Diamond channel-cut crystals for high-heat-load beam-multiplexing narrow-band X-ray monochromators

Shvyd'ko, Yuri; Terentyev, Sergey; Blank, Vladimir; Kolodziej, Tomasz

doi:10.1107/S1600577521007943

Title: Diamond channel-cut crystals for high-heat-load beam-multiplexing narrow-band X-ray monochromators

Abstract

Next-generation high-brilliance X-ray photon sources call for new X-ray optics. Here we demonstrate the possibility of using monolithic diamond channel-cut crystals as high-heat-load beam-multiplexing narrow-band mechanically stable X-ray monochromators with high-power X-ray beams at cutting-edge high-repetition-rate X-ray free-electron laser (XFEL) facilities. The diamond channel-cut crystals fabricated and characterized in these studies are designed as two-bounce Bragg reflection monochromators directing 14.4 or 12.4 keV X-rays within a 15 meV bandwidth to ⁵⁷ Fe or ⁴⁵ Sc nuclear resonant scattering experiments, respectively. The crystal design allows out-of-band X-rays transmitted with minimal losses to alternative simultaneous experiments. Only ≲2% of the incident ∼100 W X-ray beam is absorbed in the 50 µm-thick first diamond crystal reflector, ensuring that the monochromator crystal is highly stable. Other X-ray optics applications of diamond channel-cut crystals are anticipated.

Authors:

; Terentyev, Sergey; Blank, Vladimir;

Publication Date:: Mon Sep 13 00:00:00 EDT 2021

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1844808

Alternate Identifier(s):: OSTI ID: 1894243

Grant/Contract Number:: AC02-06CH11357

Resource Type:: Published Article

Journal Name:: Journal of Synchrotron Radiation (Online)

Additional Journal Information:: Journal Name: Journal of Synchrotron Radiation (Online) Journal Volume: 28 Journal Issue: 6; Journal ID: ISSN 1600-5775

Publisher:: International Union of Crystallography (IUCr)

Country of Publication:: Denmark

Language:: English

Subject:: 73 NUCLEAR PHYSICS AND RADIATION PHYSICS; Bragg diffraction; crystals; diamond; x-ray optics; x-rays

Citation Formats


                    Shvyd'ko, Yuri, Terentyev, Sergey, Blank, Vladimir, and Kolodziej, Tomasz. Diamond channel-cut crystals for high-heat-load beam-multiplexing narrow-band X-ray monochromators.  Denmark: N. p., 2021. 
Web.  doi:10.1107/S1600577521007943.

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                    Shvyd'ko, Yuri, Terentyev, Sergey, Blank, Vladimir, & Kolodziej, Tomasz. Diamond channel-cut crystals for high-heat-load beam-multiplexing narrow-band X-ray monochromators.  Denmark.  https://doi.org/10.1107/S1600577521007943

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                    Shvyd'ko, Yuri, Terentyev, Sergey, Blank, Vladimir, and Kolodziej, Tomasz. Mon .  
"Diamond channel-cut crystals for high-heat-load beam-multiplexing narrow-band X-ray monochromators".  Denmark.  https://doi.org/10.1107/S1600577521007943.

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@article{osti_1844808,

  title        = {Diamond channel-cut crystals for high-heat-load beam-multiplexing narrow-band X-ray monochromators},

  author       = {Shvyd'ko, Yuri and Terentyev, Sergey and Blank, Vladimir and Kolodziej, Tomasz},

  abstractNote = {Next-generation high-brilliance X-ray photon sources call for new X-ray optics. Here we demonstrate the possibility of using monolithic diamond channel-cut crystals as high-heat-load beam-multiplexing narrow-band mechanically stable X-ray monochromators with high-power X-ray beams at cutting-edge high-repetition-rate X-ray free-electron laser (XFEL) facilities. The diamond channel-cut crystals fabricated and characterized in these studies are designed as two-bounce Bragg reflection monochromators directing 14.4 or 12.4 keV X-rays within a 15 meV bandwidth to 57 Fe or 45 Sc nuclear resonant scattering experiments, respectively. The crystal design allows out-of-band X-rays transmitted with minimal losses to alternative simultaneous experiments. Only ≲2% of the incident ∼100 W X-ray beam is absorbed in the 50 µm-thick first diamond crystal reflector, ensuring that the monochromator crystal is highly stable. Other X-ray optics applications of diamond channel-cut crystals are anticipated.},

