Synthesis, magnetization, and heat capacity of triangular lattice materials NaErSe2 and KErSe2

Xing, Jie; Sanjeewa, Liurukara D.; Kim, Jungsoo; Meier, William R.; May, Andrew F.; Zheng, Qiang; Custelcean, Radu; Stewart, G. R.; Sefat, Athena Safa

doi:10.1103/physrevmaterials.3.114413

Title: Synthesis, magnetization, and heat capacity of triangular lattice materials ${NaErSe}_{2}$ and ${KErSe}_{2}$

Abstract

In this paper we report the synthesis, magnetization, and heat capacity of the frustrated magnets $A {ErSe}_{2}$ ( $A = Na, K$ ) which contain perfect triangular lattices of ${Er}^{3 +}$ . The magnetization data suggests no long-range magnetic order exists in $A {ErSe}_{2}$ ( $A = Na, K$ ), which is consistent with the heat capacity measurements. Large anisotropy is observed between the magnetization within the $a b$ plane and along the $c$ axis of both compounds. When the magnetic field is applied along the $a b$ plane, anomalies are observed at 1.8 $μ_{B}$ in ${NaErSe}_{2}$ at 0.2 T and 2.1 $μ_{B}$ in ${KErSe}_{2}$ at 0.18 T. Unlike ${NaErSe}_{2}$ , a plateaulike field-induced metamagnetic transition is observed for $H ∥ c$ below 1 K in ${KErSe}_{2}$ . Two broad peaks are observed in the heat capacity below 10 K indicating possible crystal electric field (CEF) effects and magnetic entropy released under different magnetic fields. All results indicate that $A {ErSe}_{2}$ are strongly anisotropic, frustrated magnets with field-induced transition at low temperature. The lack of signatures for long-range magnetic order implies that these materials are candidates for hosting a quantum spin liquid ground state.

Authors:

^[1];

^[1]; Kim, Jungsoo ^[2];

^[1];

^[1]; Zheng, Qiang ^[3];

^[4]; Stewart, G. R. ^[2];

^[1]

Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Materials Science & Technology Division
Univ. of Florida, Gainesville, FL (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Materials Science & Technology Division; Univ. of Tennessee, Knoxville, TN (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Chemical Sciences Division

Publication Date:: Tue Nov 26 00:00:00 EST 2019

Research Org.:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Materials Sciences & Engineering Division; USDOE Office of Science (SC), Basic Energy Sciences (BES). Chemical Sciences, Geosciences & Biosciences Division

OSTI Identifier:: 1761718

Grant/Contract Number:: AC05-00OR22725; FG02-86ER45268

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review Materials

Additional Journal Information:: Journal Volume: 3; Journal Issue: 11; Journal ID: ISSN 2475-9953

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; frustrated magnetism

Citation Formats


                    Xing, Jie, Sanjeewa, Liurukara D., Kim, Jungsoo, Meier, William R., May, Andrew F., Zheng, Qiang, Custelcean, Radu, Stewart, G. R., and Sefat, Athena Safa. Synthesis, magnetization, and heat capacity of triangular lattice materials NaErSe2 and KErSe2.  United States: N. p., 2019. 
Web.  doi:10.1103/physrevmaterials.3.114413.

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                    Xing, Jie, Sanjeewa, Liurukara D., Kim, Jungsoo, Meier, William R., May, Andrew F., Zheng, Qiang, Custelcean, Radu, Stewart, G. R., & Sefat, Athena Safa. Synthesis, magnetization, and heat capacity of triangular lattice materials NaErSe2 and KErSe2.  United States.  https://doi.org/10.1103/physrevmaterials.3.114413

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                    Xing, Jie, Sanjeewa, Liurukara D., Kim, Jungsoo, Meier, William R., May, Andrew F., Zheng, Qiang, Custelcean, Radu, Stewart, G. R., and Sefat, Athena Safa. Tue .  
"Synthesis, magnetization, and heat capacity of triangular lattice materials NaErSe2 and KErSe2".  United States.  https://doi.org/10.1103/physrevmaterials.3.114413.  https://www.osti.gov/servlets/purl/1761718.

