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Mechanical and environmental factors in the cyclic and static fatigue of silicon nitride

Journal Article · · Journal of the American Ceramic Society; (United States)
;  [1]
  1. Univ. of Michigan, Ann Arbor, MI (United States). Dept. of Materials Science and Engineering
The effects of environment on cyclic and static fatigue behavior were investigated with hot-pressed silicon nitride materials. Tests were conducted at ambient temperature on standard compact tension specimens, and a dc electric potential technique was used to monitor crack lengths in situ. The results indicate that the environmental sensitivity of the materials under both cyclic and static loading mirrors that of durable glasses in static fatigue. The materials were most sensitive to water in the environment, while changes in pH had no significant effect in the range tested. In addition, NH[sub 3] was much less reactive with the material than with vitreous SiO[sub 2]. In some cases, the intergranular glass appears to be the site of environmental interaction. Evidence was also found that cyclic fatigue is not simply a manifestation of static fatigue. Cyclic fatigue was seen to occur in the absence of measurable static fatigue, and the data indicate that the mechanism of cyclic fatigue involves damage to the crack wake shielding zone.
OSTI ID:
7303153
Journal Information:
Journal of the American Ceramic Society; (United States), Journal Name: Journal of the American Ceramic Society; (United States) Vol. 77:5; ISSN 0002-7820; ISSN JACTAW
Country of Publication:
United States
Language:
English