Diffraction gratings with two-orders-of-magnitude-enhanced dispersion rates for sub-meV resolution soft X-ray spectroscopy
Abstract
Diffraction gratings with large angular dispersion rates are central to obtaining high spectral resolution in grating spectrometers operating over a broad spectral range from infrared to soft X-ray domains. The greatest challenge is of course to achieve large dispersion rates in the short-wavelength X-ray domain. Here it is shown that crystals in non-coplanar asymmetric X-ray Bragg diffraction can function as high-reflectance broadband soft X-ray diffraction gratings with dispersion rates that are at least two orders of magnitude larger than those that are possible with state-of-the-art man-made gratings. Additionally, this opens new opportunities to design and implement soft X-ray resonant inelastic scattering (RIXS) spectrometers with spectral resolutions that are up to two orders of magnitude higher than what is currently possible, to further advance a very dynamic field of RIXS spectroscopy, and to make it competitive with inelastic neutron scattering. Examples of large-dispersion-rate crystal diffraction gratings operating near the 930 eV L3 absorption edge in Cu and of the 2.838 keV L3-edge in Ru are presented.
- Authors:
-
- Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Office of Basic Energy Sciences (BES)
- OSTI Identifier:
- 1756934
- Grant/Contract Number:
- AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Synchrotron Radiation (Online)
- Additional Journal Information:
- Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 27; Journal Issue: 5; Journal ID: ISSN 1600-5775
- Publisher:
- International Union of Crystallography
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 73 NUCLEAR PHYSICS AND RADIATION PHYSICS; Bragg diffraction; X-rays; crystals; diffraction gratings; spectrometers
Citation Formats
Shvyd'ko, Yuri. Diffraction gratings with two-orders-of-magnitude-enhanced dispersion rates for sub-meV resolution soft X-ray spectroscopy. United States: N. p., 2020.
Web. doi:10.1107/s1600577520008292.
Shvyd'ko, Yuri. Diffraction gratings with two-orders-of-magnitude-enhanced dispersion rates for sub-meV resolution soft X-ray spectroscopy. United States. https://doi.org/10.1107/s1600577520008292
Shvyd'ko, Yuri. Thu .
"Diffraction gratings with two-orders-of-magnitude-enhanced dispersion rates for sub-meV resolution soft X-ray spectroscopy". United States. https://doi.org/10.1107/s1600577520008292. https://www.osti.gov/servlets/purl/1756934.
@article{osti_1756934,
title = {Diffraction gratings with two-orders-of-magnitude-enhanced dispersion rates for sub-meV resolution soft X-ray spectroscopy},
author = {Shvyd'ko, Yuri},
abstractNote = {Diffraction gratings with large angular dispersion rates are central to obtaining high spectral resolution in grating spectrometers operating over a broad spectral range from infrared to soft X-ray domains. The greatest challenge is of course to achieve large dispersion rates in the short-wavelength X-ray domain. Here it is shown that crystals in non-coplanar asymmetric X-ray Bragg diffraction can function as high-reflectance broadband soft X-ray diffraction gratings with dispersion rates that are at least two orders of magnitude larger than those that are possible with state-of-the-art man-made gratings. Additionally, this opens new opportunities to design and implement soft X-ray resonant inelastic scattering (RIXS) spectrometers with spectral resolutions that are up to two orders of magnitude higher than what is currently possible, to further advance a very dynamic field of RIXS spectroscopy, and to make it competitive with inelastic neutron scattering. Examples of large-dispersion-rate crystal diffraction gratings operating near the 930 eV L3 absorption edge in Cu and of the 2.838 keV L3-edge in Ru are presented.},
doi = {10.1107/s1600577520008292},
journal = {Journal of Synchrotron Radiation (Online)},
number = 5,
volume = 27,
place = {United States},
year = {Thu Jul 30 00:00:00 EDT 2020},
month = {Thu Jul 30 00:00:00 EDT 2020}
}
Works referenced in this record:
μm-resolved high resolution X-ray diffraction imaging for semiconductor quality control
journal, April 2000
- Lübbert, D.; Baumbach, T.; Härtwig, J.
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 160, Issue 4
X-Ray Bragg Diffraction in Asymmetric Backscattering Geometry
journal, December 2006
- Shvyd’ko, Yu.; Lerche, M.; Kuetgens, U.
- Physical Review Letters, Vol. 97, Issue 23
Spin–orbital separation in the quasi-one-dimensional Mott insulator Sr2CuO3
journal, April 2012
- Schlappa, J.; Wohlfeld, K.; Zhou, K. J.
- Nature, Vol. 485, Issue 7396
Multilayer-coated blazed grating with variable line spacing and a variable blaze angle
journal, January 2014
- Voronov, D. L.; Warwick, T.; Padmore, H. A.
