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Formation and reactions of singlet oxygen, O[sub 2]([sup 1][Delta]g), under atmospheric conditions

Thesis/Dissertation ·
OSTI ID:7207250

Singlet molecular oxygen, O[sub 2]([sup 1][Delta][sub g]), plays a significant role in photochemical air pollution as a reactive and a deleterious oxidant. Gas phase O[sub 2]([sup 1][Delta][sub g]) formation by homogeneous photosensitization at atmospheric pressure was studied using a variety of compounds found in the atmosphere. The formation of O[sub 2]([sup 1][Delta][sub g]) was demonstrated by observing its 1.27 [mu]m emission using a liquid nitrogen-cooled germanium photodiode detector, and by performing chemical trapping studies with 2,3-dimethyl-2-butene (TME) and quenching studies with triethylamine (TEA). The factors affecting O[sub 2]([sup 1][Delta][sub g]) formation included sensitizer concentration, gas composition (%N[sub 2]/%O[sub 2]), total gas flow rate, irradiation wavelength, and light intensity. The disappearance of seven polycyclic aromatic hydrocarbons (PAHs) adsorbed on zeolite particles was studied under simulated atmospheric conditions. Benzo[ghi]perylene, chrysene, and benzo[e]pyrene were less susceptible to photooxidation than benz[a]anthracene (B[a]A), pyrene, dibenz[ah]anthracene, and benzo[a]pyrene. The disappearance of B[a]A in the presence of light and air involved a self-sensitized photooxidation with the formation of O[sub 2]([sup 1][Delta][sub g]) as a major process. These studies were directed at identifying viable processes for forming atmospheric O[sub 2]([sup 1][Delta][sub g]) and deleterious substances that might be formed when environmental pollutants react with O[sub 2]([sup 1][Delta][sub g]).

Research Organization:
Illinois Inst. of Tech., Chicago, IL (United States)
OSTI ID:
7207250
Country of Publication:
United States
Language:
English