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Title: Plugging micro-leaks in multi-component, ceramic tubesheets with material leached therefrom

Patent ·
OSTI ID:7250598

Cracks, in ceramic wall members, on the order of 1 micron or less in width are plugged helium-tight by selectively leaching a component of the wall member with a solvent, letting the resultant leach form a liquid bridge within the crack, removing the solvent and sintering the resultant residue. This method is of particular value for remedying microcracks or channels in a cell member constituting a tubesheet in a hollow fiber type, high temperature battery cell, such as a sodium/sulfur cell, for example. 1 fig.

DOE Contract Number:
AC02-76ET25103
Assignee:
Dow Chemical Co., Midland, MI (United States)
Patent Number(s):
US 4505995; A
Application Number:
PPN: US 6-312588
OSTI ID:
7250598
Resource Relation:
Patent File Date: 19 Oct 1981
Country of Publication:
United States
Language:
English