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The Ion-Exchange Separation of Zirconium and Hafnium

Technical Report ·
DOI:https://doi.org/10.2172/929690· OSTI ID:929690

In the course of a rather cursory examination of the elution of tetra-positive ions from the cation exchange resin Dowex 50 with hydrochloric acid solutions, the authors have discovered a very effective method of separating zirconium from hafnimu. In view of the great labor involved in preparing even reasonably pure hafnium compounds by existing methods, they feel that this procedure will prove very valuable to those interested in obtaining hafnium compounds free of zirconium. Although the conditions which give satisfactory separation were first worked out using microgram amounts of material and the radioactive tracer technique, the run described here, involving milligrams of material, illustrates the applicability of the method to the production of significant amounts of pure hafnium and zirconium.

Research Organization:
Ernest Orlando Lawrence Berkeley NationalLaboratory, Berkeley, CA (US)
Sponsoring Organization:
USAEC
DOE Contract Number:
AC02-05CH11231
OSTI ID:
929690
Report Number(s):
UCRL--191; AECD-2435
Country of Publication:
United States
Language:
English

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