304L stainless steel by hydrogen journal, January 1993

Overview of the DOE hydrogen safety, codes and standards program, part 3: Advances in research and development to enhance the scientific basis for hydrogen regulations, codes and standards journal, March 2017

A TEM investigation of hydrogen-induced deformation twinning and associated martensitic phases in 304-type stainless steel journal, February 1977

Analysis of the tensile behavior of a TWIP steel based on the texture and microstructure evolutions journal, January 2009

A model of ductile fracture based on the nucleation and growth of voids journal, August 1981

Do voids nucleate at grain boundaries during ductile rupture? journal, September 2017

Additively manufactured hierarchical stainless steels with high strength and ductility journal, October 2017

The effect of plastic deformation on the transport of hydrogen in nickel journal, October 1979

Influence of macro segregation on hydrogen environment embrittlement of SUS 316L stainless steel journal, April 2009

The effect of hydrogen on dislocation dynamics journal, April 2001

Dislocation Cell Formation in Metals
journal, July 1970

Hydrogen-enhanced-plasticity mediated decohesion for hydrogen-induced intergranular and “quasi-cleavage” fracture of lath martensitic steels
journal, March 2018

Signatures of the unique microstructure of additively manufactured steel observed via diffraction
journal, October 2018

Enumeration of the hydrogen-enhanced localized plasticity mechanism for hydrogen embrittlement in structural materials
journal, February 2019

Hydrogen Embrittlement Understood
journal, March 2015

The predominant role of strain-induced vacancies in hydrogen embrittlement of steels: Overview
journal, February 2019

Hydrogen embrittlement in compositionally complex FeNiCoCrMn FCC solid solution alloy
journal, February 2018

Hydrogen-enhanced localization of plasticity in an austenitic stainless steel
journal, November 1995

The effect of nanosized (Ti,Mo)C precipitates on hydrogen embrittlement of tempered lath martensitic steel
journal, August 2014

Influence of low temperature prestrain on hydrogen gas embrittlement of metastable austenitic stainless steels
journal, August 2013

Effect of pre-strain on hydrogen embrittlement of metastable austenitic stainless steel under different hydrogen conditions
journal, October 2019

Additive manufacturing of metallic components – Process, structure and properties
journal, March 2018

Effects of alloy composition and strain hardening on tensile fracture of hydrogen-precharged type 316 stainless steels
journal, January 2008

Hydrogen Embrittlement Susceptibility of Fe-Mn Binary Alloys with High Mn Content: Effects of Stable and Metastable ε-Martensite, and Mn Concentration
journal, March 2016

Overview of hydrogen embrittlement in high-Mn steels
journal, April 2017

Dislocation network in additive manufactured steel breaks strength–ductility trade-off
journal, May 2018

Predicting twinning stress in fcc metals: Linking twin-energy pathways to twin nucleation
journal, December 2007

Slip systems extracted from lattice rotations and dislocation structures
journal, May 2008

Hydrogen related failure of steels – a new aspect
journal, August 2004

Hydrogen-assisted failure in Ni-based superalloy 718 studied under in situ hydrogen charging: The role of localized deformation in crack propagation
journal, April 2017

Effect of weld composition and microstructure on hydrogen assisted fracture of austenitic stainless steels
journal, January 1983

On the thermo-mechanical behavior and hydrogen compatibility of 22-13-5 stainles steel
journal, June 1975

Stacking fault energies of seven commercial austenitic stainless steels
journal, July 1975

Corrosion of Additively Manufactured Alloys: A Review
journal, October 2018

Failure Analysis of SUS316L Flexible Hose for Hydrogen Station and Fatigue Life Prediction Method [水素ステーション水素漏洩トラブルの解析とSUS316Lフレキシブルホースの疲労寿命予測]
journal, January 2009

Hydrogen environment embrittlement of stable austenitic steels
journal, November 2012

Experimental validation and microstructure characterization of topology optimized, additively manufactured SS316L components
journal, March 2020

Effects of hydrogen on tensile properties and fracture surface morphologies of Type 316L stainless steel
journal, February 2014

HVEM studies of the effects of hydrogen on the deformation and fracture of AISI type 316 austenitic stainless steel
journal, November 1990

Void initiation in ductile fracture
journal, November 1973

The role of localized deformation in hydrogen-assisted crack propagation in 21Cr–6Ni–9Mn stainless steel
journal, August 2009

Hydrogen induced grain boundary fracture in high purity nickel and its alloys—Enhanced hydrogen diffusion along grain boundaries
journal, March 1988

Effect of dislocation cell walls on hydrogen adsorption, hydrogen trapping and hydrogen embrittlement resistance
journal, April 2020

Ductile Fracture by Void Growth to Coalescence
book, January 2010

Analysis of the strategies for bridging the gap towards the Hydrogen Economy
journal, November 2016

Conformity between Mechanics and Microscopic Functions of Hydrogen in Failure
journal, January 2012

