Suppression of the commensurate magnetic phase in nanosized hübnerite MnWO4

Zajdel, P.; G?gor, A.; Pajerowski, D. M.; Ptak, M.; Szlawska, M.

doi:10.1103/PhysRevB.95.174427

Title: Suppression of the commensurate magnetic phase in nanosized hübnerite $MnW O_{4}$

Abstract

Magnetic structures of nanosized (20 to 70 nm) powders of MnWO₄ and MnWO₄:Mo were studied using neutron powder diffraction (NPD). Sizes and shapes of the crystallites calculated from anisotropic peak broadening of diffraction peaks were found to be orthogonal parallelepipedlike with the longest edge along the c axis and the shortest along the b axis. SQUID measurements indicate the presence of two magnetic transitions around 8 and 12 K. Rietveld refinement of the NPD data below the magnetic transition was consistent with the presence of an incommensurate spiral-like (ac-AF2) phase. Finally, a commensurate phase AF1 was not observed down to 2.5 K for all of the samples.

Authors:

Zajdel, P. ^[1]; G?gor, A. ^[2]; Pajerowski, D. M. ^[3]; Ptak, M. ^[2]; Szlawska, M. ^[2]

Univ. of Silesia, Katowice (Poland). Inst. of Physics
Polish Academy of Sciences (PAS), Warsaw (Poland). Inst. of Low Temperature and Structure Research
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Quantum Condensed Matter Division

Publication Date:: Thu May 18 00:00:00 EDT 2017

Research Org.:: Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE; National Institute of Standards and Technology (NIST); Polish State Committee for Scientific Research

OSTI Identifier:: 1430608

Grant/Contract Number:: AC05-00OR22725

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review B

Additional Journal Information:: Journal Volume: 95; Journal Issue: 17; Journal ID: ISSN 2469-9950

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY

Citation Formats


                    Zajdel, P., G?gor, A., Pajerowski, D. M., Ptak, M., and Szlawska, M. Suppression of the commensurate magnetic phase in nanosized hübnerite MnWO4.  United States: N. p., 2017. 
Web.  doi:10.1103/PhysRevB.95.174427.

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                    Zajdel, P., G?gor, A., Pajerowski, D. M., Ptak, M., & Szlawska, M. Suppression of the commensurate magnetic phase in nanosized hübnerite MnWO4.  United States.  https://doi.org/10.1103/PhysRevB.95.174427

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                    Zajdel, P., G?gor, A., Pajerowski, D. M., Ptak, M., and Szlawska, M. Thu .  
"Suppression of the commensurate magnetic phase in nanosized hübnerite MnWO4".  United States.  https://doi.org/10.1103/PhysRevB.95.174427.  https://www.osti.gov/servlets/purl/1430608.

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@article{osti_1430608,

  title        = {Suppression of the commensurate magnetic phase in nanosized hübnerite MnWO4},

  author       = {Zajdel, P. and G?gor, A. and Pajerowski, D. M. and Ptak, M. and Szlawska, M.},

  abstractNote = {Magnetic structures of nanosized (20 to 70 nm) powders of MnWO4 and MnWO4:Mo were studied using neutron powder diffraction (NPD). Sizes and shapes of the crystallites calculated from anisotropic peak broadening of diffraction peaks were found to be orthogonal parallelepipedlike with the longest edge along the c axis and the shortest along the b axis. SQUID measurements indicate the presence of two magnetic transitions around 8 and 12 K. Rietveld refinement of the NPD data below the magnetic transition was consistent with the presence of an incommensurate spiral-like (ac-AF2) phase. Finally, a commensurate phase AF1 was not observed down to 2.5 K for all of the samples.},

  doi          = {10.1103/PhysRevB.95.174427},

  journal      = {Physical Review B},

  number       = 17,

  volume       = 95,

  place        = {United States},

  year         = {Thu May 18 00:00:00 EDT 2017},

  month        = {Thu May 18 00:00:00 EDT 2017}

}

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Title: Suppression of the commensurate magnetic phase in nanosized hübnerite MnW O 4

Abstract

Citation Formats

Suppression and recovery of the ferroelectric phase in multiferroic Mn W O 4 journal, March 2008

Magnetic control of ferroelectric polarization journal, November 2003

DAVE: A Comprehensive Software Suite for the Reduction, Visualization, and Analysis of Low Energy Neutron Spectroscopic Data journal, November 2009

Polarized-neutron-scattering studies on the chiral magnetism in multiferroic MnWO 4 journal, February 2010

Magnetic-field dependence of the ferroelectric polarization and spin-lattice coupling in multiferroic Mn W O 4 journal, February 2008

Origin of multiferroicity in MnWO 4 journal, April 2013

Electric field control of ferroelectric domain structures in MnWO 4 journal, July 2014

Control of the Magnetoelectric Domain-Wall Stability by a Magnetic Field in a Multiferroic MnWO 4 journal, November 2008

Phonon properties of nanosized MnWO4 with different size and morphology journal, September 2011

Polyol-mediated low-temperature synthesis of crystalline tungstate nanoparticles MWO4 (M = Mn, Fe, Co, Ni, Cu, Zn) journal, May 2014

Revised effective ionic radii and systematic studies of interatomic distances in halides and chalcogenides journal, September 1976

Application of symmetrized harmonics expansion to correction of the preferred orientation effect journal, August 1993

Magnetic phase transitions of MnWO 4 studied by the use of neutron diffraction journal, September 1993

A new polar symmetry of huebnerite (MnWO4) with ferrodistortive domains journal, November 2015

Spherical neutron polarimetry (SNP) study of magneto-electric coupling in the multiferroic MnWO 4 journal, January 2009

Phase transitions and magnetic structures in MnW 1− x Mo x O 4 compounds ( x ⩽ 0.2) journal, June 2016

