Transient modes of zeolite surface growth from 3D gel-like islands to 2D single layers
Abstract
Zeolite crystallization occurs by multifaceted processes involving molecule attachment and nonclassical pathways governed by the addition of amorphous precursors. Here, we use scanning probe microscopy to monitor zeolite LTA crystallization in situ with a spatiotemporal resolution that captures dynamic processes in real time. We report a distinctive pathway involving the formation of gel-like islands from supersaturated solutions comprised of (alumino)silicate molecules. Three-dimensional assembly and evolution of these islands constitutes a unique mode of growth that differs from classical theories. Time-resolved imaging also reveals that growth can occur by (nearly) oriented attachment. At later stages of crystallization, a progressive transition to lower supersaturation shifts growth to a layered mechanism involving two-dimensional nucleation and spreading of layers. Here, we show that LTA crystallization occurs by multiple pathways, thereby reconciling putative hypotheses of growth mechanisms while also highlighting new modes of nonclassical crystallization that may prove relevant to other zeolites and related materials.
- Authors:
-
- Univ. of Houston, Houston, TX (United States)
- Publication Date:
- Research Org.:
- Univ. of Houston, TX (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1511440
- Grant/Contract Number:
- SC0014468
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Nature Communications
- Additional Journal Information:
- Journal Volume: 9; Journal Issue: 1; Journal ID: ISSN 2041-1723
- Publisher:
- Nature Publishing Group
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Kumar, Manjesh, Choudhary, Madhuresh K., and Rimer, Jeffrey D. Transient modes of zeolite surface growth from 3D gel-like islands to 2D single layers. United States: N. p., 2018.
Web. doi:10.1038/s41467-018-04296-4.
Kumar, Manjesh, Choudhary, Madhuresh K., & Rimer, Jeffrey D. Transient modes of zeolite surface growth from 3D gel-like islands to 2D single layers. United States. https://doi.org/10.1038/s41467-018-04296-4
Kumar, Manjesh, Choudhary, Madhuresh K., and Rimer, Jeffrey D. Tue .
"Transient modes of zeolite surface growth from 3D gel-like islands to 2D single layers". United States. https://doi.org/10.1038/s41467-018-04296-4. https://www.osti.gov/servlets/purl/1511440.
@article{osti_1511440,
title = {Transient modes of zeolite surface growth from 3D gel-like islands to 2D single layers},
author = {Kumar, Manjesh and Choudhary, Madhuresh K. and Rimer, Jeffrey D.},
abstractNote = {Zeolite crystallization occurs by multifaceted processes involving molecule attachment and nonclassical pathways governed by the addition of amorphous precursors. Here, we use scanning probe microscopy to monitor zeolite LTA crystallization in situ with a spatiotemporal resolution that captures dynamic processes in real time. We report a distinctive pathway involving the formation of gel-like islands from supersaturated solutions comprised of (alumino)silicate molecules. Three-dimensional assembly and evolution of these islands constitutes a unique mode of growth that differs from classical theories. Time-resolved imaging also reveals that growth can occur by (nearly) oriented attachment. At later stages of crystallization, a progressive transition to lower supersaturation shifts growth to a layered mechanism involving two-dimensional nucleation and spreading of layers. Here, we show that LTA crystallization occurs by multiple pathways, thereby reconciling putative hypotheses of growth mechanisms while also highlighting new modes of nonclassical crystallization that may prove relevant to other zeolites and related materials.},
doi = {10.1038/s41467-018-04296-4},
journal = {Nature Communications},
number = 1,
volume = 9,
place = {United States},
year = {Tue May 29 00:00:00 EDT 2018},
month = {Tue May 29 00:00:00 EDT 2018}
}
Web of Science
Works referenced in this record:
Direction-Specific Interactions Control Crystal Growth by Oriented Attachment
journal, May 2012
- Li, D.; Nielsen, M. H.; Lee, J. R. I.
- Science, Vol. 336, Issue 6084
Kinetic roughening phenomena, stochastic growth, directed polymers and all that. Aspects of multidisciplinary statistical mechanics
journal, March 1995
- Halpin-Healy, Timothy; Zhang, Yi-Cheng
- Physics Reports, Vol. 254, Issue 4-6
Aggregation-Based Crystal Growth and Microstructure Development in Natural Iron Oxyhydroxide Biomineralization Products
journal, August 2000
- Banfield, J. F.
- Science, Vol. 289, Issue 5480
Mechanism of Zeolite A Nanocrystal Growth from Colloids at Room Temperature
journal, February 1999
- Mintova, S.; Olson, N. H.; Valtchev, V.