Correlation between dislocation organization and slip bands: TEM and AFM investigations in hydrogen-containing nickel and nickel–chromium
journal, June 2015

The effect of grain size and aging on hydrogen embrittlement of a maraging steel
journal, September 2008

Neutron diffraction measurements of residual stress in additively manufactured stainless steel
journal, December 2016

The dislocation cell size and dislocation density in copper deformed at temperatures between 25 and 700°C
journal, April 1972

The Effect of Pre-Strain on the Resistance to Hydrogen Embrittlement in 316L Austenitic Stainless Steel
journal, January 2014

Superior resistance to hydrogen damage for selective laser melted 316L stainless steel in a proton exchange membrane fuel cell environment
journal, April 2020

On the formation and nature of quasi-cleavage fracture surfaces in hydrogen embrittled steels
journal, February 2011

Origin of dislocation structures in an additively manufactured austenitic stainless steel 316L
journal, October 2020

On the physical differences between tensile testing of type 304 and 316 austenitic stainless steels with internal hydrogen and in external hydrogen
journal, September 2010

Hydrogen-assisted failure in a twinning-induced plasticity steel studied under in situ hydrogen charging by electron channeling contrast imaging
journal, July 2013

The synergistic action and interplay of hydrogen embrittlement mechanisms in steels and iron: Localized plasticity and decohesion
journal, July 2019

Hydrogen-assisted quasi-cleavage fracture in a single crystalline type 316 austenitic stainless steel
journal, October 2013

Hydrogen-induced strain localization and failure of austenitic stainless steels at high hydrogen concentrations
journal, June 1991

Microstructural properties controlling hydrogen environment embrittlement of cold worked 316 type austenitic stainless steels
journal, March 2015

Effect of strain-induced martensite on hydrogen embrittlement of austenitic stainless steels investigated by combined tension and hydrogen release methods
journal, June 2013

A critical review of powder-based additive manufacturing of ferrous alloys: Process parameters, microstructure and mechanical properties
journal, April 2018

Corrosion of Additively Manufactured Stainless Steels—Process, Structure, Performance: A Review
journal, February 2021

Alloying effects on the stacking fault energy in austenitic stainless steels from first-principles theory
journal, August 2006

A dimensionless number for predicting universal processing parameter boundaries in metal powder bed additive manufacturing
journal, January 2021

Subgrain-controlled grain growth in the laser-melted 316 L promoting strength at high temperatures
journal, May 2018

Validation of void growth models using X-ray microtomography characterization of damage in dual phase steels
journal, December 2011

Hydrogen thermal desorption relevant to delayed-fracture susceptibility of high-strength steels
journal, February 2001

Hydrogen effects on dislocation activity in austenitic stainless steel
journal, June 2006

Influence of solidification structures on radiation-induced swelling in an additively-manufactured austenitic stainless steel
journal, September 2019

Hydrogen embrittlement of catholically hydrogen-precharged 304L austenitic stainless steel: Effect of plastic pre-strain
journal, August 2014

Hydrogen-enhanced compatibility constraint for intergranular failure in FCC FeNiCoCrMn high-entropy alloy
journal, May 2021

Hydrogen-enhanced localized plasticity—a mechanism for hydrogen-related fracture
journal, March 1994

Grain detection from 2d and 3d EBSD data—Specification of the MTEX algorithm
journal, December 2011

Strengthening mechanisms in directed energy deposited austenitic stainless steel
journal, February 2019

Hydrogen-induced compatibility constraints across grain boundaries drive intergranular failure of Ni
journal, July 2019

Influence of hydrogen on dislocation self-organization in Ni
journal, August 2017

The effect of pre-straining and δ-ferrite on the embrittlement of 304L stainless steel by hydrogen
journal, January 1993

Overview of the DOE hydrogen safety, codes and standards program, part 3: Advances in research and development to enhance the scientific basis for hydrogen regulations, codes and standards
journal, March 2017

A TEM investigation of hydrogen-induced deformation twinning and associated martensitic phases in 304-type stainless steel
journal, February 1977

Analysis of the tensile behavior of a TWIP steel based on the texture and microstructure evolutions
journal, January 2009

A model of ductile fracture based on the nucleation and growth of voids
journal, August 1981

Do voids nucleate at grain boundaries during ductile rupture?
journal, September 2017

Additively manufactured hierarchical stainless steels with high strength and ductility
journal, October 2017

The effect of plastic deformation on the transport of hydrogen in nickel
journal, October 1979

Influence of macro segregation on hydrogen environment embrittlement of SUS 316L stainless steel
journal, April 2009

The effect of hydrogen on dislocation dynamics
journal, April 2001

Hydrogen effects on the character of dislocations in high-purity aluminum
journal, August 1999

Dislocation transport and hydrogen embrittlement
journal, November 1979

Hydrogen embrittlement of 3-D printing manufactured austenitic stainless steel part for hydrogen service
journal, March 2017