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Title: Mechanical properties of metal-ceramic nanolaminates: Effect of constraint and temperature

Abstract

Al/SiC nanolaminates with equal nominal thicknesses of the Al and SiC layers (10, 25, 50 and 100 nm) were manufactured by magnetron sputtering. The mechanical properties were measured at 25 °C and 100 °C by means of nanoindentation and micropillar compression tests and the deformation mechanisms were analyzed by in situ micropillar compression tests in the transmission electron microscope. In addition, finite element simulations of both tests were carried out to ascertain the role played by the strength of the Al layers and by the elastic constraint of the ceramic layers on the plastic flow of Al in the mechanical response. It was found that the mechanical response was mainly controlled by the constraint during nanoindentation or micropillar compression tests of very thin layered (≈10 nm) laminates, while the influence of the strength of Al layers was not as critical. This behavior was reversed, however, for thick layered laminates (100 nm). Here, these mechanisms point to the different effects of layer thickness during nanoindentation and micropillar compression, at both temperatures, and showed the critical role played by constraint on the mechanical response of nanolaminates made of materials with a very large difference in the elasto-plastic properties.

Authors:
 [1];  [2]; ORCiD logo [3]; ORCiD logo [3]; ORCiD logo [3];  [2]; ORCiD logo [4];  [1]
  1. IMDEA Materials Institute, Madrid (Spain); Polytechnic Univ. of Madrid/Univ. Politecnica de Madrid, Madrid (Spain)
  2. Arizona State Univ., Tempe, AZ (United States)
  3. Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
  4. IMDEA Materials Institute, Madrid (Spain)
Publication Date:
Research Org.:
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
OSTI Identifier:
1417175
Alternate Identifier(s):
OSTI ID: 1495895
Report Number(s):
LA-UR-17-28798
Journal ID: ISSN 1359-6454; TRN: US1801004
Grant/Contract Number:  
AC52-06NA25396
Resource Type:
Accepted Manuscript
Journal Name:
Acta Materialia
Additional Journal Information:
Journal Volume: 142; Journal Issue: C; Journal ID: ISSN 1359-6454
Publisher:
Elsevier
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; Micropillar compression; Nanoindentation; Composites; Nanolaminates

Citation Formats

Yang, Ling Wei, Mayer, Carl, Li, Nan, Baldwin, Jon Kevin Scott, Mara, Nathan Allan, Chawla, Nikhilesh, Molina-Aldareguia, Jon M., and Llorca, Javier. Mechanical properties of metal-ceramic nanolaminates: Effect of constraint and temperature. United States: N. p., 2017. Web. doi:10.1016/j.actamat.2017.09.042.
Yang, Ling Wei, Mayer, Carl, Li, Nan, Baldwin, Jon Kevin Scott, Mara, Nathan Allan, Chawla, Nikhilesh, Molina-Aldareguia, Jon M., & Llorca, Javier. Mechanical properties of metal-ceramic nanolaminates: Effect of constraint and temperature. United States. https://doi.org/10.1016/j.actamat.2017.09.042
Yang, Ling Wei, Mayer, Carl, Li, Nan, Baldwin, Jon Kevin Scott, Mara, Nathan Allan, Chawla, Nikhilesh, Molina-Aldareguia, Jon M., and Llorca, Javier. Thu . "Mechanical properties of metal-ceramic nanolaminates: Effect of constraint and temperature". United States. https://doi.org/10.1016/j.actamat.2017.09.042. https://www.osti.gov/servlets/purl/1417175.
@article{osti_1417175,
title = {Mechanical properties of metal-ceramic nanolaminates: Effect of constraint and temperature},
author = {Yang, Ling Wei and Mayer, Carl and Li, Nan and Baldwin, Jon Kevin Scott and Mara, Nathan Allan and Chawla, Nikhilesh and Molina-Aldareguia, Jon M. and Llorca, Javier},
abstractNote = {Al/SiC nanolaminates with equal nominal thicknesses of the Al and SiC layers (10, 25, 50 and 100 nm) were manufactured by magnetron sputtering. The mechanical properties were measured at 25 °C and 100 °C by means of nanoindentation and micropillar compression tests and the deformation mechanisms were analyzed by in situ micropillar compression tests in the transmission electron microscope. In addition, finite element simulations of both tests were carried out to ascertain the role played by the strength of the Al layers and by the elastic constraint of the ceramic layers on the plastic flow of Al in the mechanical response. It was found that the mechanical response was mainly controlled by the constraint during nanoindentation or micropillar compression tests of very thin layered (≈10 nm) laminates, while the influence of the strength of Al layers was not as critical. This behavior was reversed, however, for thick layered laminates (100 nm). Here, these mechanisms point to the different effects of layer thickness during nanoindentation and micropillar compression, at both temperatures, and showed the critical role played by constraint on the mechanical response of nanolaminates made of materials with a very large difference in the elasto-plastic properties.},
doi = {10.1016/j.actamat.2017.09.042},
journal = {Acta Materialia},
number = C,
volume = 142,
place = {United States},
year = {Thu Sep 21 00:00:00 EDT 2017},
month = {Thu Sep 21 00:00:00 EDT 2017}
}

