In-Situ Chemical Dynamics and Phase Mapping Under Steep Thermal Gradients Using Time-Resolved and Spatially Resolved X-Ray Diffraction

Wong, J; Larson, E M; Holt, J B; Ressler, T; Elmer, J W

doi:10.1007/978-1-4615-1205-9_22

Title: In-Situ Chemical Dynamics and Phase Mapping Under Steep Thermal Gradients Using Time-Resolved and Spatially Resolved X-Ray Diffraction

Conference · Fri Sep 17 00:00:00 EDT 1999

DOI:https://doi.org/10.1007/978-1-4615-1205-9_22· OSTI ID:791390

Wong, J; Larson, E M; Holt, J B; Ressler, T; Elmer, J W

Time-resolved and spatially-resolved diffraction techniques have been developed recently to perform materials dynamics study in-situ extending into the time and spatial domain in high temperature processes. The applications of these methods to investigate the chemical dynamics of solid combustion reactions and to map phases and their transformation in fusion welds are exemplified in this paper.

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Research Organization:: Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE Office of Defense Programs (DP) (US)

DOE Contract Number:: W-7405-Eng-48

OSTI ID:: 791390

Report Number(s):: UCRL-JC-136132; TRN: US200206%%34

Resource Relation:: Conference: International Alloys Conference-2, Davos (CH), 08/08/1999--08/13/1999; Other Information: PBD: 17 Sep 1999

Country of Publication:: United States

Language:: English

References (9)

Combustion synthesis of the YBa2Cu3O7−x superconductor Lebrat, Jean-Pascal; Varma, Arvind Physica C: Superconductivity, Vol. 184, Issue 4-6 https://doi.org/10.1016/0921-4534(91)90386-D	journal	December 1991
Real-time probe of reaction centers in solid combustions on the subsecond time scale Frahm, R.; Wong, Joe; Holt, J. B. Physical Review B, Vol. 46, Issue 14 https://doi.org/10.1103/PhysRevB.46.9205	journal	October 1992
Spatially resolved X-ray diffraction phase mapping and α → β → α transformation kinetics in the heat-affected zone of commercially pure titanium arc welds Elmer, John W.; Wong, Joe; Ressler, Thorsten Metallurgical and Materials Transactions A, Vol. 29, Issue 11 https://doi.org/10.1007/s11661-998-0317-5	journal	November 1998
Time-Resolved X-ray Diffraction Study of Solid Combustion Reactions Wong, J.; Larson, E. M.; Holt, J. B. Science, Vol. 249, Issue 4975 https://doi.org/10.1126/science.249.4975.1406	journal	September 1990
Analysis of heat-affected zone phase transformations usingin situ spatially resolved x-ray diffraction with synchrotron radiation Elmer, J. W.; Wong, Joe; Fröba, M. Metallurgical and Materials Transactions A, Vol. 27, Issue 3 https://doi.org/10.1007/BF02648965	journal	March 1996
Beamline 10: A multipole wiggler beamline at SSRL (invited) Karpenko, V.; Kinney, J. H.; Kulkarni, S. Review of Scientific Instruments, Vol. 60, Issue 7 https://doi.org/10.1063/1.1140961	journal	July 1989
Self-propagating exothermic reactions: The synthesis of high-temperature materials by combustion Munir, Zuhair A.; Anselmi-Tamburini, Umberto Materials Science Reports, Vol. 3, Issue 7-8 https://doi.org/10.1016/0920-2307(89)90001-7	journal	May 1989
Investigation of Real-Time Microstructure Evolution in Steep Thermal Gradients Using in-Situ Spatially Resolved X-ray Diffraction: A Case Study for Ti Fusion Welds Ressler, Thorsten; Wong, Joe; Elmer, John W. The Journal of Physical Chemistry B, Vol. 102, Issue 52 https://doi.org/10.1021/jp983045j	journal	December 1998
High‐speed diffractometer‐reaction chamber using synchrotron radiation Larson, E. M.; Waide, P. A.; Wong, Joe Review of Scientific Instruments, Vol. 62, Issue 1 https://doi.org/10.1063/1.1142281	journal	January 1991

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Related Subjects

37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
36 MATERIALS SCIENCE
ALLOYS
COMBUSTION KINETICS
TEMPERATURE GRADIENTS
PHASE TRANSFORMATIONS
X-RAY DIFFRACTION
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Title: In-Situ Chemical Dynamics and Phase Mapping Under Steep Thermal Gradients Using Time-Resolved and Spatially Resolved X-Ray Diffraction

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References (9)

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