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@article{osti_1761718,

  title        = {Synthesis, magnetization, and heat capacity of triangular lattice materials NaErSe2 and KErSe2},

  author       = {Xing, Jie and Sanjeewa, Liurukara D. and Kim, Jungsoo and Meier, William R. and May, Andrew F. and Zheng, Qiang and Custelcean, Radu and Stewart, G. R. and Sefat, Athena Safa},

  abstractNote = {In this paper we report the synthesis, magnetization, and heat capacity of the frustrated magnets AErSe2(A=Na,K) which contain perfect triangular lattices of Er3+. The magnetization data suggests no long-range magnetic order exists in AErSe2(A=Na,K), which is consistent with the heat capacity measurements. Large anisotropy is observed between the magnetization within the ab plane and along the c axis of both compounds. When the magnetic field is applied along the ab plane, anomalies are observed at 1.8 μB in NaErSe2 at 0.2 T and 2.1 μB in KErSe2 at 0.18 T. Unlike NaErSe2, a plateaulike field-induced metamagnetic transition is observed for H∥c below 1 K in KErSe2. Two broad peaks are observed in the heat capacity below 10 K indicating possible crystal electric field (CEF) effects and magnetic entropy released under different magnetic fields. All results indicate that AErSe2 are strongly anisotropic, frustrated magnets with field-induced transition at low temperature. The lack of signatures for long-range magnetic order implies that these materials are candidates for hosting a quantum spin liquid ground state.},

  doi          = {10.1103/physrevmaterials.3.114413},

  journal      = {Physical Review Materials},

  number       = 11,

  volume       = 3,

  place        = {United States},

  year         = {Tue Nov 26 00:00:00 EST 2019},

  month        = {Tue Nov 26 00:00:00 EST 2019}

}

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Works referencing / citing this record:

Frustrated Magnetism in Triangular Lattice TlYbS$_2$ Crystals Grown via Molten Flux
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Ferreira, Timothy; Xing, Jie; Sanjeewa, Liurukara D.
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Title: Synthesis, magnetization, and heat capacity of triangular lattice materials NaErSe 2 and KErSe 2

Abstract

Citation Formats

Structural Disorder and Elementary Magnetic Properties of Triangular Lattice ErMgGaO4 Single Crystals text, January 2018

Quasi-two-dimensional antiferromagnet on a triangular lattice RbFe ( MoO 4 ) 2 journal, March 2003

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NaYbS 2 : A planar spin- 1 2 triangular-lattice magnet and putative spin liquid journal, December 2018

Evidence for a spinon Fermi surface in a triangular-lattice quantum-spin-liquid candidate journal, December 2016

Hidden multipolar orders of dipole-octupole doublets on a triangular lattice journal, November 2016

Magnetic transitions under ultrahigh magnetic fields of up to 130 T in the breathing pyrochlore antiferromagnet LiInCr 4 O 8 journal, April 2017

Field-tunable quantum disordered ground state in the triangular-lattice antiferromagnet NaYbO2 journal, July 2019

Anyons in an exactly solved model and beyond text, January 2005

A spin–orbital-entangled quantum liquid on a honeycomb lattice journal, February 2018

Experimental Realization of a Spin- 1 / 2 Triangular-Lattice Heisenberg Antiferromagnet journal, January 2012

Magnetization Process of the Spin-1/2 Antiferromagnetic Ising-Like Heisenberg Model on the Triangular Lattice journal, December 1986

Kitaev-Heisenberg Model on a Honeycomb Lattice: Possible Exotic Phases in Iridium Oxides A 2 IrO 3 journal, July 2010

Hidden multipolar orders of dipole-octupole doublets on a triangular lattice text, January 2016

Chemical disorder and spin-liquid-like magnetism in the van der Waals layered 5 d transition metal halide Os 0.55 Cl 2 journal, June 2019

Valence Bonds in Random Quantum Magnets: Theory and Application to YbMgGaO 4 journal, July 2018

Na2IrO3 as a molecular orbital crystal text, January 2012

Neutron scattering in the proximate quantum spin liquid α-RuCl3. text, January 2017

