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Title: Task Technical and Quality Assurance Plan for the Characterization of Tank 25F Saltcake Core Samples

Technical Report ·
DOI:https://doi.org/10.2172/890226· OSTI ID:890226

The Department of Energy (DOE) recognizes the need for the characterization of High-Level Waste (HLW) saltcake in the Savannah River Site (SRS) F- and H-area tank farms to support upcoming salt processing activities. As part of the enhanced characterization efforts, Tank 25F will be sampled and the samples analyzed at the Savannah River National Laboratory (SRNL). This Task Technical and Quality Assurance Plan documents the planned activities for the physical, chemical, and radiological analysis of the Tank 25F saltcake core samples. This plan does not cover other characterization activities that do not involve core sample analysis and it does not address issues regarding sampling or sample transportation. The objectives of this report are: (1) Provide information useful in projecting the composition of dissolved salt batches by quantifying important components (such as actinides, {sup 137}Cs, and {sup 90}Sr) on a per batch basis. This will assist in process selection for the treatment of salt batches and provide data for the validation of dissolution modeling. (2) Determine the properties of the heel resulting from dissolution of the bulk saltcake. Also note tendencies toward post-mixing precipitation. (3) Provide a basis for determining the number of samples needed for the characterization of future saltcake tanks. Gather information useful towards performing characterization in a manner that is more cost and time effective.

Research Organization:
Savannah River Site (SRS), Aiken, SC (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
DE-AC09-96SR18500
OSTI ID:
890226
Report Number(s):
WSRC-RP-2004-00513-Rev1; TRN: US0604631
Country of Publication:
United States
Language:
English