Simple Setup Miniaturization with Multiple Benefits for Green Chemistry in Nanoparticle Synthesis

Mathiesen, Jette K.; Cooper, Susan R.; Anker, Andy S.; Kinnibrugh, Tiffany L.; Jensen, Kirsten M. Ø.; Quinson, Jonathan

doi:10.1021/acsomega.2c00030

Title: Simple Setup Miniaturization with Multiple Benefits for Green Chemistry in Nanoparticle Synthesis

Journal Article · 24 January 2022 · ACS Omega

DOI: https://doi.org/10.1021/acsomega.2c00030 · OSTI ID:1905315

Mathiesen, Jette K. ^[1];

^[1];

^[1]; Kinnibrugh, Tiffany L. ^[2];

^[1];

^[1]

Univ. of Copenhagen (Denmark)
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

The development of nanomaterials often relies on wet-chemical synthesis performed in reflux setups using round-bottom flasks. Here, an alternative approach to synthesize nanomaterials is presented that uses glass tubes designed for NMR analysis as reactors. This approach uses less solvent and energy, generates less waste, provides safer conditions, is less prone to contamination, and is compatible with high-throughput screening. The benefits of this approach are illustrated by an in breadth study with the synthesis of gold, iridium, osmium, and copper sulfide nanoparticles.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: Danish National Research Foundation; European Union (EU); USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division; Villum Foundation

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1905315

Journal Information:: ACS Omega, Journal Name: ACS Omega Journal Issue: 5 Vol. 7; ISSN 2470-1343

Publisher:: American Chemical Society (ACS)Copyright Statement

Country of Publication:: United States

Language:: English

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Related Subjects

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
High throughput
Miniaturization
Nanoparticles
Screening
Synthesis

Title: Simple Setup Miniaturization with Multiple Benefits for Green Chemistry in Nanoparticle Synthesis

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