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Title: Axial-torsion behavior of superelastic tubes: Part I, proportional isothermal experiments

Abstract

The tensile response of superelastic shape memory alloys (SMAs) has been widely researched, but detailed experimental studies under multi-axial loading are relatively rare. In Part I, we introduce the isothermal responses of commercially-available superelastic NiTi tubes for a series of proportional stretch-twist controlled histories, spanning pure tension to simple torsion to pure compression. These axial-shear responses are used to quantify the onset and saturation during forward (loading) and reverse (unloading) stress-induced transformations for the first time. Each of the four transformation surfaces is well-captured by a smooth (three-parameter) ellipse in both strain and stress space. A simple Gibbs free energy model is presented to show how the driving force for phase transformation is approximately constant across all proportional strain paths and how the stress and strain transformation surfaces are conjugate to one another. In addition, transformation kinetics and surface strain morphologies are characterized by stereo digital image correlation (DIC). Under extension at low amounts of twist, stress-induced transformation involves strain localization in helical bands that evolve into axial propagation of ring-like transformation fronts with fine criss-crossing fingers (similar to those seen by Q. P. Sun and co-workers in pure extension). Yet, at large amounts of twist, including simple torsion andmore » pure torsion, we report a new transformation morphology, involving strain localization along nearly longitudinal bands in the tube. The sequel (Part II) will address the response to non-proportional stretch-twist paths. Together, these detailed multi-axial results advance the scientific understanding of superelasticity and inform efforts to develop high-fidelity SMA constitutive models and simulation tools.« less

Authors:
; ORCiD logo; ORCiD logo;
Publication Date:
Research Org.:
Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES); National Science Foundation (NSF); UM/General Motors
OSTI Identifier:
1881358
Alternate Identifier(s):
OSTI ID: 1617827; OSTI ID: 1618100; OSTI ID: 1619230; OSTI ID: 1619827
Report Number(s):
SAND2020-3638J; SAND2019-4077J; SAND-2020-3638J
Journal ID: ISSN 0020-7683; S0020768320301062; PII: S0020768320301062
Grant/Contract Number:  
SC0003996; CMMI 1251891; AC04-94AL85000; 1251891
Resource Type:
Published Article
Journal Name:
International Journal of Solids and Structures
Additional Journal Information:
Journal Name: International Journal of Solids and Structures Journal Volume: 199 Journal Issue: C; Journal ID: ISSN 0020-7683
Publisher:
Elsevier
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 42 ENGINEERING; shape memory alloy; NiTi; Nitinol; superelasticity; phase transformation; multi-axial testing; constitutive behavior

Citation Formats

Reedlunn, Benjamin, LePage, William S., Daly, Samantha H., and Shaw, John A. Axial-torsion behavior of superelastic tubes: Part I, proportional isothermal experiments. United States: N. p., 2020. Web. doi:10.1016/j.ijsolstr.2020.03.018.
Reedlunn, Benjamin, LePage, William S., Daly, Samantha H., & Shaw, John A. Axial-torsion behavior of superelastic tubes: Part I, proportional isothermal experiments. United States. https://doi.org/10.1016/j.ijsolstr.2020.03.018
Reedlunn, Benjamin, LePage, William S., Daly, Samantha H., and Shaw, John A. Sat . "Axial-torsion behavior of superelastic tubes: Part I, proportional isothermal experiments". United States. https://doi.org/10.1016/j.ijsolstr.2020.03.018.
@article{osti_1881358,
title = {Axial-torsion behavior of superelastic tubes: Part I, proportional isothermal experiments},
author = {Reedlunn, Benjamin and LePage, William S. and Daly, Samantha H. and Shaw, John A.},
abstractNote = {The tensile response of superelastic shape memory alloys (SMAs) has been widely researched, but detailed experimental studies under multi-axial loading are relatively rare. In Part I, we introduce the isothermal responses of commercially-available superelastic NiTi tubes for a series of proportional stretch-twist controlled histories, spanning pure tension to simple torsion to pure compression. These axial-shear responses are used to quantify the onset and saturation during forward (loading) and reverse (unloading) stress-induced transformations for the first time. Each of the four transformation surfaces is well-captured by a smooth (three-parameter) ellipse in both strain and stress space. A simple Gibbs free energy model is presented to show how the driving force for phase transformation is approximately constant across all proportional strain paths and how the stress and strain transformation surfaces are conjugate to one another. In addition, transformation kinetics and surface strain morphologies are characterized by stereo digital image correlation (DIC). Under extension at low amounts of twist, stress-induced transformation involves strain localization in helical bands that evolve into axial propagation of ring-like transformation fronts with fine criss-crossing fingers (similar to those seen by Q. P. Sun and co-workers in pure extension). Yet, at large amounts of twist, including simple torsion and pure torsion, we report a new transformation morphology, involving strain localization along nearly longitudinal bands in the tube. The sequel (Part II) will address the response to non-proportional stretch-twist paths. Together, these detailed multi-axial results advance the scientific understanding of superelasticity and inform efforts to develop high-fidelity SMA constitutive models and simulation tools.},
doi = {10.1016/j.ijsolstr.2020.03.018},
journal = {International Journal of Solids and Structures},
number = C,
volume = 199,
place = {United States},
year = {Sat Aug 01 00:00:00 EDT 2020},
month = {Sat Aug 01 00:00:00 EDT 2020}
}

Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
https://doi.org/10.1016/j.ijsolstr.2020.03.018

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Cited by: 13 works
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Works referenced in this record:

Tension–compression asymmetry of the stress–strain response in aged single crystal and polycrystalline NiTi
journal, March 1999


Mechanical Behavior of an Ni-Ti Shape Memory Alloy Under Axial-Torsional Proportional and Nonproportional Loading
journal, January 1999

  • Lim, T. Jesse; McDowell, David L.
  • Journal of Engineering Materials and Technology, Vol. 121, Issue 1
  • DOI: 10.1115/1.2816007

Orthotropic yield criterion for hexagonal closed packed metals
journal, July 2006


Experimental study on the thermoelastic martensitic transformation in shape memory alloy polycrystal induced by combined external forces
journal, November 1995

  • Sittner, Petr; Hara, Yasuhiro; Tokuda, Masataka
  • Metallurgical and Materials Transactions A, Vol. 26, Issue 11
  • DOI: 10.1007/BF02669649

Anisotropic behavior of superelastic NiTi shape memory alloys; an experimental investigation and constitutive modeling
journal, October 2014


Tension, compression, and bending of superelastic shape memory alloy tubes
journal, February 2014

  • Reedlunn, Benjamin; Churchill, Christopher B.; Nelson, Emily E.
  • Journal of the Mechanics and Physics of Solids, Vol. 63
  • DOI: 10.1016/j.jmps.2012.12.012

Shape Memory Alloy Based Morphing Aerostructures
journal, November 2010

  • Calkins, Frederick T.; Mabe, James H.
  • Journal of Mechanical Design, Vol. 132, Issue 11
  • DOI: 10.1115/1.4001119

New interpretation of monotonic Swift effects: Role of tension–compression asymmetry
journal, February 2013


Correlation between swift effects and tension–compression asymmetry in various polycrystalline materials
journal, October 2014

  • Revil-Baudard, Benoit; Chandola, Nitin; Cazacu, Oana
  • Journal of the Mechanics and Physics of Solids, Vol. 70
  • DOI: 10.1016/j.jmps.2014.05.012

Macroscopic equilibrium domain structure and geometric compatibility in elastic phase transition of thin plates
journal, February 2010


Uniaxial, pure bending, and column buckling experiments on superelastic NiTi rods and tubes
journal, August 2018


Non-proportional multiaxial whole-life transformation ratchetting and fatigue failure of super-elastic NiTi shape memory alloy micro-tubes
journal, November 2015


Phase transformation in superelastic NiTi polycrystalline micro-tubes under tension and torsion––from localization to homogeneous deformation
journal, June 2002


A criterion for description of anisotropy and yield differential effects in pressure-insensitive metals
journal, November 2004


Tips and Tricks for Characterizing Shape Memory Wire Part 5: Full-Field Strain Measurement by Digital Image Correlation
journal, May 2011


The initiation and growth of macroscopic martensite band in nano-grained NiTi microtube under tension
journal, November 2002


Deformation and transition behavior associated with theR-phase in Ti-Ni alloys
journal, January 1986

  • Miyazaki, S.; Otsuka, K.
  • Metallurgical Transactions A, Vol. 17, Issue 1
  • DOI: 10.1007/BF02644442

Experimental Study of NiTi Thin-Walled Tubes Under Uniaxial Tension, Torsion, Proportional and Non-Proportional Loadings
journal, April 2015


Initiation and propagation of localized deformation in elasto-plastic strips under uniaxial tension
journal, December 1997


Multiaxial low-cycle fatigue failure mechanism of super-elastic NiTi shape memory alloy micro-tubes
journal, May 2016


Effect of product form and heat treatment on the crystallographic texture of austenitic Nitinol
journal, February 2006

  • Robertson, S. W.; Gong, X. Y.; Ritchie, R. O.
  • Journal of Materials Science, Vol. 41, Issue 3
  • DOI: 10.1007/s10853-006-6478-y

Path dependence and multiaxial behavior of a polycrystalline NiTi alloy within the pseudoelastic and pseudoplastic temperature regimes
journal, March 2009


Evolution of localization in pseudoelastic NiTi tubes under biaxial stress states
journal, July 2016


On the viscous and strain rate dependent behavior of polycrystalline NiTi
journal, April 2008


Multiaxial Shape Memory Effect and Superelasticity
journal, February 2009


On equilibrium domains in superelastic NiTi tubes — helix versus cylinder
journal, May 2012


Underlying material response for Lüders-like instabilities
journal, August 2013


Evolution of phase transformation fronts and associated thermal effects in a NiTi tube under a biaxial stress state
journal, September 2016


Tension/torsion tests of pseudoelastic, polycrystalline NiTi shape memory alloys under temperature control
journal, May 2008


An experimental study of the superelastic effect in a shape-memory Nitinol alloy under biaxial loading
journal, October 2003


On the nucleation and propagation of phase transformation fronts in a NiTi alloy
journal, February 1997


Impact of thermomechanical texture on the superelastic response of Nitinol implants
journal, October 2011

  • Barney, M. M.; Xu, D.; Robertson, S. W.
  • Journal of the Mechanical Behavior of Biomedical Materials, Vol. 4, Issue 7
  • DOI: 10.1016/j.jmbbm.2011.05.013

Optimum Paint Sequence for Speckle Patterns in Digital Image Correlation
journal, June 2017


Experimental Study of the Biaxial Cyclic Behavior of Thin-Wall Tubes of NiTi Shape Memory Alloys
journal, July 2012

  • Wang, X. M.; Zhou, Q. T.; Liu, H.
  • Metallurgical and Materials Transactions A, Vol. 43, Issue 11
  • DOI: 10.1007/s11661-012-1225-2