- Science, Vol. 283, Issue 5404
Elastically Coupled Two-Level Systems as a Model for Biopolymer Extensibility
journal, November 1998
- Rief, Matthias; Fernandez, Julio M.; Gaub, Hermann E.
- Physical Review Letters, Vol. 81, Issue 21
Formation Pathway for LTA Zeolite Crystals Synthesized via a Charge Density Mismatch Approach
journal, December 2012
- Park, Min Bum; Lee, Yoorim; Zheng, Anmin
- Journal of the American Chemical Society, Vol. 135, Issue 6
Mechanistic principles of nanoparticle evolution to zeolite crystals
journal, April 2006
- Davis, Tracy M.; Drews, Timothy O.; Ramanan, Harikrishnan
- Nature Materials, Vol. 5, Issue 5
Mechanical and chemical unfolding of a single protein: A comparison
journal, March 1999
- Carrion-Vazquez, M.; Oberhauser, A. F.; Fowler, S. B.
- Proceedings of the National Academy of Sciences, Vol. 96, Issue 7
Spontaneous Formation of Silica Nanoparticles in Basic Solutions of Small Tetraalkylammonium Cations
journal, July 2004
- Fedeyko, Joseph M.; Rimer, Jeffrey D.; Lobo, Raul F.
- The Journal of Physical Chemistry B, Vol. 108, Issue 33
Crystallization by particle attachment in synthetic, biogenic, and geologic environments
journal, July 2015
- De Yoreo, J. J.; Gilbert, P. U. P. A.; Sommerdijk, N. A. J. M.
- Science, Vol. 349, Issue 6247
In situ TEM imaging of CaCO3 nucleation reveals coexistence of direct and indirect pathways
journal, September 2014
- Nielsen, M. H.; Aloni, S.; De Yoreo, J. J.
- Science, Vol. 345, Issue 6201
Structure of the Silica Phase Extracted from Silica/(TPA)OH Solutions Containing Nanoparticles
journal, September 2003
- Kragten, David D.; Fedeyko, Joseph M.; Sawant, Kaveri R.
- The Journal of Physical Chemistry B, Vol. 107, Issue 37, p. 10006-10016
Nucleation of FAU and LTA Zeolites from Heterogeneous Aluminosilicate Precursors
journal, July 2016
- Oleksiak, Matthew D.; Soltis, Jennifer A.; Conato, Marlon T.
- Chemistry of Materials, Vol. 28, Issue 14
SSZ-13 Crystallization by Particle Attachment and Deterministic Pathways to Crystal Size Control
journal, September 2015
- Kumar, Manjesh; Luo, Helen; Román-Leshkov, Yuriy
- Journal of the American Chemical Society, Vol. 137, Issue 40
In situ atomic force microscopy of zeolite A dissolution
journal, January 2008
- Itzel Meza, L.; Anderson, Michael W.; Slater, Ben
- Physical Chemistry Chemical Physics, Vol. 10, Issue 33
Kinetic roughening of Kossel and non-Kossel steps
journal, October 2004
- Cuppen, H. M.; Meekes, H.; Enckevort, W. J. P. van
- Surface Science, Vol. 569, Issue 1-3
Covalently functionalized nanotubes as nanometre- sized probes in chemistry and biology
journal, July 1998
- Wong, Stanislaus S.; Joselevich, Ernesto; Woolley, Adam T.
- Nature, Vol. 394, Issue 6688
Investigation of the Crystallization Stages of LTA-Type Zeolite by Complementary Characterization Techniques
journal, December 2003
- Smaihi, Monique; Barida, Olivier; Valtchev, Valentin
- European Journal of Inorganic Chemistry, Vol. 2003, Issue 24
Modeling layered crystal growth at increasing supersaturation by connecting growth regimes
journal, February 2017
- Tilbury, Carl J.; Doherty, Michael F.
- AIChE Journal, Vol. 63, Issue 4
Near-Equilibrium Chemical Force Microscopy
journal, March 2008
- Friddle, Raymond W.; Podsiadlo, Paul; Artyukhin, Alexander B.
- The Journal of Physical Chemistry C, Vol. 112, Issue 13
Electron Microscopy Reveals the Nucleation Mechanism of Zeolite Y from Precursor Colloids
journal, November 1999
- Mintova, Svetlana; Olson, Norman H.; Bein, Thomas
- Angewandte Chemie International Edition, Vol. 38, Issue 21, p. 3201-3204
Nanoscale Control of Homoepitaxial Growth on a Two-Dimensional Zeolite
journal, December 2016
- Shete, Meera; Kumar, Manjesh; Kim, Donghun
- Angewandte Chemie International Edition, Vol. 56, Issue 2
Crystallization in Zeolite A Studied by Atomic Force Microscopy
journal, October 1998
- Agger, Jonathan R.; Pervaiz, Noreen; Cheetham, Anthony K.
