Rapid ordering of block copolymer thin films
Abstract
Block-copolymers self-assemble into diverse morphologies, where nanoscale order can be finely tuned via block architecture and processing conditions. However, the ultimate usage of these materials in real-world applications may be hampered by the extremely long thermal annealing times—hours or days—required to achieve good order. Here, we provide an overview of the fundamentals of block-copolymer self-assembly kinetics, and review the techniques that have been demonstrated to influence, and enhance, these ordering kinetics. We discuss the inherent tradeoffs between oven annealing, solvent annealing, microwave annealing, zone annealing, and other directed self-assembly methods; including an assessment of spatial and temporal characteristics. Here, we also review both real-space and reciprocal-space analysis techniques for quantifying order in these systems.
- Authors:
-
- Brookhaven National Lab. (BNL), Upton, NY (United States); Univ. of Warsaw, Warsaw (Poland)
- Brookhaven National Lab. (BNL), Upton, NY (United States)
- Publication Date:
- Research Org.:
- Brookhaven National Laboratory (BNL), Upton, NY (United States). Center for Functional Nanomaterials (CFN)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1337654
- Alternate Identifier(s):
- OSTI ID: 1298332
- Report Number(s):
- BNL-113314-2016-JA
Journal ID: ISSN 0953-8984; KC0403020
- Grant/Contract Number:
- SC00112704; SC0012704
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Physics. Condensed Matter
- Additional Journal Information:
- Journal Volume: 28; Journal Issue: 40; Journal ID: ISSN 0953-8984
- Publisher:
- IOP Publishing
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 77 NANOSCIENCE AND NANOTECHNOLOGY; block copolymer; self-assembly; ordering; Center for Functional Nanomaterials; annealing; grain size; image analysis; ordering kinetics; morphology characterization; x-ray scattering
Citation Formats
Majewski, Pawel W., and Yager, Kevin G. Rapid ordering of block copolymer thin films. United States: N. p., 2016.
Web. doi:10.1088/0953-8984/28/40/403002.
Majewski, Pawel W., & Yager, Kevin G. Rapid ordering of block copolymer thin films. United States. https://doi.org/10.1088/0953-8984/28/40/403002
Majewski, Pawel W., and Yager, Kevin G. Thu .
"Rapid ordering of block copolymer thin films". United States. https://doi.org/10.1088/0953-8984/28/40/403002. https://www.osti.gov/servlets/purl/1337654.
@article{osti_1337654,
title = {Rapid ordering of block copolymer thin films},
author = {Majewski, Pawel W. and Yager, Kevin G.},
abstractNote = {Block-copolymers self-assemble into diverse morphologies, where nanoscale order can be finely tuned via block architecture and processing conditions. However, the ultimate usage of these materials in real-world applications may be hampered by the extremely long thermal annealing times—hours or days—required to achieve good order. Here, we provide an overview of the fundamentals of block-copolymer self-assembly kinetics, and review the techniques that have been demonstrated to influence, and enhance, these ordering kinetics. We discuss the inherent tradeoffs between oven annealing, solvent annealing, microwave annealing, zone annealing, and other directed self-assembly methods; including an assessment of spatial and temporal characteristics. Here, we also review both real-space and reciprocal-space analysis techniques for quantifying order in these systems.},
doi = {10.1088/0953-8984/28/40/403002},
journal = {Journal of Physics. Condensed Matter},
number = 40,
volume = 28,
place = {United States},
year = {Thu Aug 18 00:00:00 EDT 2016},
month = {Thu Aug 18 00:00:00 EDT 2016}
}
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