Analysis of RDX and HMX in PBX 9404 by high performance liquid chromatography
An analysis for the HMX and RDX contents of PBX 9404 has been developed. Instrumental parmeters, such as column type, solvent, flow rate, and method of detection are discussed. The calibration method is examined, and precision and accuracy investigated. The average percent recovery of HMX is 98.75% with a standard deviation of 0.82%; for RDX, the percent recovery is 98.66% with a standard deviation of 0.27%.
- Research Organization:
- Mason and Hanger-Silas Mason Co., Inc., Amarillo, TX (USA)
- DOE Contract Number:
- AC04-76DP00487
- OSTI ID:
- 6788017
- Report Number(s):
- MHSMP-80-55
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400102 -- Chemical & Spectral Procedures
45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEFENSE
450100* -- Military Technology
Weaponry
& National Defense-- Chemical Explosions & Explosives
CHEMICAL ANALYSIS
CHEMICAL EXPLOSIVES
CHROMATOGRAPHY
EXPLOSIVES
LIQUID COLUMN CHROMATOGRAPHY
QUALITATIVE CHEMICAL ANALYSIS
SEPARATION PROCESSES
400102 -- Chemical & Spectral Procedures
45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEFENSE
450100* -- Military Technology
Weaponry
& National Defense-- Chemical Explosions & Explosives
CHEMICAL ANALYSIS
CHEMICAL EXPLOSIVES
CHROMATOGRAPHY
EXPLOSIVES
LIQUID COLUMN CHROMATOGRAPHY
QUALITATIVE CHEMICAL ANALYSIS
SEPARATION PROCESSES