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Works referenced in this record:

Metal Matrix Composites
journal, June 2010


An analysis of the effects of matrix void growth on deformation and ductility in metal-ceramic composites
journal, October 1991


Influence of matrix strength on reinforcement fracture and ductility in AlAl2O3 composites
journal, September 1994


Effects of heat treatment and reinforcement size
journal, November 1993

  • Singh, Preet M.; Lewandowski, John J.
  • Metallurgical Transactions A, Vol. 24, Issue 11
  • DOI: 10.1007/BF02646532

Indentation mechanics and fracture behavior of metal/ceramic nanolaminate composites
journal, July 2008


High-temperature nanoindentation behavior of Al/SiC multilayers
journal, August 2012


High temperature micropillar compression of Al/SiC nanolaminates
journal, July 2013


Effect of layer thickness on the high temperature mechanical properties of Al/SiC nanolaminates
journal, November 2014


Anisotropy, size, and aspect ratio effects on micropillar compression of Al SiC nanolaminate composites
journal, August 2016


Deformation mechanisms of ultra-thin Al layers in Al/SiC nanolaminates as a function of thickness and temperature
journal, August 2016


Indentation Fracture Response of Al–TiN Nanolaminates
journal, February 2013


In situ Nanoindentation Study of Plastic Co-deformation in Al-TiN Nanocomposites
journal, October 2014

  • Li, N.; Wang, H.; Misra, A.
  • Scientific Reports, Vol. 4, Issue 1
  • DOI: 10.1038/srep06633

On the origins of hardness of Cu–TiN nanolayered composites
journal, December 2015


Compressive flow behavior of Al–TiN multilayers at nanometer scale layer thickness
journal, June 2011


Optimum high temperature strength of two-dimensional nanocomposites
journal, November 2013

  • Monclús, M. A.; Zheng, S. J.; Mayeur, J. R.
  • APL Materials, Vol. 1, Issue 5
  • DOI: 10.1063/1.4828757

An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments
journal, June 1992

  • Oliver, W. C.; Pharr, G. M.
  • Journal of Materials Research, Vol. 7, Issue 06, p. 1564-1583
  • DOI: 10.1557/JMR.1992.1564

The relation between load and penetration in the axisymmetric boussinesq problem for a punch of arbitrary profile
journal, May 1965


Characterization of nanoindentation damage in metal/ceramic multilayered films by transmission electron microscopy (TEM)
journal, May 2010


An indentation-based method to determine constituent strengths within nanolayered composites
journal, June 2015


Works referencing / citing this record:

Effects of Sample and Indenter Configurations of Nanoindentation Experiment on the Mechanical Behavior and Properties of Ductile Materials
journal, June 2018

  • Rahimian Koloor, Seyed; Karimzadeh, Atefeh; Tamin, Mohd
  • Metals, Vol. 8, Issue 6
  • DOI: 10.3390/met8060421