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Behavior of titanium sublimation and sputter ion pumps in the 10/sup -11/ torr range

Conference ·
OSTI ID:7152287
In the proposed Intersecting Storage Accelerator, ISABELLE, 1200 pumping stations will be used to keep two 3 km long rings at a pressure of 1 x 10/sup -11/ torr. It is clear that in such a large system, price and simplicity are very important. A study was made on a well instrumented room temperature vacuum system with a surface area of 6000 cm/sup 2/ and a volume of 17 l, pumped by a Ti-ball and an ion pump. Total pressure and residual gas composition were measured by a Helmer gauge and a quadrupole mass spectrometer. The final pressures of approximately 1 x 10/sup -11/ torr were reached with Ti films and a 20 l s/sup -1/ sputter-ion pump. The main residual gas components were hydrogen and methane. The ultimate pressure was determined primarily by the ability of Ti films to pump H/sub 2/ which depends on the method of laying down the film and the surface temperature. Previous surface preparation seemed relatively unimportant. Two methods of pumping CH/sub 4/ were investigated: (1) cracking the molecules on hot tungsten filament; and (2) conventional sputter-ion pumping. Sputter-ion pumping was found to be more efficient and preferable.
Research Organization:
Brookhaven National Lab., Upton, N.Y. (USA)
DOE Contract Number:
E(30-1)-16
OSTI ID:
7152287
Report Number(s):
BNL-21615; CONF-760921-2
Country of Publication:
United States
Language:
English