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Title: Materials Characterization by Dynamic Nuclear Polarization-Enhanced Solid-State NMR Spectroscopy

Abstract

Here, high-resolution solid-state NMR spectroscopy is a powerful tool for the study of organic and inorganic materials because it can directly probe the symmetry and structure at nuclear sites, the connectivity/bonding of atoms and precisely measure interatomic distances. However, NMR spectroscopy is hampered by intrinsically poor sensitivity; consequently, the application of NMR spectroscopy to many solid materials is often infeasible. High-field dynamic nuclear polarization (DNP) has emerged as a technique to routinely enhance the sensitivity of solid-state NMR experiments by 1–3 orders of magnitude. This Perspective gives a general overview of how DNP-enhanced solid-state NMR spectroscopy can be applied to a variety of inorganic and organic materials. DNP-enhanced solid-state NMR experiments provide unique insights into the molecular structure, which makes it possible to form structure–activity relationships that ultimately assist in the rational design and improvement of materials.

Authors:
ORCiD logo [1]
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  1. Ames Lab. and Iowa State Univ., Ames, IA (United States)
Publication Date:
Research Org.:
Ames Lab., Ames, IA (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
OSTI Identifier:
1471221
Report Number(s):
IS-J-9750
Journal ID: ISSN 1948-7185
Grant/Contract Number:  
AC02-07CH11358
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Physical Chemistry Letters
Additional Journal Information:
Journal Volume: 9; Journal Issue: 17; Journal ID: ISSN 1948-7185
Publisher:
American Chemical Society
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 36 MATERIALS SCIENCE

Citation Formats

Rossini, Aaron J. Materials Characterization by Dynamic Nuclear Polarization-Enhanced Solid-State NMR Spectroscopy. United States: N. p., 2018. Web. doi:10.1021/acs.jpclett.8b01891.
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Rossini, Aaron J. Materials Characterization by Dynamic Nuclear Polarization-Enhanced Solid-State NMR Spectroscopy. United States. https://doi.org/10.1021/acs.jpclett.8b01891
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Rossini, Aaron J. Tue . "Materials Characterization by Dynamic Nuclear Polarization-Enhanced Solid-State NMR Spectroscopy". United States. https://doi.org/10.1021/acs.jpclett.8b01891. https://www.osti.gov/servlets/purl/1471221.
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@article{osti_1471221,
title = {Materials Characterization by Dynamic Nuclear Polarization-Enhanced Solid-State NMR Spectroscopy},
author = {Rossini, Aaron J.},
abstractNote = {Here, high-resolution solid-state NMR spectroscopy is a powerful tool for the study of organic and inorganic materials because it can directly probe the symmetry and structure at nuclear sites, the connectivity/bonding of atoms and precisely measure interatomic distances. However, NMR spectroscopy is hampered by intrinsically poor sensitivity; consequently, the application of NMR spectroscopy to many solid materials is often infeasible. High-field dynamic nuclear polarization (DNP) has emerged as a technique to routinely enhance the sensitivity of solid-state NMR experiments by 1–3 orders of magnitude. This Perspective gives a general overview of how DNP-enhanced solid-state NMR spectroscopy can be applied to a variety of inorganic and organic materials. DNP-enhanced solid-state NMR experiments provide unique insights into the molecular structure, which makes it possible to form structure–activity relationships that ultimately assist in the rational design and improvement of materials.},
doi = {10.1021/acs.jpclett.8b01891},
journal = {Journal of Physical Chemistry Letters},
number = 17,
volume = 9,
place = {United States},
year = {Tue Aug 14 00:00:00 EDT 2018},
month = {Tue Aug 14 00:00:00 EDT 2018}
}
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