- Journal of the American Chemical Society, Vol. 120, Issue 41
Advances in theory and their application within the field of zeolite chemistry
journal, January 2015
- Van Speybroeck, Veronique; Hemelsoet, Karen; Joos, Lennart
- Chemical Society Reviews, Vol. 44, Issue 20
Probing the Relation Between Force—Lifetime—and Chemistry in Single Molecular Bonds
journal, June 2001
- Evans, Evan
- Annual Review of Biophysics and Biomolecular Structure, Vol. 30, Issue 1
In Situ Investigation of Si-TPA-MFI Crystallization Using (Ultra-) Small- and Wide-Angle X-ray Scattering
journal, December 1997
- de Moor, Peter-Paul E. A.; Beelen, Theo P. M.; Komanschek, Bernd U.
- The Journal of Physical Chemistry B, Vol. 101, Issue 51
From molecular to macroscopic via the rational design of a self-assembled 3D DNA crystal
journal, September 2009
- Zheng, Jianping; Birktoft, Jens J.; Chen, Yi
- Nature, Vol. 461, Issue 7260
UV–Raman and NMR Spectroscopic Studies on the Crystallization of Zeolite A and a New Synthetic Route
journal, April 2011
- Ren, Limin; Li, Caijin; Fan, Fengtao
- Chemistry – A European Journal, Vol. 17, Issue 22
Aggregative Growth of Silicalite-1
journal, April 2007
- Kumar, Sandeep; Davis, Tracy M.; Ramanan, Harikrishnan
- The Journal of Physical Chemistry B, Vol. 111, Issue 13
Nanomechanics of lipid bilayers by force spectroscopy with AFM: A perspective
journal, April 2010
- Garcia-Manyes, Sergi; Sanz, Fausto
- Biochimica et Biophysica Acta (BBA) - Biomembranes, Vol. 1798, Issue 4
Functional Group Imaging by Chemical Force Microscopy
journal, September 1994
- Frisbie, C. D.; Rozsnyai, L. F.; Noy, A.
- Science, Vol. 265, Issue 5181
Ion-association complexes unite classical and non-classical theories for the biomimetic nucleation of calcium phosphate
journal, February 2013
- Habraken, Wouter J. E. M.; Tao, Jinhui; Brylka, Laura J.
- Nature Communications, Vol. 4, Issue 1
AFM observation of double 4-rings on zeolite LTA crystals surface
journal, March 1999
- Sugiyama, S.; Yamamoto, S.; Matsuoka, O.
- Microporous and Mesoporous Materials, Vol. 28, Issue 1
Atomistic simulation of zeolite surfaces
journal, October 2001
- Slater, B.; Titiloye, J. O.; Higgins, F. M.
- Current Opinion in Solid State and Materials Science, Vol. 5, Issue 5
Reversible Unfolding of Individual Titin Immunoglobulin Domains by AFM
journal, May 1997
- Rief, M.
- Science, Vol. 276, Issue 5315
In situ observation of the growth of silicalite nuclei by small-angle X-ray and neutron scattering
journal, January 1996
- Watson, Jonathan N.; Iton, Lennox E.; White, John W.
- Chemical Communications, Issue 24
AFM and HRSEM Invesitigation of Zeolite A Crystal Growth. Part 1: In the Absence of Organic Additives
journal, June 2011
- Cubillas, Pablo; Stevens, Sam M.; Blake, Nicola
- The Journal of Physical Chemistry C, Vol. 115, Issue 25
Fully Copper-Exchanged High-Silica LTA Zeolites as Unrivaled Hydrothermally Stable NH 3 -SCR Catalysts
journal, January 2017
- Ryu, Taekyung; Ahn, Nak Ho; Seo, Seungwan
- Angewandte Chemie International Edition, Vol. 56, Issue 12
Effects of silicon sources on the formation of nanosized LTA: An in situ small angle X-ray scattering and wide angle X-ray scattering study
journal, April 2007
- Fan, Wei; Meneau, Florian; Bras, Wim
- Microporous and Mesoporous Materials, Vol. 101, Issue 1-2
Real-Time Imaging of Pt3Fe Nanorod Growth in Solution
journal, May 2012
- Liao, H. -G.; Cui, L.; Whitelam, S.
- Science, Vol. 336, Issue 6084
In Situ Imaging of Silicalite-1 Surface Growth Reveals the Mechanism of Crystallization
journal, May 2014
- Lupulescu, A. I.; Rimer, J. D.