Domain dynamics in the multiferroic phase of MnWO 4 journal, April 2014

Phenomenological model of anisotropic peak broadening in powder diffraction journal, April 1999

VESTA 3 for three-dimensional visualization of crystal, volumetric and morphology data journal, October 2011

Ferroelectricity in the cycloidal spiral magnetic phase of Mn W O 4 journal, November 2006

A new multiferroic material: MnWO 4 journal, September 2006

Increasing the Phase-Transition Temperatures in Spin-Frustrated Multiferroic MnWO 4 by Mo Doping journal, December 2011

Local symmetry and magnetic anisotropy in multiferroic MnWO 4 and antiferromagnetic CoWO 4 studied by soft x-ray absorption spectroscopy journal, November 2010

A new protocol for the determination of magnetic structures using simulated annealing and representational analysis (SARAh) journal, March 2000

Phonon and magnetic properties of nanocrystalline MnWO4 prepared by hydrothermal method journal, January 2012

Magnetic structure of manganesetungstate MnWO4 at 4.2°K journal, September 1966

Rietveld refinement of Debye–Scherrer synchrotron X-ray data from Al 2 O 3 journal, April 1987

Ultrafine MnWO4 nanoparticles and their magnetic properties journal, August 2015

Incommensurate magnetic structures of multiferroic MnWO 4 studied within the superspace formalism journal, January 2013

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A profile refinement method for nuclear and magnetic structures journal, June 1969

Long-range magnetic interactions in the multiferroic antiferromagnet MnWO 4 journal, April 2011

Spin Current and Magnetoelectric Effect in Noncollinear Magnets journal, July 2005

Correlation between ferroelectric polarization and sense of helical spin order in multiferroic MnWO 4 journal, June 2008

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Title: Suppression of the commensurate magnetic phase in nanosized hübnerite $MnW O_{4}$

Suppression and recovery of the ferroelectric phase in multiferroic $Mn W O_{4}$
journal, March 2008

Magnetic control of ferroelectric polarization
journal, November 2003

DAVE: A Comprehensive Software Suite for the Reduction, Visualization, and Analysis of Low Energy Neutron Spectroscopic Data
journal, November 2009

Polarized-neutron-scattering studies on the chiral magnetism in multiferroic MnWO ₄
journal, February 2010

Magnetic-field dependence of the ferroelectric polarization and spin-lattice coupling in multiferroic $Mn W O_{4}$
journal, February 2008

Origin of multiferroicity in MnWO $_{4}$
journal, April 2013

Electric field control of ferroelectric domain structures in MnWO ₄
journal, July 2014

Control of the Magnetoelectric Domain-Wall Stability by a Magnetic Field in a Multiferroic ${MnWO}_{4}$
journal, November 2008

Phonon properties of nanosized MnWO4 with different size and morphology
journal, September 2011

Polyol-mediated low-temperature synthesis of crystalline tungstate nanoparticles MWO4 (M = Mn, Fe, Co, Ni, Cu, Zn)
journal, May 2014

Revised effective ionic radii and systematic studies of interatomic distances in halides and chalcogenides
journal, September 1976

Application of symmetrized harmonics expansion to correction of the preferred orientation effect
journal, August 1993

Magnetic phase transitions of ${MnWO}_{4}$ studied by the use of neutron diffraction
journal, September 1993

A new polar symmetry of huebnerite (MnWO4) with ferrodistortive domains
journal, November 2015

Spherical neutron polarimetry (SNP) study of magneto-electric coupling in the multiferroic MnWO ₄
journal, January 2009

Phase transitions and magnetic structures in MnW _{1− x} Mo _x O ₄ compounds ( x ⩽ 0.2)
journal, June 2016

Domain dynamics in the multiferroic phase of ${MnWO}_{4}$
journal, April 2014

Phenomenological model of anisotropic peak broadening in powder diffraction
journal, April 1999

VESTA 3 for three-dimensional visualization of crystal, volumetric and morphology data
journal, October 2011

Ferroelectricity in the cycloidal spiral magnetic phase of $Mn W O_{4}$
journal, November 2006

A new multiferroic material: MnWO ₄
journal, September 2006

Increasing the Phase-Transition Temperatures in Spin-Frustrated Multiferroic MnWO ₄ by Mo Doping
journal, December 2011

Local symmetry and magnetic anisotropy in multiferroic ${MnWO}_{4}$ and antiferromagnetic ${CoWO}_{4}$ studied by soft x-ray absorption spectroscopy
journal, November 2010

A new protocol for the determination of magnetic structures using simulated annealing and representational analysis (SARAh)
journal, March 2000

Phonon and magnetic properties of nanocrystalline MnWO4 prepared by hydrothermal method
journal, January 2012

Magnetic structure of manganesetungstate MnWO4 at 4.2°K
journal, September 1966

Rietveld refinement of Debye–Scherrer synchrotron X-ray data from Al ₂ O ₃
journal, April 1987

Ultrafine MnWO4 nanoparticles and their magnetic properties
journal, August 2015

Incommensurate magnetic structures of multiferroic MnWO $_{4}$ studied within the superspace formalism
journal, January 2013

Morphology control of MnWO4 nanocrystals by a solvothermal route
journal, March 2003

A profile refinement method for nuclear and magnetic structures
journal, June 1969

Long-range magnetic interactions in the multiferroic antiferromagnet MnWO $_{4}$
journal, April 2011

Spin Current and Magnetoelectric Effect in Noncollinear Magnets
journal, July 2005

Correlation between ferroelectric polarization and sense of helical spin order in multiferroic ${MnWO}_{4}$
journal, June 2008

Ion doping effects in multiferroic MnWO ₄
journal, April 2012