  doi          = {10.1107/S1600577521007943},

  journal      = {Journal of Synchrotron Radiation (Online)},

  number       = 6,

  volume       = 28,

  place        = {Denmark},

  year         = {Mon Sep 13 00:00:00 EDT 2021},

  month        = {Mon Sep 13 00:00:00 EDT 2021}

}

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Title: Diamond channel-cut crystals for high-heat-load beam-multiplexing narrow-band X-ray monochromators

Abstract

Citation Formats

The multicrystal monochromators of the TROIKA beamline at ESRF journal, May 1998

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μm-resolved high resolution X-ray diffraction imaging for semiconductor quality control journal, April 2000

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A novel self-seeding scheme for hard X-ray FELs journal, September 2011

X-ray FEL with a meV bandwidth journal, December 2001

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X-ray photon correlation spectroscopy journal, August 2014

Principles and design of Laue-case X-Ray interferometers journal, April 1965

Parabolic single-crystal diamond lenses for coherent x-ray imaging journal, September 2015

Maximizing spectral flux from self-seeding hard x-ray free electron lasers journal, December 2013

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The influence of crystallization temperature and boron concentration in growth environment on its distribution in growth sectors of type IIb diamond journal, April 2007

High-reflectivity high-resolution X-ray crystal optics with diamonds journal, January 2010

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Small Bragg-plane slope errors revealed in synthetic diamond crystals journal, October 2020

Thermal Expansion of Diamond at Low Temperatures journal, February 2010

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Performance of a beam-multiplexing diamond crystal monochromator at the Linac Coherent Light Source journal, June 2014

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All-diamond optical assemblies for a beam-multiplexing X-ray monochromator at the Linac Coherent Light Source journal, August 2014

Thermal conductivity of isotopically modified single crystal diamond journal, June 1993

Near-100% Bragg reflectivity of X-rays journal, August 2011

The multicrystal monochromators of the TROIKA beamline at ESRF
journal, May 1998

Diamond x-ray optics: Transparent, resilient, high-resolution, and wavefront preserving
journal, June 2017

Thermal conductivity of high purity synthetic single crystal diamonds
journal, April 2018

μm-resolved high resolution X-ray diffraction imaging for semiconductor quality control
journal, April 2000

Ultraprecise studies of the thermal expansion coefficient of diamond using backscattering x-ray diffraction
journal, March 2011

Performance of a silicon monochromator under high heat load
journal, January 2014

A novel self-seeding scheme for hard X-ray FELs
journal, September 2011

X-ray FEL with a meV bandwidth
journal, December 2001

Ultra-high-resolution inelastic X-ray scattering at high-repetition-rate self-seeded X-ray free-electron lasers
journal, February 2016

X-ray photon correlation spectroscopy
journal, August 2014

Principles and design of Laue-case X-Ray interferometers
journal, April 1965

Parabolic single-crystal diamond lenses for coherent x-ray imaging
journal, September 2015

Maximizing spectral flux from self-seeding hard x-ray free electron lasers
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Diamond drumhead crystals for X-ray optics applications
journal, July 2016

The influence of crystallization temperature and boron concentration in growth environment on its distribution in growth sectors of type IIb diamond
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journal, October 2020

Thermal Expansion of Diamond at Low Temperatures
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Demonstration of self-seeding in a hard-X-ray free-electron laser
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journal, April 1966

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On the direct measurement of nuclear γ-resonance parameters of long-lived (≥1 s) isomers
journal, October 1990

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journal, November 1994

An X‐Ray Interferometer
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