- Science, Vol. 344, Issue 6185
Dynamic force spectroscopy of single DNA molecules
journal, September 1999
- Strunz, T.; Oroszlan, K.; Schafer, R.
- Proceedings of the National Academy of Sciences, Vol. 96, Issue 20
Modeling the Nucleation of Zeolite A
journal, November 2013
- Yang, Chao-Shiang; Mora-Fonz, José Miguel; Catlow, C. Richard A.
- The Journal of Physical Chemistry C, Vol. 117, Issue 47
Adhesion Forces between E. c oli Bacteria and Biomaterial Surfaces
journal, April 1999
- Ong, Yea-Ling; Razatos, Anneta; Georgiou, George
- Langmuir, Vol. 15, Issue 8
Interpreting the widespread nonlinear force spectra of intermolecular bonds
journal, August 2012
- Friddle, R. W.; Noy, A.; De Yoreo, J. J.
- Proceedings of the National Academy of Sciences, Vol. 109, Issue 34
Chemical Force Microscopy
journal, August 1997
- Noy, Aleksandr; Vezenov, Dmitri V.; Lieber, Charles M.
- Annual Review of Materials Science, Vol. 27, Issue 1
Controlling Crystal Polymorphism in Organic-Free Synthesis of Na-Zeolites
journal, January 2013
- Maldonado, Miguel; Oleksiak, Matthew D.; Chinta, Sivadinarayana
- Journal of the American Chemical Society, Vol. 135, Issue 7
Using the Atomic Force Microscope to Study the Interaction between Two Solid Supported Lipid Bilayers and the Influence of Synapsin I
journal, October 2004
- Pera, Ioana; Stark, Rüdiger; Kappl, Michael
- Biophysical Journal, Vol. 87, Issue 4
Investigation of the surface structure of zeolite A
journal, January 2005
- Wakihara, Toru; Sasaki, Yukichi; Kato, Hitoshi
- Physical Chemistry Chemical Physics, Vol. 7, Issue 19
Nanomechanics of Lipid Bilayers: Heads or Tails?
journal, September 2010
- Garcia-Manyes, Sergi; Redondo-Morata, Lorena; Oncins, Gerard
- Journal of the American Chemical Society, Vol. 132, Issue 37
Evidences for Zeolite Nucleation at the Solid−Liquid Interface of Gel Cavities
journal, November 2005
- Valtchev, Valentin P.; Bozhilov, Krassimir N.
- Journal of the American Chemical Society, Vol. 127, Issue 46, p. 16171-16177
Entropic Barriers in Nanoscale Adhesion Studied by Variable Temperature Chemical Force Microscopy
journal, February 2003
- Noy, Aleksandr; Zepeda, Salvador; Orme, Christine A.
- Journal of the American Chemical Society, Vol. 125, Issue 5
Methods for in situ spectroscopic probing of the synthesis of a zeolite
journal, January 2010
- Aerts, Alexander; Kirschhock, Christine E. A.; Martens, Johan A.
- Chemical Society Reviews, Vol. 39, Issue 12
Cell and molecular mechanics of biological materials
journal, November 2003
- Bao, G.; Suresh, S.
- Nature Materials, Vol. 2, Issue 11
Force measurements with the atomic force microscope: Technique, interpretation and applications
journal, October 2005
- Butt, Hans-Jürgen; Cappella, Brunero; Kappl, Michael
- Surface Science Reports, Vol. 59, Issue 1-6
Practical single molecule force spectroscopy: How to determine fundamental thermodynamic parameters of intermolecular bonds with an atomic force microscope
journal, April 2013
- Noy, Aleksandr; Friddle, Raymond W.
- Methods, Vol. 60, Issue 2
Stretching Single Talin Rod Molecules Activates Vinculin Binding
journal, January 2009
- del Rio, A.; Perez-Jimenez, R.; Liu, R.
- Science, Vol. 323, Issue 5914
Evolution of Self-Assembled Silica−Tetrapropylammonium Nanoparticles at Elevated Temperatures
journal, July 2005
- Rimer, Jeffrey D.; Vlachos, Dionisios G.; Lobo, Raul F.
- The Journal of Physical Chemistry B, Vol. 109, Issue 26
Mechanism on solvent-free crystallization of NaA zeolite
journal, January 2017
- Xiao, Yuchen; Sheng, Na; Chu, Yueying
- Microporous and Mesoporous Materials, Vol. 237
Supramolecular self-assembled molecules as organic directing agent for synthesis of zeolites
journal, September 2004
- Corma, Avelino; Rey, Fernando; Rius, Jordi
- Nature, Vol. 431, Issue 7006
Direct Visualization of Surfactant Hemimicelles by Force Microscopy of the Electrical Double Layer
journal, December 1994
- Manne, S.; Cleveland, J. P.; Gaub, H. E.
