Magnetite (Fe3O4)—multiwalled carbon nanotube composite structures with performance as high rate electrode materials for Li-ion batteries

Wong, Stanislaus; Wang, Lei; McBean, Coray; Marschilok, Amy C.; Takeuchi, Kenneth; Takeuchi, Esther S.

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Title: Magnetite (Fe₃O₄)—multiwalled carbon nanotube composite structures with performance as high rate electrode materials for Li-ion batteries

Abstract

A method of synthesizing an electrode material for lithium ion batteries from Fe₃O₄ nanoparticles and multiwalled carbon nanotubes (MWNTs) to yield (Fe₃O₄-NWNTs) composite heterostructures. The method includes linking the Fe₃O₄ nanoparticles and multiwalled carbon nanotubes using a π-π interaction synthesis process to yield the composite heterostructure electrode material. Since Fe₃O₄ has an intermediate voltage, it can be considered an anode (when paired with a higher voltage material) or a cathode (when paired with a lower voltage material).

Inventors:: Wong, Stanislaus; Wang, Lei; McBean, Coray; Marschilok, Amy C.; Takeuchi, Kenneth; Takeuchi, Esther S.

Issue Date:: Tue May 31 00:00:00 EDT 2022

Research Org.:: Stony Brook Univ., NY (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1892998

Patent Number(s):: 11349117

Application Number:: 16/250,838

Assignee:: The Research Foundation of State University of New York (Albany, NY)

Patent Classifications (CPCs):: C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F

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C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B32/174 - Derivatisation

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
C01G49/08 - Ferroso-ferric oxide

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
C01P2002/82 - by IR- or Raman-data
C01P2004/04 - obtained by TEM, STEM, STM or AFM
C01P2004/64 - Nanometer sized, i.e. from 1-100 nanometer
C01P2004/80 - Particles consisting of a mixture of two or more inorganic phases

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M10/0525 - Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes
H01M2004/021 - {Physical characteristics, e.g. porosity, surface area}
H01M2004/027 - {Negative electrodes}
H01M4/13 - Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators
H01M4/139 - Processes of manufacture
H01M4/364 - {as mixtures}
H01M4/366 - {as layered products}
H01M4/485 - of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
H01M4/523 - {for non-aqueous cells
H01M4/587 - for inserting or intercalating light metals
H01M4/624 - {Electric conductive fillers}
H01M4/625 - {Carbon or graphite}

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/10 - Energy storage

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DOE Contract Number:: SC0012673

Resource Type:: Patent

Resource Relation:: Patent File Date: 01/17/2019

Country of Publication:: United States

Language:: English

Citation Formats


                    Wong, Stanislaus, Wang, Lei, McBean, Coray, Marschilok, Amy C., Takeuchi, Kenneth, and Takeuchi, Esther S. Magnetite (Fe3O4)—multiwalled carbon nanotube composite structures with performance as high rate electrode materials for Li-ion batteries.  United States: N. p., 2022. 
        Web.

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                    Wong, Stanislaus, Wang, Lei, McBean, Coray, Marschilok, Amy C., Takeuchi, Kenneth, & Takeuchi, Esther S. Magnetite (Fe3O4)—multiwalled carbon nanotube composite structures with performance as high rate electrode materials for Li-ion batteries.  United States.

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                    Wong, Stanislaus, Wang, Lei, McBean, Coray, Marschilok, Amy C., Takeuchi, Kenneth, and Takeuchi, Esther S. Tue .  
        "Magnetite (Fe3O4)—multiwalled carbon nanotube composite structures with performance as high rate electrode materials for Li-ion batteries".  United States.  https://www.osti.gov/servlets/purl/1892998.

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@article{osti_1892998,

  title        = {Magnetite (Fe3O4)—multiwalled carbon nanotube composite structures with performance as high rate electrode materials for Li-ion batteries},

  author       = {Wong, Stanislaus and Wang, Lei and McBean, Coray and Marschilok, Amy C. and Takeuchi, Kenneth and Takeuchi, Esther S.},

  abstractNote = {A method of synthesizing an electrode material for lithium ion batteries from Fe3O4 nanoparticles and multiwalled carbon nanotubes (MWNTs) to yield (Fe3O4-NWNTs) composite heterostructures. The method includes linking the Fe3O4 nanoparticles and multiwalled carbon nanotubes using a π-π interaction synthesis process to yield the composite heterostructure electrode material. Since Fe3O4 has an intermediate voltage, it can be considered an anode (when paired with a higher voltage material) or a cathode (when paired with a lower voltage material).},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue May 31 00:00:00 EDT 2022},

  month        = {Tue May 31 00:00:00 EDT 2022}

}

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Title: Magnetite (Fe3O4)—multiwalled carbon nanotube composite structures with performance as high rate electrode materials for Li-ion batteries

Abstract

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Title: Magnetite (Fe₃O₄)—multiwalled carbon nanotube composite structures with performance as high rate electrode materials for Li-ion batteries

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Graphene foam-protected metal fluoride and metal chloride cathode active materials for lithium batteries
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Hybrid materials and nanocomposite materials, methods of making same, and uses thereof
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Methods for making graphene-supported metal oxide monolith
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Method of making carbon nanotubes doped with iron, nitrogen and sulphur
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Conductive nanocomposite-based electrodes for lithium batteries
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Composite electrode active material, lithium battery including the same, and method of preparing the composite electrode active material
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Electrode, related material, process for production, and use thereof
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Encapsulated phthalocyanine particles, high-capacity cathode containing these particles, and rechargeable lithium cell containing such a cathode
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Monolithic electrode, related material, process for production, and use thereof
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Method of fabricating electrodes including high-capacity, binder-free anodes for lithium-ion batteries
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Method of fabricating metal oxide film
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Internal hybrid electrochemical energy storage cell having both high power and high energy density
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Electrosynthesis of nanofibers and nano-composite films
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Process for producing hybrid nano-filament electrodes for lithium batteries
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Nanoarchitectured multi-component electrode materials and methods of making the same
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Nanocomposite of graphene and metal oxide materials
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Strongly coupled inorganic-graphene hybrid materials, apparatuses, systems and methods
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Carbon material supported hollow metal oxide nanoparticles, methods and applications
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Anode materials for lithium-ion batteries
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Nitride and carbide anode materials
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Layered high capacity electrodes
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Nanofibrous electrocatalyst including nanofibrous continuous network of graphitic nanofibers having embedded catalytically active metal moieties
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Sodium iron(II)-hexacyanoferrate(II) battery electrode and synthesis method
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Lithium ion-based internal hybrid electrochemical energy storage cell
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Method of manufacture of an electrode material and an electrode material
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Mixed nano-filament electrode materials for lithium ion batteries
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Lithium ion batteries with titania/graphene anodes
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Correlating Preparative Approaches with Electrochemical Performance of Fe ₃ O ₄ -MWNT Composites Used as Anodes in Li-Ion Batteries
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Graphene-enabled metal fluoride and metal chloride cathode active materials for lithium batteries
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Porous Fe3O4/S composites for Li/S batteries
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Hollow nanoparticle cathode materials for sodium electrochemical cells and batteries
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Coating of porous carbon for use in lithium air batteries
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Nanoscale intercalation materials on carbon powder, process for production, and use thereof
patent, December 2013

Carbon encapsulated transition metal oxide nanocomposite, a method for its preparation and its use in li-ion batteries
patent, July 2016