Microstructural and crystallographic relationships in directionally solidified Nb-Cr[sub 2]Nb and Cr-Cr[sub 2]Nb eutectics

Journal Article · Mon Aug 01 04:00:00 EDT 1994 · Acta Metallurgica et Materialia; (United States)

DOI:https://doi.org/10.1016/0956-7151(94)90228-3· OSTI ID:6987574

Bewlay, B P; Sutliff, J A; Jackson, M R ^[1]; Lipsitt, H A ^[2]

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1. General Electric Co., Schenectady, NY (United States). Corporate Research and Development Center
2. Wright State Univ., Dayton, OH (United States). Dept. of Mechanical and Materials Engineering

The present paper describes processing, microstructures and phase relationships in directionally solidified Cr[sub 2]Nb-Nb and Cr[sub 2]Nb-C eutectics. Both of these eutectics, and the stoichiometric Laves phase Cr[sub 2]Nb, were directionally solidified using cold crucible Czochralski crystal growth with growth rates from 1 to 15 mm/min. Cr[sub 2]Nb-Nb had a rod/ribbon-type structure and Cr[sub 2]Nb-Cr had a lamellar structure. The crystallographic orientation relationships between both Cr and Nb and the Cr[sub 2]Nb Laves phase in the individual eutectics were characterized using transmission electron microscopy. Inter-phase orientation relationships in these eutectics were complicated by the transformation of Cr[sub 2]Nb from the C14 to the C15 crystal structure on post-solidification cooling. Twins were observed in the C15 Cr[sub 2]Nb phase in both the single phase and eutectic samples. The relationship between the twins, the C14-C15 transformation, and the eutectic morphology is also discussed.

• OSTI ID: 6987574
• Journal Information: Acta Metallurgica et Materialia; (United States), Journal Name: Acta Metallurgica et Materialia; (United States) Vol. 42:8; ISSN 0956-7151; ISSN AMATEB
• Country of Publication: United States
• Language: English

Related Subjects

36 MATERIALS SCIENCE
360102* -- Metals & Alloys-- Structure & Phase Studies
ALLOYS
CHROMIUM ALLOYS
MICROSTRUCTURE
NIOBIUM ALLOYS
PHASE STUDIES
PHASE TRANSFORMATIONS
SOLIDIFICATION