- Langmuir, Vol. 10, Issue 12
Combined NMR, SAXS, and DLS Study of Concentrated Clear Solutions Used in Silicalite-1 Zeolite Synthesis
journal, July 2007
- Aerts, Alexander; Follens, Lana R. A.; Haouas, Mohamed
- Chemistry of Materials, Vol. 19, Issue 14
In situ observation of homogeneous nucleation of nanosized zeolite A
journal, January 2006
- Fan, Wei; O’Brien, Matthew; Ogura, Masaru
- Physical Chemistry Chemical Physics, Vol. 8, Issue 11
Single-Molecule Determination of the Face-Specific Adsorption of Amelogenin’s C-Terminus on Hydroxyapatite
journal, June 2011
- Friddle, Raymond W.; Battle, Keith; Trubetskoy, Vasily
- Angewandte Chemie International Edition, Vol. 50, Issue 33
Unusual Pathway of Crystallization of Zeolite ZSM-5 in a Heterogeneous System: Phenomenology and Starting Considerations
journal, May 2012
- Ren, Nan; Subotić, Boris; Bronić, Josip
- Chemistry of Materials, Vol. 24, Issue 10
Comparison of Techniques for Measuring the Electrical Double Layer Properties of Surfaces in Aqueous Solution: Hexadecyltrimethylammonium Bromide Self-Assembly Structures as a Model System
journal, July 1995
- Johnson, Stephen B.; Drummond, Calum J.; Scales, Peter J.
- Langmuir, Vol. 11, Issue 7
Chemical force microscopy of chemical and biological interactions
journal, January 2006
- Noy, Aleksandr
- Surface and Interface Analysis, Vol. 38, Issue 11
Platinum-based nanocages with subnanometer-thick walls and well-defined, controllable facets
journal, July 2015
- Zhang, L.; Roling, L. T.; Wang, X.
- Science, Vol. 349, Issue 6246
Fully Copper-Exchanged High-Silica LTA Zeolites as Unrivaled Hydrothermally Stable NH 3 -SCR Catalysts
journal, January 2017
- Ryu, Taekyung; Ahn, Nak Ho; Seo, Seungwan
- Angewandte Chemie, Vol. 129, Issue 12
Nanoscale Control of Homoepitaxial Growth on a Two-Dimensional Zeolite
journal, December 2016
- Shete, Meera; Kumar, Manjesh; Kim, Donghun
- Angewandte Chemie, Vol. 129, Issue 2
Supramolecular Self-Assembled Molecules as Organic Directing Agent for Synthesis of Zeolites.
journal, November 2004
- Corma, Avelino; Rey, Fernando; Rius, Jordi
- ChemInform, Vol. 35, Issue 47
Chemical Force Microscopy
journal, August 1997
- Lieber, Charles M.; Vezenov, Dmitri; Noy, Aleksandr
- Microscopy and Microanalysis, Vol. 3, Issue S2
Seeing crystal formation one particle at a time
journal, March 2020
- Han, Yilong
- Nature Materials, Vol. 19, Issue 4
Nanomechanics of Lipid Bilayers: Heads or Tails?
journal, January 2010
- Garcia-Manyes, Sergi; Oncins, Gerard; Redondo, Lorena
- Biophysical Journal, Vol. 98, Issue 3
Modeling layered crystal growth at increasing supersaturation by connecting growth regimes
journal, February 2017
- Tilbury, Carl J.; Doherty, Michael F.
- AIChE Journal, Vol. 63, Issue 4
Single-Molecule Determination of the Face-Specific Adsorption of Amelogenin’s C-Terminus on Hydroxyapatite
journal, June 2011
- Friddle, Raymond W.; Battle, Keith; Trubetskoy, Vasily
- Angewandte Chemie International Edition, Vol. 50, Issue 33
UV–Raman and NMR Spectroscopic Studies on the Crystallization of Zeolite A and a New Synthetic Route
journal, April 2011
- Ren, Limin; Li, Caijin; Fan, Fengtao
- Chemistry – A European Journal, Vol. 17, Issue 22
Effects of silicon sources on the formation of nanosized LTA: An in situ small angle X-ray scattering and wide angle X-ray scattering study
journal, April 2007
- Fan, Wei; Meneau, Florian; Bras, Wim
- Microporous and Mesoporous Materials, Vol. 101, Issue 1-2
Mechanism on solvent-free crystallization of NaA zeolite
journal, January 2017
- Xiao, Yuchen; Sheng, Na; Chu, Yueying
- Microporous and Mesoporous Materials, Vol. 237
Practical single molecule force spectroscopy: How to determine fundamental thermodynamic parameters of intermolecular bonds with an atomic force microscope
journal, April 2013
- Noy, Aleksandr; Friddle, Raymond W.
