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Title: Multiscale dynamic experiments on fiber-reinforced composites with damage assessment using high-speed synchrotron X-ray phase-contrast imaging

Abstract

We report fiber-reinforced composites (FRCs) have been widely used as protection materials to replace heavier metals. However, predictive capabilities for the impact-induced failure of FRCs have not been well-developed. In this work, we introduced an integrated technique to visualize the dynamic failure of FRCs, with the modified Kolsky bar loading and the high-speed synchrotron X-ray phase-contrast imaging (PCI). We summarize our experimental studies across the FRCs’ structural levels by using this integrated technique, including single-fiber tensile experiments, fiber/matrix debonding experiments, and single-edge notched bending experiments on composite laminates. It is revealed that the high-speed synchrotron X-ray PCI technique possesses sufficient spatial resolution to identify the failure behavior of a single fiber in the 10-μm scale level, as well as temporal resolution to identify the time sequence of internal dynamic damage evolution. The technique can penetrate through the opaque composite sample and provide real-time visualization of small-scale damaging mechanisms such as the embedded fiber’s sliding in the matrix and the fiber’s transverse debonding with the matrix. At an expanding scale, the technique can identify the crack initiation and track the cracking behavior inside a single ply or between different plies of a composite laminate. High-speed visualization inside the material by thismore » integrated technique provides critical deformation and failure information to develop physical understanding of the damage inside composites under impact.« less

Authors:
 [1]; ORCiD logo [2];  [1]
  1. Purdue University, West Lafayette, IN (United States)
  2. Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES); Army Research Laboratory (ARL); US Air Force Office of Scientific Research (AFOSR)
OSTI Identifier:
1894893
Alternate Identifier(s):
OSTI ID: 1867938
Grant/Contract Number:  
AC02-06CH11357; W911NF-12-2-0022; FA9550-16-1-0315
Resource Type:
Accepted Manuscript
Journal Name:
NDT & E International
Additional Journal Information:
Journal Volume: 129; Journal ID: ISSN 0963-8695
Publisher:
Elsevier
Country of Publication:
United States
Language:
English
Subject:
47 OTHER INSTRUMENTATION; dynamic failure; fiber-reinforced composites; Kolsky bar; phase-contrast imaging; synchrotron radiation

Citation Formats

Gao, Jinling, Fezzaa, Kamel, and Chen, Weinong. Multiscale dynamic experiments on fiber-reinforced composites with damage assessment using high-speed synchrotron X-ray phase-contrast imaging. United States: N. p., 2022. Web. doi:10.1016/j.ndteint.2022.102636.
Gao, Jinling, Fezzaa, Kamel, & Chen, Weinong. Multiscale dynamic experiments on fiber-reinforced composites with damage assessment using high-speed synchrotron X-ray phase-contrast imaging. United States. https://doi.org/10.1016/j.ndteint.2022.102636
Gao, Jinling, Fezzaa, Kamel, and Chen, Weinong. Fri . "Multiscale dynamic experiments on fiber-reinforced composites with damage assessment using high-speed synchrotron X-ray phase-contrast imaging". United States. https://doi.org/10.1016/j.ndteint.2022.102636. https://www.osti.gov/servlets/purl/1894893.
@article{osti_1894893,
title = {Multiscale dynamic experiments on fiber-reinforced composites with damage assessment using high-speed synchrotron X-ray phase-contrast imaging},
author = {Gao, Jinling and Fezzaa, Kamel and Chen, Weinong},
abstractNote = {We report fiber-reinforced composites (FRCs) have been widely used as protection materials to replace heavier metals. However, predictive capabilities for the impact-induced failure of FRCs have not been well-developed. In this work, we introduced an integrated technique to visualize the dynamic failure of FRCs, with the modified Kolsky bar loading and the high-speed synchrotron X-ray phase-contrast imaging (PCI). We summarize our experimental studies across the FRCs’ structural levels by using this integrated technique, including single-fiber tensile experiments, fiber/matrix debonding experiments, and single-edge notched bending experiments on composite laminates. It is revealed that the high-speed synchrotron X-ray PCI technique possesses sufficient spatial resolution to identify the failure behavior of a single fiber in the 10-μm scale level, as well as temporal resolution to identify the time sequence of internal dynamic damage evolution. The technique can penetrate through the opaque composite sample and provide real-time visualization of small-scale damaging mechanisms such as the embedded fiber’s sliding in the matrix and the fiber’s transverse debonding with the matrix. At an expanding scale, the technique can identify the crack initiation and track the cracking behavior inside a single ply or between different plies of a composite laminate. High-speed visualization inside the material by this integrated technique provides critical deformation and failure information to develop physical understanding of the damage inside composites under impact.},
doi = {10.1016/j.ndteint.2022.102636},
journal = {NDT & E International},
number = ,
volume = 129,
place = {United States},
year = {Fri Mar 18 00:00:00 EDT 2022},
month = {Fri Mar 18 00:00:00 EDT 2022}
}

Works referenced in this record:

Fatigue micromechanism characterisation in carbon fibre reinforced polymers using synchrotron radiation computed tomography
journal, July 2014


Transverse impact by RCCs on S-glass and Kevlar® FRC strips
journal, July 2021


Gas gun shock experiments with single-pulse x-ray phase contrast imaging and diffraction at the Advanced Photon Source
journal, July 2012

  • Luo, S. N.; Jensen, B. J.; Hooks, D. E.
  • Review of Scientific Instruments, Vol. 83, Issue 7
  • DOI: 10.1063/1.4733704

Failure behaviors of single high-performance fibers under transverse dynamic cut
journal, October 2020


Real-time damage characterization for GFRCs using high-speed synchrotron X-ray phase contrast imaging
journal, February 2021


Interlaminar fracture micro-mechanisms in toughened carbon fibre reinforced plastics investigated via synchrotron radiation computed tomography and laminography
journal, April 2015


The role of twist in dry spun carbon nanotube yarns
journal, January 2016


Review and benchmark study on the analysis of low-velocity impact on composite laminates
journal, April 2018


Rate effects on fiber–matrix interfacial transverse debonding behavior
journal, October 2019

  • Chu, Jou-Mei; Claus, Benjamin; Lim, Boon Him
  • Journal of Composite Materials, Vol. 54, Issue 4
  • DOI: 10.1177/0021998319866904

X-Ray Interactions: Photoabsorption, Scattering, Transmission, and Reflection at E = 50-30,000 eV, Z = 1-92
journal, July 1993

  • Henke, B. L.; Gullikson, E. M.; Davis, J. C.
  • Atomic Data and Nuclear Data Tables, Vol. 54, Issue 2, p. 181-342
  • DOI: 10.1006/adnd.1993.1013

Strong, Light, Multifunctional Fibers of Carbon Nanotubes with Ultrahigh Conductivity
journal, January 2013


An experimental investigation into dynamic fracture: III. On steady-state crack propagation and crack branching
journal, October 1984

  • Ravi-Chandar, K.; Knauss, W. G.
  • International Journal of Fracture, Vol. 26, Issue 2
  • DOI: 10.1007/BF01157550

Ballistic impact mechanisms – A review on textiles and fibre-reinforced composites impact responses
journal, September 2019


In Situ Visual Observation of Fracture Processes in Several High-Performance Fibers
journal, February 2015

  • Hudspeth, Matthew; Claus, Ben; Parab, Niranjan
  • Journal of Dynamic Behavior of Materials, Vol. 1, Issue 1
  • DOI: 10.1007/s40870-015-0009-3

Experimental investigation of the influence of dynamic multiaxial transverse loading on ultrahigh molecular weight polyethylene single fiber failure
journal, March 2021

  • Thomas, Frank David; Alexander, Stephen L.; Weerasooriya, Tusit
  • Composites Part A: Applied Science and Manufacturing, Vol. 142
  • DOI: 10.1016/j.compositesa.2020.106250

A comparison of multi-scale 3D X-ray tomographic inspection techniques for assessing carbon fibre composite impact damage
journal, February 2013


In situ observations of fractures in short carbon fiber/epoxy composites
journal, February 2014


Visualization of dynamic fiber-matrix interfacial shear debonding
journal, October 2017

  • Chu, Jou-Mei; Claus, Benjamin; Parab, Niranjan
  • Journal of Materials Science, Vol. 53, Issue 8
  • DOI: 10.1007/s10853-017-1759-1

Quasi-static and dynamic fracture of graphite/epoxy composites: An optical study of loading-rate effects
journal, September 2010


Effects of extreme transverse deformation on the strength of UHMWPE single filaments for ballistic applications
journal, June 2016


X-ray computed tomography study of kink bands in unidirectional composites
journal, January 2017


In situ synchrotron tomographic evaluation of the effect of toughening strategies on fatigue micromechanisms in carbon fibre reinforced polymers
journal, March 2015


In-situ observation of cutting-induced failure processes of single high-performance fibers inside a SEM
journal, April 2020


Quantitative X-ray tomography
journal, December 2013


Mesoscale ballistic damage mechanisms of a single-layer woven glass/epoxy composite
journal, March 2018

  • Meyer, Christopher S.; Haque, Bazle Z. (Gama); O'Brien, Daniel J.
  • International Journal of Impact Engineering, Vol. 113
  • DOI: 10.1016/j.ijimpeng.2017.11.005

A method for characterization of multiple dynamic constitutive parameters of FRCs
journal, February 2021


Damage investigation and modeling of 3D woven ceramic matrix composites from X-ray tomography in-situ tensile tests
journal, November 2017


X-ray computed tomography of polymer composites
journal, March 2018


Artefacts in X-ray microtomography of materials
journal, September 2006


Key Factors Limiting Carbon Nanotube Yarn Strength: Exploring Processing-Structure-Property Relationships
journal, October 2014

  • Beese, Allison M.; Wei, Xiaoding; Sarkar, Sourangsu
  • ACS Nano, Vol. 8, Issue 11
  • DOI: 10.1021/nn5045504