Synthesis of 8-phenyl-10H-pyrido(1,2-. cap alpha. )indole salts from 2,3,3-trimethyl-3H-indole chlorides with cinnamaldehyde

Journal Article · Thu Oct 01 04:00:00 EDT 1987 · Chem. Heterocycl. Compd. (Engl. Transl.); (United States)

DOI:https://doi.org/10.1007/BF00546734· OSTI ID:6909014

Shachkus, A A; Degutis, Yu A

Reaction of 2,3,3-trimethyl-3H-indole chloride with cinnamic and 4-dimethylaminocinnamic aldehydes led to salts of 8-phenyl and 8-(4-dimethylaminophenyl)-10,10-dimethyl-10H-pyrido(1,2-..cap alpha..)indole. PMR spectra were recorded on a Tesla BS-487C (80 MHz) instrument (internal standard HMDS) and IR spectra on a UR-20 spectrometer (KBr pellets).

• Research Organization: A. Snechkus Polytechnic Institute, Kaunas (USSR)
• OSTI ID: 6909014
• Journal Information: Chem. Heterocycl. Compd. (Engl. Transl.); (United States), Journal Name: Chem. Heterocycl. Compd. (Engl. Transl.); (United States) Vol. 23:4; ISSN CHCCA
• Country of Publication: United States
• Language: English

Related Subjects

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400201* -- Chemical & Physicochemical Properties
640302 -- Atomic
Molecular & Chemical Physics-- Atomic & Molecular Properties & Theory
74 ATOMIC AND MOLECULAR PHYSICS
ACETONITRILE
ALCOHOLS
ALDEHYDES
AMINES
AMMONIUM COMPOUNDS
AROMATICS
AZAARENES
AZINES
AZOLES
CARBOXYLIC ACIDS
CHEMICAL SHIFT
CHLORINE COMPOUNDS
CINNAMIC ACID
COUPLING
COUPLING CONSTANTS
DEUTERIUM COMPOUNDS
HALOGEN COMPOUNDS
HETEROCYCLIC COMPOUNDS
HYDROGEN COMPOUNDS
HYDROXY COMPOUNDS
INDOLES
INFRARED SPECTRA
INTERMEDIATE COUPLING
ISOTOPE EFFECTS
J-J COUPLING
METHANOL
MONOCARBOXYLIC ACIDS
NITRILES
NMR SPECTRA
ORGANIC ACIDS
ORGANIC CHLORINE COMPOUNDS
ORGANIC COMPOUNDS
ORGANIC HALOGEN COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
OXYGEN COMPOUNDS
PERCHLORATES
PYRIDINES
PYRIDINIUM COMPOUNDS
PYRROLES
QUATERNARY COMPOUNDS
SPECTRA
SYNTHESIS