- Methods, Vol. 60, Issue 2
Imaging of crystal growth-induced fine surface features in zeolite A by atomic force microscopy
journal, July 2002
- Dumrul, Seyda; Bazzana, Stephane; Warzywoda, Juliusz
- Microporous and Mesoporous Materials, Vol. 54, Issue 1-2
Combined NMR, SAXS, and DLS Study of Concentrated Clear Solutions Used in Silicalite-1 Zeolite Synthesis
journal, July 2007
- Aerts, Alexander; Follens, Lana R. A.; Haouas, Mohamed
- Chemistry of Materials, Vol. 19, Issue 14
Entropic Barriers in Nanoscale Adhesion Studied by Variable Temperature Chemical Force Microscopy
journal, February 2003
- Noy, Aleksandr; Zepeda, Salvador; Orme, Christine A.
- Journal of the American Chemical Society, Vol. 125, Issue 5
Evidences for Zeolite Nucleation at the Solid−Liquid Interface of Gel Cavities
journal, November 2005
- Valtchev, Valentin P.; Bozhilov, Krassimir N.
- Journal of the American Chemical Society, Vol. 127, Issue 46, p. 16171-16177
Nanomechanics of Lipid Bilayers: Heads or Tails?
journal, September 2010
- Garcia-Manyes, Sergi; Redondo-Morata, Lorena; Oncins, Gerard
- Journal of the American Chemical Society, Vol. 132, Issue 37
Controlling Crystal Polymorphism in Organic-Free Synthesis of Na-Zeolites
journal, January 2013
- Maldonado, Miguel; Oleksiak, Matthew D.; Chinta, Sivadinarayana
- Journal of the American Chemical Society, Vol. 135, Issue 7
Crystallization in Zeolite A Studied by Atomic Force Microscopy
journal, October 1998
- Agger, Jonathan R.; Pervaiz, Noreen; Cheetham, Anthony K.
- Journal of the American Chemical Society, Vol. 120, Issue 41
SSZ-13 Crystallization by Particle Attachment and Deterministic Pathways to Crystal Size Control
journal, September 2015
- Kumar, Manjesh; Luo, Helen; Román-Leshkov, Yuriy
- Journal of the American Chemical Society, Vol. 137, Issue 40
Structure of the Silica Phase Extracted from Silica/(TPA)OH Solutions Containing Nanoparticles
journal, September 2003
- Kragten, David D.; Fedeyko, Joseph M.; Sawant, Kaveri R.
- The Journal of Physical Chemistry B, Vol. 107, Issue 37, p. 10006-10016
Spontaneous Formation of Silica Nanoparticles in Basic Solutions of Small Tetraalkylammonium Cations
journal, July 2004
- Fedeyko, Joseph M.; Rimer, Jeffrey D.; Lobo, Raul F.
- The Journal of Physical Chemistry B, Vol. 108, Issue 33
Evolution of Self-Assembled Silica−Tetrapropylammonium Nanoparticles at Elevated Temperatures
journal, July 2005
- Rimer, Jeffrey D.; Vlachos, Dionisios G.; Lobo, Raul F.
- The Journal of Physical Chemistry B, Vol. 109, Issue 26
Aggregative Growth of Silicalite-1
journal, April 2007
- Kumar, Sandeep; Davis, Tracy M.; Ramanan, Harikrishnan
- The Journal of Physical Chemistry B, Vol. 111, Issue 13
Modeling the Nucleation of Zeolite A
journal, November 2013
- Yang, Chao-Shiang; Mora-Fonz, José Miguel; Catlow, C. Richard A.
- The Journal of Physical Chemistry C, Vol. 117, Issue 47
Near-Equilibrium Chemical Force Microscopy
journal, March 2008
- Friddle, Raymond W.; Podsiadlo, Paul; Artyukhin, Alexander B.
- The Journal of Physical Chemistry C, Vol. 112, Issue 13
Comparison of Techniques for Measuring the Electrical Double Layer Properties of Surfaces in Aqueous Solution: Hexadecyltrimethylammonium Bromide Self-Assembly Structures as a Model System
journal, July 1995
- Johnson, Stephen B.; Drummond, Calum J.; Scales, Peter J.