Low-temperature crystal and magnetic structure of α − RuCl 3 journal, April 2016

Selective measurements of intertwined multipolar orders: Non-Kramers doublets on a triangular lattice journal, July 2018

Proximate Kitaev quantum spin liquid behaviour in a honeycomb magnet journal, April 2016

Rare-Earth Chalcogenides: A Large Family of Triangular Lattice Spin Liquid Candidates journal, October 2018

Anyons in an exactly solved model and beyond journal, January 2006

Spin liquids in frustrated magnets journal, March 2010

Topography of Spin Liquids on a Triangular Lattice journal, May 2018

Magnetic pyrochlore oxides journal, January 2010

Simple Variational Wave Functions for Two-Dimensional Heisenberg Spin-½ Antiferromagnets journal, June 1988

Disorder-Induced Mimicry of a Spin Liquid in YbMgGaO 4 journal, October 2017

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Fractionalized excitations in the partially magnetized spin liquid candidate YbMgGaO4 journal, October 2018

Structural disorder and elementary magnetic properties of triangular lattice ErMgGaO4 single crystals journal, August 2018

Field-induced instability of the quantum spin liquid ground state in the J eff = 1 2 triangular-lattice compound NaYbO 2 journal, May 2019

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Hierarchy of exchange interactions in the triangular-lattice spin-liquid YbMgGaO$_{4}$ text, January 2017

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Relevance of the Heisenberg-Kitaev Model for the Honeycomb Lattice Iridates A 2 IrO 3 journal, March 2012

Continuous excitations of the triangular-lattice quantum spin liquid YbMgGaO4 journal, December 2016

Rare-Earth Triangular Lattice Spin Liquid: A Single-Crystal Study of YbMgGaO 4 journal, October 2015

Selective measurements of intertwined multipolar orders: non-Kramers doublets on a triangular lattice text, January 2018

Magnetization plateau in the frustrated quantum spin system Cs 2 CuBr 4 journal, March 2003

Field-induced lattice staircase in a frustrated antiferromagnet Cu Fe O 2 journal, November 2006

Kitaev materials beyond iridates: Order by quantum disorder and Weyl magnons in rare-earth double perovskites journal, February 2017

Kitaev materials beyond iridates: order by quantum disorder and Weyl magnons in rare-earth double perovskites text, January 2016

Anomalous Thermal Conductivity and Magnetic Torque Response in the Honeycomb Magnet α − RuCl 3 journal, May 2017

Quantum spin liquid in the spin- 1 ∕ 2 triangular antiferromagnet Et Me 3 Sb [ Pd ( dmit ) 2 ] 2 journal, March 2008

Resonating valence bonds: A new kind of insulator? journal, February 1973

Direct evidence of a zigzag spin-chain structure in the honeycomb lattice: A neutron and x-ray diffraction investigation of single-crystal Na 2 IrO 3 journal, May 2012

Antiferromagnetic Mott insulating state in single crystals of the honeycomb lattice material Na 2 IrO 3 journal, August 2010

Muon Spin Relaxation Evidence for the U(1) Quantum Spin-Liquid Ground State in the Triangular Antiferromagnet YbMgGaO 4 journal, August 2016

Hierarchy of Exchange Interactions in the Triangular-Lattice Spin Liquid YbMgGaO 4 journal, July 2018

Continuous excitations of the triangular-lattice quantum spin liquid YbMgGaO4 text, January 2016

Na 2 IrO 3 as a Molecular Orbital Crystal journal, November 2012

Direct evidence for dominant bond-directional interactions in a honeycomb lattice iridate Na2IrO3 journal, May 2015

Geometrical Frustration book, January 2010

Crystalline Electric-Field Randomness in the Triangular Lattice Spin-Liquid YbMgGaO 4 journal, March 2017

Gapless spin-liquid state in the structurally disorder-free triangular antiferromagnet NaYbO 2 journal, October 2019

Spin-Wave Excitations Evidencing the Kitaev Interaction in Single Crystalline α − RuCl 3 journal, March 2017

Frustrated Magnetism in Triangular Lattice TlYbS$_2$ Crystals Grown via Molten Flux text, January 2020

