Silver behenate as a calibration standard of grazing-incidence small-angle X-ray scattering

Journal Article · Tue Sep 12 00:00:00 EDT 2006 · Journal of Applied Crystallography

DOI:https://doi.org/10.1107/S0021889806031244· OSTI ID:898681

Lee, Byeongdu; Lo, Chieh-Tsung; Seifert, Soenke; Winans, Randall E.

Grazing-incidence small-angle X-ray scattering (GISAXS) patterns of a silver behenate composite film, which has a typical layered structure, are described. The peak position of the film in the GISAXS pattern was varied depending on the incident angle, which was well described by taking into account the refraction and the reflection effects. Since the refractive index of samples depends on sample preparation, it is recommended that the measurement of silver behenate as a standard be done in conventional transmission mode to avoid any complexity.

• Research Organization: Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
• Sponsoring Organization: USDOE
• DOE Contract Number: DE-AC02-06CH11357
• OSTI ID: 898681
• Journal Information: Journal of Applied Crystallography, Vol. 39, Issue 5; ISSN 0021-8898
• Publisher: International Union of Crystallography
• Country of Publication: United States
• Language: English

Related Subjects

37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
CALIBRATION STANDARDS
SMALL ANGLE SCATTERING
X-RAY DIFFRACTION
SILVER COMPOUNDS
CARBOXYLIC ACID SALTS
advanced photon source