Method for the synthesis of metal cyanometallates
Abstract
Methods are presented for synthesizing metal cyanometallate (MCM). A first method provides a first solution of AXM2Y(CN)Z, to which a second solution including M1 is dropwise added. As a result, a precipitate is formed of ANM1PM2Q(CN)R.FH2O, where N is in the range of 1 to 4. A second method for synthesizing MCM provides a first solution of M2C(CN)B, which is dropwise added to a second solution including M1. As a result, a precipitate is formed of M1[M2S(CN)G]1/T. DH2O, where S/T is greater than or equal to 0.8. Low vacancy MCM materials are also presented.
- Inventors:
- Issue Date:
- Research Org.:
- Sharp Labs of America, Inc., Camas, WA (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1531956
- Patent Number(s):
- 9484578
- Application Number:
- 14/289,746
- Assignee:
- Sharp Laboratories of America, Inc. (Camas, WA)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01C - AMMONIA
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- DOE Contract Number:
- AR0000297
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 2014-05-29
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 25 ENERGY STORAGE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Lu, Yuhao, Wang, Long, Vail, Sean, and Lee, Jong-Jan. Method for the synthesis of metal cyanometallates. United States: N. p., 2016.
Web.
Lu, Yuhao, Wang, Long, Vail, Sean, & Lee, Jong-Jan. Method for the synthesis of metal cyanometallates. United States.
Lu, Yuhao, Wang, Long, Vail, Sean, and Lee, Jong-Jan. Tue .
"Method for the synthesis of metal cyanometallates". United States. https://www.osti.gov/servlets/purl/1531956.
@article{osti_1531956,
title = {Method for the synthesis of metal cyanometallates},
author = {Lu, Yuhao and Wang, Long and Vail, Sean and Lee, Jong-Jan},
abstractNote = {Methods are presented for synthesizing metal cyanometallate (MCM). A first method provides a first solution of AXM2Y(CN)Z, to which a second solution including M1 is dropwise added. As a result, a precipitate is formed of ANM1PM2Q(CN)R.FH2O, where N is in the range of 1 to 4. A second method for synthesizing MCM provides a first solution of M2C(CN)B, which is dropwise added to a second solution including M1. As a result, a precipitate is formed of M1[M2S(CN)G]1/T. DH2O, where S/T is greater than or equal to 0.8. Low vacancy MCM materials are also presented.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Nov 01 00:00:00 EDT 2016},
month = {Tue Nov 01 00:00:00 EDT 2016}
}
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Works referenced in this record:
High Rate, Long Cycle Life Battery Electrode Materials With An Open Framework Structure
patent-application, December 2012
- Wessells, Colin; Huggins, Robert; Cui, Yi
- US Patent Application 13/482793; 20120328936