Field-induced magnetic transition and spin fluctuations in the quantum spin-liquid candidate CsYbSe 2 journal, December 2019

Frustrated Magnetism in Triangular Lattice TlYbS2 Crystals Grown via Molten Flux journal, February 2020

Title: Synthesis, magnetization, and heat capacity of triangular lattice materials ${NaErSe}_{2}$ and ${KErSe}_{2}$

Structural Disorder and Elementary Magnetic Properties of Triangular Lattice ErMgGaO4 Single Crystals
text, January 2018

Quasi-two-dimensional antiferromagnet on a triangular lattice $RbFe ({MoO}_{4})_{2}$
journal, March 2003

Geometrical frustration
journal, February 2006

${NaYbS}_{2}$ : A planar spin- $\frac{1}{2}$ triangular-lattice magnet and putative spin liquid
journal, December 2018

Evidence for a spinon Fermi surface in a triangular-lattice quantum-spin-liquid candidate
journal, December 2016

Hidden multipolar orders of dipole-octupole doublets on a triangular lattice
journal, November 2016

Magnetic transitions under ultrahigh magnetic fields of up to 130 T in the breathing pyrochlore antiferromagnet ${LiInCr}_{4} O_{8}$
journal, April 2017

Field-tunable quantum disordered ground state in the triangular-lattice antiferromagnet NaYbO2
journal, July 2019

Anyons in an exactly solved model and beyond
text, January 2005

A spin–orbital-entangled quantum liquid on a honeycomb lattice
journal, February 2018

Experimental Realization of a Spin- $1 / 2$ Triangular-Lattice Heisenberg Antiferromagnet
journal, January 2012

Magnetization Process of the Spin-1/2 Antiferromagnetic Ising-Like Heisenberg Model on the Triangular Lattice
journal, December 1986

Kitaev-Heisenberg Model on a Honeycomb Lattice: Possible Exotic Phases in Iridium Oxides $A_{2} {IrO}_{3}$
journal, July 2010

Hidden multipolar orders of dipole-octupole doublets on a triangular lattice
text, January 2016

Chemical disorder and spin-liquid-like magnetism in the van der Waals layered $5 d$ transition metal halide ${Os}_{0.55} {Cl}_{2}$
journal, June 2019

Valence Bonds in Random Quantum Magnets: Theory and Application to ${YbMgGaO}_{4}$
journal, July 2018

Na2IrO3 as a molecular orbital crystal
text, January 2012

Neutron scattering in the proximate quantum spin liquid α-RuCl3.
text, January 2017

Low-temperature crystal and magnetic structure of $α - {RuCl}_{3}$
journal, April 2016

Selective measurements of intertwined multipolar orders: Non-Kramers doublets on a triangular lattice
journal, July 2018

Proximate Kitaev quantum spin liquid behaviour in a honeycomb magnet
journal, April 2016

Rare-Earth Chalcogenides: A Large Family of Triangular Lattice Spin Liquid Candidates
journal, October 2018

Anyons in an exactly solved model and beyond
journal, January 2006

Spin liquids in frustrated magnets
journal, March 2010

Topography of Spin Liquids on a Triangular Lattice
journal, May 2018

Magnetic pyrochlore oxides
journal, January 2010

Simple Variational Wave Functions for Two-Dimensional Heisenberg Spin-½ Antiferromagnets
journal, June 1988

Disorder-Induced Mimicry of a Spin Liquid in ${YbMgGaO}_{4}$
journal, October 2017

Cu ₂ IrO ₃ : A New Magnetically Frustrated Honeycomb Iridate
journal, October 2017

Fractionalized excitations in the partially magnetized spin liquid candidate YbMgGaO4
journal, October 2018

Structural disorder and elementary magnetic properties of triangular lattice ErMgGaO4 single crystals
journal, August 2018

Field-induced instability of the quantum spin liquid ground state in the $J_{eff} = \frac{1}{2}$ triangular-lattice compound ${NaYbO}_{2}$
journal, May 2019

Anisotropic spin model of strong spin-orbit-coupled triangular antiferromagnets
journal, July 2016

Magnetic Phases of a Highly Frustrated Magnet, ${ZnCr}_{2} O_{4}$ , up to an Ultrahigh Magnetic Field of 600 T
journal, November 2011