- Optics Letters, Vol. 39, Issue 21
Theory of angular-dispersive, imaging hard-x-ray spectrographs
journal, May 2015
- Shvyd'ko, Yuri
- Physical Review A, Vol. 91, Issue 5
Complete polarization analysis of high energy soft x-rays by combining a multilayer phase retarder with crystal analyzer
journal, June 2012
- Wang, H.; Dhesi, S. S.; Maccherozzi, F.
- Journal of Applied Physics, Vol. 111, Issue 12
High-contrast sub-millivolt inelastic X-ray scattering for nano- and mesoscale science
journal, June 2014
- Shvyd’ko, Yuri; Stoupin, Stanislav; Shu, Deming
- Nature Communications, Vol. 5, Issue 1
SAXES, a high resolution spectrometer for resonant x-ray emission in the 400–1600eV energy range
journal, November 2006
- Ghiringhelli, G.; Piazzalunga, A.; Dallera, C.
- Review of Scientific Instruments, Vol. 77, Issue 11
The beamline ID32 at the ESRF for soft X-ray high energy resolution resonant inelastic X-ray scattering and polarisation dependent X-ray absorption spectroscopy
journal, September 2018
- Brookes, N. B.; Yakhou-Harris, F.; Kummer, K.
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 903
Intense paramagnon excitations in a large family of high-temperature superconductors
journal, July 2011
- Le Tacon, M.; Ghiringhelli, G.; Chaloupka, J.
- Nature Physics, Vol. 7, Issue 9
Experimental resolution in soft X-ray monochromators
journal, February 1989
- Kortboyer, S. W.; Goedkoop, J. B.; De Groot, F. M. F.
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 275, Issue 2
A double-crystal monochromator for EXAFS measurement at NSRL
journal, June 1998
- Xu, Chaoyin; Zhao, Weichang; Pan, Guoqiang
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 410, Issue 2
Specular x-ray reflection from a crystal coated with an amorphous film under the conditions for strongly asymmetric noncoplanar diffraction
journal, May 2001
- Bushuev, V. A.; Oreshko, A. P.
- Physics of the Solid State, Vol. 43, Issue 5
Persistence of magnetic excitations in La2−xSrxCuO4 from the undoped insulator to the heavily overdoped non-superconducting metal
journal, August 2013
- Dean, M. P. M.; Dellea, G.; Springell, R. S.
- Nature Materials, Vol. 12, Issue 11
High-resolution soft X-ray beamline ADRESS at the Swiss Light Source for resonant inelastic X-ray scattering and angle-resolved photoelectron spectroscopies
journal, July 2010
- Strocov, V. N.; Schmitt, T.; Flechsig, U.
- Journal of Synchrotron Radiation, Vol. 17, Issue 5
Modular soft x-ray spectrometer for applications in energy sciences and quantum materials
journal, January 2017
- Chuang, Yi-De; Shao, Yu-Cheng; Cruz, Alejandro
- Review of Scientific Instruments, Vol. 88, Issue 1
X-ray diffraction under specular reflection conditions. Ideal crystals
journal, March 1983
- Afanas'ev, A. M.; Melkonyan, M. K.
- Acta Crystallographica Section A Foundations of Crystallography, Vol. 39, Issue 2
Magnetic Excitations and Phase Separation in the Underdoped Superconductor Measured by Resonant Inelastic X-Ray Scattering
journal, February 2010
- Braicovich, L.; van den Brink, J.; Bisogni, V.
- Physical Review Letters, Vol. 104, Issue 7
Towards 10 meV resolution: The design of an ultrahigh resolution soft X-ray RIXS spectrometer
journal, November 2016
- Dvorak, Joseph; Jarrige, Ignace; Bisogni, Valentina
- Review of Scientific Instruments, Vol. 87, Issue 11
Bragg-Laue diffraction in inclined geometry
journal, November 1984
- Aleksandrov, P. A.; Afanasiev, A. M.; Stepanov, S. A.
- Physica Status Solidi (a), Vol. 86, Issue 1
Dispersive charge density wave excitations in Bi2Sr2CaCu2O8+δ
journal, June 2017
- Chaix, L.; Ghiringhelli, G.; Peng, Y. Y.
- Nature Physics, Vol. 13, Issue 10
High-order multilayer coated blazed gratings for high resolution soft x-ray spectroscopy
journal, January 2015
- Voronov, Dmitriy L.; Goray, Leonid I.; Warwick, Tony
- Optics Express, Vol. 23, Issue 4
Hard-X-Ray Spectroscopy with a Spectrographic Approach
journal, August 2019
- Chumakov, Aleksandr I.; Shvyd’ko, Yuri; Sergueev, Ilya
- Physical Review Letters, Vol. 123, Issue 9
The Crystal Monochromator at BESSY
conference, December 1987
- Feldhaus, J.; Schafers, F.; Peatman, W.
- Soft X-Rays Optics and Technology, SPIE Proceedings