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Title: Metal cyanometallate synthesis method

Abstract

A method is provided for synthesizing metal cyanometallate (MCM). The method provides a solution of AXM1Y(CN)Z; where “A” is selected from a first group of metals and M1 is selected from a second group of metals. The method adds a material including M2 to the solution to form a liquid phase material that may be either a suspension or a solution. M2 is selected from the second group of metals. The method adds acid to the liquid phase material. The addition of acid to the liquid phase material decomposes the M2 material into M2-ions. Simultaneous with the addition of the acid, a precipitate of ANM1PM2Q(CN)R.FH2O is formed, where N is in a range of 1 to 2. A variation of the above-described synthesis method is also provided.

Inventors:
; ;
Issue Date:
Research Org.:
Univ. of Texas, Austin, TX (United States); Sharp Labs. of America, Inc., Camas, WA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1532012
Patent Number(s):
9745202
Application Number:
14/731,607
Assignee:
Board of Regents, The University of Texas System (Austin, TX); Sharp Laboratories of America, Inc. (Camas, WA)
Patent Classifications (CPCs):
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01C - AMMONIA
Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
DOE Contract Number:  
AR0000297
Resource Type:
Patent
Resource Relation:
Patent File Date: 2015-06-05
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats

Song, Jie, Lu, Yuhao, and Wang, Long. Metal cyanometallate synthesis method. United States: N. p., 2017. Web.
Song, Jie, Lu, Yuhao, & Wang, Long. Metal cyanometallate synthesis method. United States.
Song, Jie, Lu, Yuhao, and Wang, Long. Tue . "Metal cyanometallate synthesis method". United States. https://www.osti.gov/servlets/purl/1532012.
@article{osti_1532012,
title = {Metal cyanometallate synthesis method},
author = {Song, Jie and Lu, Yuhao and Wang, Long},
abstractNote = {A method is provided for synthesizing metal cyanometallate (MCM). The method provides a solution of AXM1Y(CN)Z; where “A” is selected from a first group of metals and M1 is selected from a second group of metals. The method adds a material including M2 to the solution to form a liquid phase material that may be either a suspension or a solution. M2 is selected from the second group of metals. The method adds acid to the liquid phase material. The addition of acid to the liquid phase material decomposes the M2 material into M2-ions. Simultaneous with the addition of the acid, a precipitate of ANM1PM2Q(CN)R.FH2O is formed, where N is in a range of 1 to 2. A variation of the above-described synthesis method is also provided.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2017},
month = {8}
}

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