Selection of CVD Diamond Crystals for X-ray Monochromator Applications Using X-ray Diffraction Imaging
Abstract
A set of 20 single crystal diamond plates synthesized using chemical vapor deposition (CVD) was studied using X-ray diffraction imaging to determine their applicability as side-bounce (single-reflection) Laue monochromators for synchrotron radiation. The crystal plates were of optical grade (as provided by the supplier) with (001) nominal surface orientation. High dislocation density was found for all samples. Distortions in the crystal lattice were quantified for low-index Laue reflections of interests using rocking curve topography. Maps of effective radius of curvature in the scattering plane were calculated using spline interpolation of the rocking curve peak position across the studied plates. For several selected plates, nearly flat regions with large effective radius of curvature were found (R0 ≳ 30 - 70 m, some regions as large as 1 × 4 mm2). The average width of the rocking curve for these regions was found to be about 150 μ rad (r.m.s.). These observations suggest that the selected CVD diamond plates could be used as intermediate-bandwidth monochromators refocusing the radiation source to a specific location downstream with close to 1:1 distance ratio.
- Authors:
-
- Cornell Univ., Ithaca, NY (United States)
- Argonne National Lab. (ANL), Lemont, IL (United States)
- Publication Date:
- Research Org.:
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- Cornell High Energy Synchrotron Source (CHESS); National Science Foundation (NSF); Argonne National Laboratory, Advanced Photon Source
- OSTI Identifier:
- 1572342
- Grant/Contract Number:
- AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Crystals
- Additional Journal Information:
- Journal Volume: 9; Journal Issue: 8; Journal ID: ISSN 2073-4352
- Publisher:
- MDPI
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; CVD diamond; X-ray monochromator; synchrotron radiation
Citation Formats
Stoupin, Stanislav, Krawczyk, Thomas, Liu, Zunping, and Franck, Carl. Selection of CVD Diamond Crystals for X-ray Monochromator Applications Using X-ray Diffraction Imaging. United States: N. p., 2019.
Web. doi:10.3390/cryst9080396.
Stoupin, Stanislav, Krawczyk, Thomas, Liu, Zunping, & Franck, Carl. Selection of CVD Diamond Crystals for X-ray Monochromator Applications Using X-ray Diffraction Imaging. United States. https://doi.org/10.3390/cryst9080396
Stoupin, Stanislav, Krawczyk, Thomas, Liu, Zunping, and Franck, Carl. Wed .
"Selection of CVD Diamond Crystals for X-ray Monochromator Applications Using X-ray Diffraction Imaging". United States. https://doi.org/10.3390/cryst9080396. https://www.osti.gov/servlets/purl/1572342.
@article{osti_1572342,
title = {Selection of CVD Diamond Crystals for X-ray Monochromator Applications Using X-ray Diffraction Imaging},
author = {Stoupin, Stanislav and Krawczyk, Thomas and Liu, Zunping and Franck, Carl},
abstractNote = {A set of 20 single crystal diamond plates synthesized using chemical vapor deposition (CVD) was studied using X-ray diffraction imaging to determine their applicability as side-bounce (single-reflection) Laue monochromators for synchrotron radiation. The crystal plates were of optical grade (as provided by the supplier) with (001) nominal surface orientation. High dislocation density was found for all samples. Distortions in the crystal lattice were quantified for low-index Laue reflections of interests using rocking curve topography. Maps of effective radius of curvature in the scattering plane were calculated using spline interpolation of the rocking curve peak position across the studied plates. For several selected plates, nearly flat regions with large effective radius of curvature were found (R0 ≳ 30 - 70 m, some regions as large as 1 × 4 mm2). The average width of the rocking curve for these regions was found to be about 150 μ rad (r.m.s.). These observations suggest that the selected CVD diamond plates could be used as intermediate-bandwidth monochromators refocusing the radiation source to a specific location downstream with close to 1:1 distance ratio.},
doi = {10.3390/cryst9080396},
journal = {Crystals},
number = 8,
volume = 9,
place = {United States},
year = {Wed Jul 31 00:00:00 EDT 2019},
month = {Wed Jul 31 00:00:00 EDT 2019}
}
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