Neutron scattering in the proximate quantum spin liquid α-RuCl ₃
journal, June 2017

Hierarchy of exchange interactions in the triangular-lattice spin-liquid YbMgGaO$_{4}$
text, January 2017

Hyperhoneycomb Iridate $β − {Li}_{2} {IrO}_{3}$ as a Platform for Kitaev Magnetism
journal, February 2015

Gapless quantum spin liquid ground state in the two-dimensional spin-1/2 triangular antiferromagnet YbMgGaO4
journal, November 2015

Quantum theory of an antiferromagnet on a triangular lattice in a magnetic field
journal, January 1991

Quantum Stabilization of the $1 / 3$ -Magnetization Plateau in ${Cs}_{2} {CuBr}_{4}$
journal, March 2009

Relevance of the Heisenberg-Kitaev Model for the Honeycomb Lattice Iridates $A_{2} {IrO}_{3}$
journal, March 2012

Continuous excitations of the triangular-lattice quantum spin liquid YbMgGaO4
journal, December 2016

Rare-Earth Triangular Lattice Spin Liquid: A Single-Crystal Study of ${YbMgGaO}_{4}$
journal, October 2015

Selective measurements of intertwined multipolar orders: non-Kramers doublets on a triangular lattice
text, January 2018

Magnetization plateau in the frustrated quantum spin system ${Cs}_{2} {CuBr}_{4}$
journal, March 2003

Field-induced lattice staircase in a frustrated antiferromagnet $Cu Fe O_{2}$
journal, November 2006

Kitaev materials beyond iridates: Order by quantum disorder and Weyl magnons in rare-earth double perovskites
journal, February 2017

Kitaev materials beyond iridates: order by quantum disorder and Weyl magnons in rare-earth double perovskites
text, January 2016

Anomalous Thermal Conductivity and Magnetic Torque Response in the Honeycomb Magnet $α − {RuCl}_{3}$
journal, May 2017

Quantum spin liquid in the spin- $1 ∕ 2$ triangular antiferromagnet $Et {Me}_{3} Sb {[Pd {(dmit)}_{2}]}_{2}$
journal, March 2008

Resonating valence bonds: A new kind of insulator?
journal, February 1973

Direct evidence of a zigzag spin-chain structure in the honeycomb lattice: A neutron and x-ray diffraction investigation of single-crystal Na $_{2}$ IrO $_{3}$
journal, May 2012

Antiferromagnetic Mott insulating state in single crystals of the honeycomb lattice material ${Na}_{2} {IrO}_{3}$
journal, August 2010

Muon Spin Relaxation Evidence for the U(1) Quantum Spin-Liquid Ground State in the Triangular Antiferromagnet ${YbMgGaO}_{4}$
journal, August 2016

Hierarchy of Exchange Interactions in the Triangular-Lattice Spin Liquid ${YbMgGaO}_{4}$
journal, July 2018

Continuous excitations of the triangular-lattice quantum spin liquid YbMgGaO4
text, January 2016

${Na}_{2} {IrO}_{3}$ as a Molecular Orbital Crystal
journal, November 2012

Direct evidence for dominant bond-directional interactions in a honeycomb lattice iridate Na2IrO3
journal, May 2015

Geometrical Frustration
book, January 2010

Crystalline Electric-Field Randomness in the Triangular Lattice Spin-Liquid ${YbMgGaO}_{4}$
journal, March 2017

Gapless spin-liquid state in the structurally disorder-free triangular antiferromagnet ${NaYbO}_{2}$
journal, October 2019

Spin-Wave Excitations Evidencing the Kitaev Interaction in Single Crystalline $α − {RuCl}_{3}$
journal, March 2017

Frustrated Magnetism in Triangular Lattice TlYbS$_2$ Crystals Grown via Molten Flux
text, January 2020

Field-induced magnetic transition and spin fluctuations in the quantum spin-liquid candidate ${CsYbSe}_{2}$
journal, December 2019

Frustrated Magnetism in Triangular Lattice TlYbS2 Crystals Grown via Molten Flux
journal, February 2020