Transient modes of zeolite surface growth from 3D gel-like islands to 2D single layers
Abstract
Zeolite crystallization occurs by multifaceted processes involving molecule attachment and nonclassical pathways governed by the addition of amorphous precursors. Here, we use scanning probe microscopy to monitor zeolite LTA crystallization in situ with a spatiotemporal resolution that captures dynamic processes in real time. We report a distinctive pathway involving the formation of gel-like islands from supersaturated solutions comprised of (alumino)silicate molecules. Three-dimensional assembly and evolution of these islands constitutes a unique mode of growth that differs from classical theories. Time-resolved imaging also reveals that growth can occur by (nearly) oriented attachment. At later stages of crystallization, a progressive transition to lower supersaturation shifts growth to a layered mechanism involving two-dimensional nucleation and spreading of layers. Here, we show that LTA crystallization occurs by multiple pathways, thereby reconciling putative hypotheses of growth mechanisms while also highlighting new modes of nonclassical crystallization that may prove relevant to other zeolites and related materials.
- Publication Date:
- Research Org.:
- Univ. of Houston, TX (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1511440
- Grant/Contract Number:
- SC0014468
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Nature Communications
- Additional Journal Information:
- Journal Volume: 9; Journal Issue: 1; Journal ID: ISSN 2041-1723
- Publisher:
- Nature Publishing Group
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Kumar, Manjesh, Choudhary, Madhuresh K., and Rimer, Jeffrey D. Transient modes of zeolite surface growth from 3D gel-like islands to 2D single layers. United States: N. p., 2018.
Web. doi:10.1038/s41467-018-04296-4.
Kumar, Manjesh, Choudhary, Madhuresh K., & Rimer, Jeffrey D. Transient modes of zeolite surface growth from 3D gel-like islands to 2D single layers. United States. https://doi.org/10.1038/s41467-018-04296-4
Kumar, Manjesh, Choudhary, Madhuresh K., and Rimer, Jeffrey D. Tue .
"Transient modes of zeolite surface growth from 3D gel-like islands to 2D single layers". United States. https://doi.org/10.1038/s41467-018-04296-4. https://www.osti.gov/servlets/purl/1511440.
@article{osti_1511440,
title = {Transient modes of zeolite surface growth from 3D gel-like islands to 2D single layers},
author = {Kumar, Manjesh and Choudhary, Madhuresh K. and Rimer, Jeffrey D.},
abstractNote = {Zeolite crystallization occurs by multifaceted processes involving molecule attachment and nonclassical pathways governed by the addition of amorphous precursors. Here, we use scanning probe microscopy to monitor zeolite LTA crystallization in situ with a spatiotemporal resolution that captures dynamic processes in real time. We report a distinctive pathway involving the formation of gel-like islands from supersaturated solutions comprised of (alumino)silicate molecules. Three-dimensional assembly and evolution of these islands constitutes a unique mode of growth that differs from classical theories. Time-resolved imaging also reveals that growth can occur by (nearly) oriented attachment. At later stages of crystallization, a progressive transition to lower supersaturation shifts growth to a layered mechanism involving two-dimensional nucleation and spreading of layers. Here, we show that LTA crystallization occurs by multiple pathways, thereby reconciling putative hypotheses of growth mechanisms while also highlighting new modes of nonclassical crystallization that may prove relevant to other zeolites and related materials.},
doi = {10.1038/s41467-018-04296-4},
journal = {Nature Communications},
number = 1,
volume = 9,
place = {United States},
year = {Tue May 29 00:00:00 EDT 2018},
month = {Tue May 29 00:00:00 EDT 2018}
}
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journal, September 2015
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Structure of the Silica Phase Extracted from Silica/(TPA)OH Solutions Containing Nanoparticles
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Comparison of Techniques for Measuring the Electrical Double Layer Properties of Surfaces in Aqueous Solution: Hexadecyltrimethylammonium Bromide Self-Assembly Structures as a Model System
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Direct Visualization of Surfactant Hemimicelles by Force Microscopy of the Electrical Double Layer
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Adhesion Forces between E. c oli Bacteria and Biomaterial Surfaces
journal, April 1999
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Supramolecular self-assembled molecules as organic directing agent for synthesis of zeolites
journal, September 2004
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From molecular to macroscopic via the rational design of a self-assembled 3D DNA crystal
journal, September 2009
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Cell and molecular mechanics of biological materials
journal, November 2003
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Mechanistic principles of nanoparticle evolution to zeolite crystals
journal, April 2006
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In situ observation of homogeneous nucleation of nanosized zeolite A
journal, January 2006
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Methods for in situ spectroscopic probing of the synthesis of a zeolite
journal, January 2010
- Aerts, Alexander; Kirschhock, Christine E. A.; Martens, Johan A.
- Chemical Society Reviews, Vol. 39, Issue 12
Dynamic force spectroscopy of single DNA molecules
journal, September 1999
- Strunz, T.; Oroszlan, K.; Schafer, R.
- Proceedings of the National Academy of Sciences, Vol. 96, Issue 20
Stretching Single Talin Rod Molecules Activates Vinculin Binding
journal, January 2009
- del Rio, A.; Perez-Jimenez, R.; Liu, R.
- Science, Vol. 323, Issue 5914
Real-Time Imaging of Pt3Fe Nanorod Growth in Solution
journal, May 2012
- Liao, H. -G.; Cui, L.; Whitelam, S.
- Science, Vol. 336, Issue 6084
In situ TEM imaging of CaCO3 nucleation reveals coexistence of direct and indirect pathways
journal, September 2014
- Nielsen, M. H.; Aloni, S.; De Yoreo, J. J.
- Science, Vol. 345, Issue 6201
Functional Group Imaging by Chemical Force Microscopy
journal, September 1994
- Frisbie, C. D.; Rozsnyai, L. F.; Noy, A.
- Science, Vol. 265, Issue 5181
Reversible Unfolding of Individual Titin Immunoglobulin Domains by AFM
journal, May 1997
- Rief, M.
- Science, Vol. 276, Issue 5315
Aggregation-Based Crystal Growth and Microstructure Development in Natural Iron Oxyhydroxide Biomineralization Products
journal, August 2000
- Banfield, J. F.
- Science, Vol. 289, Issue 5480
Probing the Relation Between Force—Lifetime—and Chemistry in Single Molecular Bonds
journal, June 2001
- Evans, Evan
- Annual Review of Biophysics and Biomolecular Structure, Vol. 30, Issue 1
Chemical Force Microscopy
journal, August 1997
- Noy, Aleksandr; Vezenov, Dmitri V.; Lieber, Charles M.
- Annual Review of Materials Science, Vol. 27, Issue 1
Using the Atomic Force Microscope to Study the Interaction between Two Solid Supported Lipid Bilayers and the Influence of Synapsin I
journal, October 2004
- Pera, Ioana; Stark, Rüdiger; Kappl, Michael
- Biophysical Journal, Vol. 87, Issue 4
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