Analysis of nitrocellulose and tris-beta-chloroethyl phosphate in PBX 9404 by high performance liquid chromatography
A procedure for determining the nitrocellulose and tris-beta-chloroethyl phosphate content in PBX 9404 by high performance liquid chromatography is discussed. For a sample which contained 2.88% NC, 2.87% was found with a standard deviation of 0.02%. The same sample, known to contain 2.72% CEF, was found to be composed of 2.69% CEF with a standard deviation of 0.04%.
- Research Organization:
- Mason and Hanger-Silas Mason Co., Inc., Amarillo, TX (USA)
- DOE Contract Number:
- AC04-76DP00487
- OSTI ID:
- 5100670
- Report Number(s):
- MHSMP-80-52
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400102 -- Chemical & Spectral Procedures
45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEFENSE
450100* -- Military Technology
Weaponry
& National Defense-- Chemical Explosions & Explosives
CHEMICAL ANALYSIS
CHEMICAL EXPLOSIVES
CHROMATOGRAPHY
EXPLOSIVES
LIQUID COLUMN CHROMATOGRAPHY
NITRO COMPOUNDS
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
ORGANIC PHOSPHORUS COMPOUNDS
QUANTITATIVE CHEMICAL ANALYSIS
SEPARATION PROCESSES
400102 -- Chemical & Spectral Procedures
45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEFENSE
450100* -- Military Technology
Weaponry
& National Defense-- Chemical Explosions & Explosives
CHEMICAL ANALYSIS
CHEMICAL EXPLOSIVES
CHROMATOGRAPHY
EXPLOSIVES
LIQUID COLUMN CHROMATOGRAPHY
NITRO COMPOUNDS
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
ORGANIC PHOSPHORUS COMPOUNDS
QUANTITATIVE CHEMICAL ANALYSIS
SEPARATION PROCESSES