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Reduction of outgassing rate by glow discharge cleaning

Journal Article · · Journal of Vacuum Science Technology A
OSTI ID:801734

The effectiveness of glow discharge cleaning (GDC) as a means of decreasing the pump-down time of vacuum systems was studied. We measured the outgassing rate of an electropolished stainless steel surface after it was exposed to glow discharges fueled by various gases (He, He/1%-3%H{sub 2}, He/1%-3%CH{sub 4}, H{sub 2}, Ar) following a standard 1 h of venting to ambient air. It is shown that He GDC is most effective in reduction of outgassing rate: a He GDC trial with a dose of 0.8 C/cm{sub 2} reduces the outgassing rate and subsequently the pump-down time by a factor of 13. For given glow discharge currents, the outgassing reduction factor is directly proportional to the glow discharge duration. The reduction of post-GDC outgassing is a result of enhanced desorption of H{sub 2}, CO, and CO{sub 2} by He GDC as observed by residual gas analysis during the discharge. The GDC results are consistent with our previously proposed diffusion models for water outgassing from metal surfaces.

Research Organization:
Thomas Jefferson National Accelerator Facility, Newport News, VA (US)
Sponsoring Organization:
USDOE Office of Energy Research (ER) (US)
DOE Contract Number:
AC05-84ER40150
OSTI ID:
801734
Report Number(s):
CEBAF-PR-94-010; DOE/ER/40150-2219
Journal Information:
Journal of Vacuum Science Technology A, Journal Name: Journal of Vacuum Science Technology A Vol. 13
Country of Publication:
United States
Language:
English

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