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Title: Opposed type double stage cell for Mbar pressure experiment with large sample volume

Abstract

We report a new opposed type double-stage large volume cell has been developed to compress large volume samples to more than 100 GPa (Mbar) pressure. A pair of second-stage diamond anvils is introduced into the first-stage Paris-Edinburgh press. The double-stage large volume cell allows the generation of ultrahigh pressures using a large culet diameter of the second-stage diamond anvils (diameters of 0.5-1.2 mm). Pressure generation up to 131 GPa has been achieved by using the culet diameter of 0.5 mm. Sample volume of the double-stage large volume cell can be more than similar to 100 times larger than that of conventional Mbar experiment using a diamond anvil cell. The double-stage large volume cell has a large opening in the horizontal plane for X-ray measurements, which is particularly suited for the multi-angle energy dispersive X-ray diffraction measurement, thus opening a new way of in situ structural determinations of amorphous materials at Mbar pressures.

Authors:
 [1];  [2];  [2]
  1. Carnegie Inst. of Washington, Argonne, IL (United States); Ehime Univ., Matsuyama (Japan)
  2. Argonne National Lab. (ANL), Argonne, IL (United States). High Pressure Collaborative Access Team
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Sponsoring Org.:
USDOE National Nuclear Security Administration (NNSA); National Science Foundation (NSF)
OSTI Identifier:
1607423
Grant/Contract Number:  
AC02-06CH11357; EAR-1722495
Resource Type:
Accepted Manuscript
Journal Name:
High Pressure Research
Additional Journal Information:
Journal Volume: 40; Journal Issue: 1; Journal ID: ISSN 0895-7959
Publisher:
Taylor & Francis
Country of Publication:
United States
Language:
English
Subject:
71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS; Mbar; glass structure; high pressure; large volume

Citation Formats

Kono, Yoshio, Kenney-Benson, Curtis, and Shen, Guoyin. Opposed type double stage cell for Mbar pressure experiment with large sample volume. United States: N. p., 2020. Web. https://doi.org/10.1080/08957959.2019.1710744.
Kono, Yoshio, Kenney-Benson, Curtis, & Shen, Guoyin. Opposed type double stage cell for Mbar pressure experiment with large sample volume. United States. https://doi.org/10.1080/08957959.2019.1710744
Kono, Yoshio, Kenney-Benson, Curtis, and Shen, Guoyin. Wed . "Opposed type double stage cell for Mbar pressure experiment with large sample volume". United States. https://doi.org/10.1080/08957959.2019.1710744. https://www.osti.gov/servlets/purl/1607423.
@article{osti_1607423,
title = {Opposed type double stage cell for Mbar pressure experiment with large sample volume},
author = {Kono, Yoshio and Kenney-Benson, Curtis and Shen, Guoyin},
abstractNote = {We report a new opposed type double-stage large volume cell has been developed to compress large volume samples to more than 100 GPa (Mbar) pressure. A pair of second-stage diamond anvils is introduced into the first-stage Paris-Edinburgh press. The double-stage large volume cell allows the generation of ultrahigh pressures using a large culet diameter of the second-stage diamond anvils (diameters of 0.5-1.2 mm). Pressure generation up to 131 GPa has been achieved by using the culet diameter of 0.5 mm. Sample volume of the double-stage large volume cell can be more than similar to 100 times larger than that of conventional Mbar experiment using a diamond anvil cell. The double-stage large volume cell has a large opening in the horizontal plane for X-ray measurements, which is particularly suited for the multi-angle energy dispersive X-ray diffraction measurement, thus opening a new way of in situ structural determinations of amorphous materials at Mbar pressures.},
doi = {10.1080/08957959.2019.1710744},
journal = {High Pressure Research},
number = 1,
volume = 40,
place = {United States},
year = {2020},
month = {1}
}

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Works referenced in this record:

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