- Langmuir, Vol. 11, Issue 7
Direct Visualization of Surfactant Hemimicelles by Force Microscopy of the Electrical Double Layer
journal, December 1994
- Manne, S.; Cleveland, J. P.; Gaub, H. E.
- Langmuir, Vol. 10, Issue 12
Adhesion Forces between E. c oli Bacteria and Biomaterial Surfaces
journal, April 1999
- Ong, Yea-Ling; Razatos, Anneta; Georgiou, George
- Langmuir, Vol. 15, Issue 8
Supramolecular self-assembled molecules as organic directing agent for synthesis of zeolites
journal, September 2004
- Corma, Avelino; Rey, Fernando; Rius, Jordi
- Nature, Vol. 431, Issue 7006
From molecular to macroscopic via the rational design of a self-assembled 3D DNA crystal
journal, September 2009
- Zheng, Jianping; Birktoft, Jens J.; Chen, Yi
- Nature, Vol. 461, Issue 7260
Cell and molecular mechanics of biological materials
journal, November 2003
- Bao, G.; Suresh, S.
- Nature Materials, Vol. 2, Issue 11
Mechanistic principles of nanoparticle evolution to zeolite crystals
journal, April 2006
- Davis, Tracy M.; Drews, Timothy O.; Ramanan, Harikrishnan
- Nature Materials, Vol. 5, Issue 5
In situ observation of homogeneous nucleation of nanosized zeolite A
journal, January 2006
- Fan, Wei; O’Brien, Matthew; Ogura, Masaru
- Physical Chemistry Chemical Physics, Vol. 8, Issue 11
Methods for in situ spectroscopic probing of the synthesis of a zeolite
journal, January 2010
- Aerts, Alexander; Kirschhock, Christine E. A.; Martens, Johan A.
- Chemical Society Reviews, Vol. 39, Issue 12
Dynamic force spectroscopy of single DNA molecules
journal, September 1999
- Strunz, T.; Oroszlan, K.; Schafer, R.
- Proceedings of the National Academy of Sciences, Vol. 96, Issue 20
Stretching Single Talin Rod Molecules Activates Vinculin Binding
journal, January 2009
- del Rio, A.; Perez-Jimenez, R.; Liu, R.
- Science, Vol. 323, Issue 5914
Real-Time Imaging of Pt3Fe Nanorod Growth in Solution
journal, May 2012
- Liao, H. -G.; Cui, L.; Whitelam, S.
- Science, Vol. 336, Issue 6084
In situ TEM imaging of CaCO3 nucleation reveals coexistence of direct and indirect pathways
journal, September 2014
- Nielsen, M. H.; Aloni, S.; De Yoreo, J. J.
- Science, Vol. 345, Issue 6201
Functional Group Imaging by Chemical Force Microscopy
journal, September 1994
- Frisbie, C. D.; Rozsnyai, L. F.; Noy, A.
- Science, Vol. 265, Issue 5181
Reversible Unfolding of Individual Titin Immunoglobulin Domains by AFM
journal, May 1997
- Rief, M.
- Science, Vol. 276, Issue 5315
Aggregation-Based Crystal Growth and Microstructure Development in Natural Iron Oxyhydroxide Biomineralization Products
journal, August 2000
- Banfield, J. F.
- Science, Vol. 289, Issue 5480
Probing the Relation Between Force—Lifetime—and Chemistry in Single Molecular Bonds
journal, June 2001
- Evans, Evan
- Annual Review of Biophysics and Biomolecular Structure, Vol. 30, Issue 1
Chemical Force Microscopy
journal, August 1997
- Noy, Aleksandr; Vezenov, Dmitri V.; Lieber, Charles M.
- Annual Review of Materials Science, Vol. 27, Issue 1
Using the Atomic Force Microscope to Study the Interaction between Two Solid Supported Lipid Bilayers and the Influence of Synapsin I
journal, October 2004
- Pera, Ioana; Stark, Rüdiger; Kappl, Michael
- Biophysical Journal, Vol. 87, Issue 4
Works referencing / citing this record:
Bridging the Gap between Structurally Distinct 2D Lamellar Zeolitic Precursors through a 3D Germanosilicate Intermediate
journal, September 2019
- Xu, Le; Choudhary, Madhuresh K.; Muraoka, Koki
- Angewandte Chemie, Vol. 131, Issue 41
Regulating Nonclassical Pathways of Silicalite‐1 Crystallization through Controlled Evolution of Amorphous Precursors
journal, September 2019
- Choudhary, Madhuresh K.; Kumar, Manjesh; Rimer, Jeffrey D.
- Angewandte Chemie, Vol. 131, Issue 44
Uniformly Oriented Zeolite ZSM-5 Membranes with Tunable Wettability on a Porous Ceramic
journal, August 2018
- Fu, Donglong; Schmidt, Joel E.; Pletcher, Paul
- Angewandte Chemie International Edition, Vol. 57, Issue 38
Bridging the Gap between Structurally Distinct 2D Lamellar Zeolitic Precursors through a 3D Germanosilicate Intermediate
journal, September 2019
- Xu, Le; Choudhary, Madhuresh K.; Muraoka, Koki
- Angewandte Chemie International Edition, Vol. 58, Issue 41
Regulating Nonclassical Pathways of Silicalite‐1 Crystallization through Controlled Evolution of Amorphous Precursors
journal, September 2019
- Choudhary, Madhuresh K.; Kumar, Manjesh; Rimer, Jeffrey D.
- Angewandte Chemie International Edition, Vol. 58, Issue 44
Organic‐Free Interzeolite Transformation in the Absence of Common Building Units
journal, March 2019
- Qin, Wei; Jain, Rishabh; Robles Hernández, Francisco C.
- Chemistry – A European Journal, Vol. 25, Issue 23
Time‐Resolved Dynamics of Struvite Crystallization: Insights from the Macroscopic to Molecular Scale
journal, March 2020
- Kim, Doyoung; Olympiou, Chara; McCoy, Colin P.
- Chemistry – A European Journal, Vol. 26, Issue 16
Organic Mesopore Generating Agents (OMeGAs) for Hierarchical Zeolites: Combining Functions on Multiple Scales
journal, May 2019
- Hong, Mei; Dong, Lei; Yang, Shihe
- ChemNanoMat, Vol. 5, Issue 7
A zeolite supramolecular framework with LTA topology based on a tetrahedral metal–organic cage
journal, January 2019
- Zhang, Hai-Xia; Yan, Xiaodong; Chen, Yu-Xin
- Chemical Communications, Vol. 55, Issue 8
A phase-transfer crystallization pathway to synthesize ultrasmall silicoaluminophosphate for enhanced catalytic conversion of dimethylether-to-olefin
journal, January 2019
- Ding, Hongxin; Ding, Jiajia; Liu, Wei
- CrystEngComm, Vol. 21, Issue 4
Interface engineered surface morphology evolution of Au@Pd core–shell nanorods
journal, January 2018
- Xu, Yanchao; Cui, Xiaoqiang; Qi, Kun
- Nanoscale, Vol. 10, Issue 45
Influence of alkalinity on the synthesis of hierarchical LTA zeolite by using bridged polysilsesquioxane
journal, January 2019
- Hu, Sufang; Song, Guoqiang; Xue, Da
- RSC Advances, Vol. 9, Issue 5
Tracking the rearrangement of atomic configurations during the conversion of FAU zeolite to CHA zeolite
journal, January 2019
- Muraoka, Koki; Sada, Yuki; Shimojima, Atsushi
- Chemical Science, Vol. 10, Issue 37
A new kind of atlas of zeolite building blocks
journal, October 2019
- Helfrecht, Benjamin A.; Semino, Rocio; Pireddu, Giovanni
- The Journal of Chemical Physics, Vol. 151, Issue 15
Nuclear Magnetic Resonance Spectroscopy for In Situ Monitoring of Porous Materials Formation under Hydrothermal Conditions
journal, August 2018
- Haouas, Mohamed
- Materials, Vol. 11, Issue 8
Uniformly Oriented Zeolite ZSM-5 Membranes with Tunable Wettability on a Porous Ceramic
journal, August 2018
- Fu, Donglong; Schmidt, Joel E.; Pletcher, Paul
- Angewandte Chemie, Vol. 130, Issue 38
Cover Feature: Time‐Resolved Dynamics of Struvite Crystallization: Insights from the Macroscopic to Molecular Scale (Chem. Eur. J. 16/2020)
journal, March 2020
- Kim, Doyoung; Olympiou, Chara; McCoy, Colin P.
- Chemistry – A European Journal, Vol. 26, Issue 16
Uniformly Oriented Zeolite ZSM-5 Membranes with Tunable Wettability on a Porous Ceramic
journal, August 2018
- Fu, Donglong; Schmidt, Joel E.; Pletcher, Paul
- Angewandte Chemie International Edition, Vol. 57, Issue 38
Nuclear Magnetic Resonance Spectroscopy for In Situ Monitoring of Porous Materials Formation under Hydrothermal Conditions
journal, August 2018
- Haouas, Mohamed
- Materials, Vol. 11, Issue 8